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HomeMy WebLinkAboutThermal Energy Integrated Power Systems (TIPS) AK Coal 2008 append B through D4 [hermoEnergy Analysis of ThermoEnergy Integrated Power Systems in New Power Facilities Using Alaska Coals Interim Report Appendix B:Experimental Data Appendix C:Thar Phase Monitor Data Appendix D:Small Vessel Experiment Data Appendix E:Synthesis,Characterization And SO2 Oxidation Behavior Of Noble Metal Loaded (Pt,Pd)On Mixed Oxide Support (AI,0;3-TiO,) August 2008 Submitted by Alex Fassbender,Robert Henry,and Li Tao ThermoEnergy Corporation 5 Kane Industrial Drive Hudson,MA 01749 This work was sponsored by The Alaska Energy Authority Interim Draft Report Federal Grant Number EM-833233301-0 August 22,2008 Appendix B:Experimental Data BIA:Heat Exchanger Data,Pure Carbon Dioxide Run 1: Heat Exchanger Composition -Pure Carbon Dioxide Front Page - Water Flow Rate -1.3485 kg/min (0.022475 kg/s) Pressure Gauge -565 psi Pressure Transducer -600 psi Gas Inlet Temperature -130°C (266°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474TotalVolumeofSystem-0.00334 m? 287 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas GasiIn |GasIn_|Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In (°C)|Out Out Out (°C)Density |Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)|Coefficient |Transfer (lb/hr)(kg/m3)(U)Coefficient W/m2K (W/m2K) 26.53 42.19 |16.73 |22.17 19.68 |105.91 }128.40 60.17 62.38 63.70 |28.89 0.88 |5.67E+07 |2.16E+04 |0.0080 26.60 42.20 |16.61 |22.22 19.64 |106.00 |131.96 59.49 62.43 63.75 |28.75 0.87 |5.64E+07 |2.16E+04 |0.0079 23.22 39.93 16.64 |22.22 19.59 97.61 |133.66 $5.75 53.84 54.82 |25.08 0.86 |4.84E+07 |1.88E+04 |0.0077 26.49 42.10 |16.68 |22.26 19.60 |105.66 |134.45 58.86 62.94 64.29 |28.90 0.87 |5.57E+07 |2.14E+04 |0.0079 26.27 42.07]16.76]22.11 19.68 |105.45 |131.04 59.46 62.02 63.32 |28.63 0.87 |5.60E+07 |2.13E+04 |0.0080 26.42 42.09 |16.64]22.14]19.70]105.52 |130.60 59.59 61.64 62.93 |28.47 0.87 |5.62E+07 |2.14E+04 |0.0080 26.33 42.09 |16.71 |22.02 19.67 |105.52 |129.87 59.72 61.80 63.09 |28.57 0.87 |5.63E+07 |2.14E+04 |0.0080 26.42 42.11 16.76 |22.20]19.71 |105.59 |130.81 59.58 62.26 63.58 |28.75 0.87 |5.61E+07 |2.14E+04 |0.0080 26.53 42.20 |16.80 |22.28]19.71 |105.91 |131.77 59.52 62.86 64.20 |28.97 0.87 |5.63E+07 |2.15E+04 |0.0080 26.52 42.16}16.89 |22.39]19.75 |105.74 |133.52 59.13 63.27 64.63 |29.09 0.87 |5.58E+07 |2.14E+04 |0.0079 26.52 42.19 |16.94]22.39]19.80 |105.79 |133.52 59.18 63.24 64.59 |29.07 0.87 |5.59E+07 |2.14E+04 |0.0079 26.16 41.96 |17.00}22.28 |19.79 |104.91 |132.41 59.03 62.44 63.76 |28.79 0.87 |5.52E+07 |2.12E+04 |0.0079 26.14 42.04 |17.07 |22.08 19.83 |105.18 |127.90 60.04 62.20 63.51 |28.87 0.88 |5.61E+07 |2.13E+04 |0.0080 26.40 42.13 17.06 |22.25 19.80 |105.58 |129.02 59.96 63.18 64.54 |29.26 0.88 |5.62E+07 |2.15E+04 |0.0080 26.54 42.21 17.08 |22.41 19.82 |105.83 }131.87 59.51 63.81 65.19]29.41 0.87 |5.61E+07 |2.1SE+04 |0.0079 26.40 42.11 17.04 |22.45 19.87 |105.39 |133.57 59.04 63.02 64.36 |28.98 0.87 |5.55E+07 |2.14E+04 |0.0079 26.50 42.17 |17.03 |22.35 19.77 |105.73 |133.06 59.23 63.76 65.13 |29.34 0.87 |5.S9E+07 |2.14E+04 |0.0079 26.49 42.15 17.04 |22.47 |19.78 |105.66 |134.11 59.00 63.90 65.29 |29.36 0.87 |5.56E+07 |2.14E+04 |0.0079 26.42 42.16]16.94]22.48]19.88 |105.61 |133.28 59.18 62.51 63.83 |28.74 0.87 |5.58E+07 |2.14E+04 |0.0079 26.51 42.20 |16.92]22.54]19.89}105.72 |133.90 $9.11 62.68 64.02 |28.79 0.87 |5.58E+07 |2.14E+04 |0.0079 26.50 42.18 |17.00]22.58]19.95 |105.59 |135.02 58.88 62.73 64.06 |28.77 0.87 |5.56E+07 |2.14E+04 |0.0079 26.24 42.05 17.11 |22.42]19.96 |105.10 |133.29 59.01 62.46 63.78 |28.75 0.87 |5.53E+07 |2.12E+04 |0.0079 26.37 42.11 17.16 |22.44)19.94]105.34 |132.08 59.33 63.06 64.40 |29.07 0.87 |5.56E+07 |2.14E+04 |0.0079 25.84 41.78 |17.12]22.21 19.87 |104.17 |129.96 59.24 61.55 62.83 |28.53 0.87 |5.48E+07 |2.10E+04 |0.0079 288 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure Water Water Gas Gas GasIn GasIn Total Heat Gas Side Nu Pr Gr Re Friction Flow (bar)In@C)Out Out Out (°C)Density Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)Coefficient Transfer (lb/hr)(kg/m3)(U)Coefficient W/m2K (W/m2K) 25.34 41.55 |17.12}21.92]19.87}103.29 |125.89 59.68 59.80 61.01 |27.93 0.88 |5.46E+07 |2.07E+04 |0.0080 26.23 42.00 |16.91}22.29)19.78 |105.11 |131.80 $9.23 62.23 63.55]28.71 0.87 |5.55E+07 |2.13E+04 |0.0079 Red data is an average of all data points. Run 2: Heat Exchanger Composition -Pure Carbon Dioxide Front Page - Water Flow Rate -1.3 kg/min (0.021667 kg/s) Pressure Gauge -525 psi Pressure Transducer -562 psi Gas Inlet Temperature 258°C (500°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474TotalVolumeofSystem-0.00334 m 289 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Gas In |GasIn |Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In (°C)|Out Out Out (PC)Density |Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)|Coefficient |Transfer (lb/hr)(kg/m3)(U)Coefficient W/m2K (W/m2K) 26.53 42.19 16.73 |22.17]19.68 |105.91 |128.40 60.17 62.38 63.70 |28.89 0.88 |5.67E+07 |2.16E+04 |0.0080 26.60 42.20 |16.61 |22.22]19.64]106.00 |131.96 59.49 62.43 63.75 |28.75 0.87 |5.64E+07 |2.16E+04 |0.0079 23.22 39.93 16.64 |22.22 |19.59 97.61 |133.66 55.75 53.84 $4.82 |25.08 0.86 |4.84E+07 |1.88E+04 |0.0077 26.49 42.10 |16.68 |22.26]19.60]105.66 |134.45 58.86 62.94 64.29 |28.90 0.87 |5.S7E+07 |2.14E+04 |0.0079 26.27 42.07 |16.76]22.11 19.68 |105.45 |131.04 59.46 62.02 63.32 |28.63 0.87 |5.60E+07 |2.13E+04 |0.0080 26.42 42.09 |16.64}22.14]19.70]105.52 |130.60 $9.59 61.64 62.93 |28.47 0.87 |5.62E+07 |2.14E+04 |0.0080 26.33 42.09 |16.71 |22.02]19.67 |105.52 |129.87 59.72 61.80 63.09 |28.57 0.87 |5.63E+07 |2.14E+04 |0.0080 26.42 42.11 16.76 |22.20}19.71 |105.59 |130.81 59.58 62.26 63.58 |28.75 0.87 |5.61E+07 |2.14E+04 |0.0080 26.53 42.20 |16.80}22.28]19.71 |105.91 |131.77 59.52 62.86 64.20 |28.97 0.87 |5.63E+07 |2.15E+04 |0.0080 26.52 42.16 |16.89]22.39]19.75 |105.74 |133.52 59.13 63.27 64.63 |29,09 0.87 |5.58E+07 |2.14E+04 |0.0079 26.52 42.19 |16.94]22.39]19.80]105.79 |133.52 59.18 63.24 64.59 |29.07 0.87 |5.S9E+07 |2.14E+04 |0.0079 26.16 41.96}17.00}22.28)19.79 |104.91 |132.41 59.03 62.44 63.76 |28.79 0.87 |5.52E+07 |2.12E+04 |0.0079 26.14 42.04 |17.07]22.08]19.83 |105.18 |127.90 60.04 62.20 63.51 |28.87 0.88 |5.61E+07 |2.13E+04 |0.0080 26.40 42.13 17.06 |22.25]19.80}105.58 |129.02 59.96 63.18 64.54 |29.26 0.88 |5.62E+07 |2.1SE+04 |0.0080 26.54 42.21 17.08 |22.41 19.82 |105.83 |131.87 59.51 63.81 65.19 |29.41 0.87 |5.61E+07 |2.1SE+04 |0.0079 26.40 42.11 17.04 |22.45]19.87]105.39 |133.57 59.04 63.02 64.36 |28.98 0.87 |5.55E+07 |2.14E+04 |0.0079 26.50 42.17 |17.03 |22.35]19.77 |105.73 |133.06 59.23 63.76 65.13 |29.34 0.87 |5.59E+07 |2.14E+04 |0.0079 26.49 42.15 17.04 |22.47}19.78 |105.66 |134.11 59.00 63.90 65.29 |29.36 0.87 |5.56E+07 |2.14E+04 |0.0079 26.42 42.16 16.94 |22.48]19.88]105.61 |133.28 59.18 62.51 63.83 |28.74 0.87 |5.58E+07 |2.14E+04 |0.0079 26.51 42.20 |16.92 |22.54]19.89]105.72 |133.90 59.11 62.68 64.02 |28.79 0.87 |5.58E+07 |2.14E+04 |0.0079 26.50 42.18 17.00 }22.58]19.95}105.59 |135.02 58.88 62.73 64.06 |28.77 0.87 |5.S6E+07 |2.14E+04 |0.0079 26.24 42.05 17.11 |22.42 |19.96]105.10 |133.29 59.01 62.46 63.78 |28.75 0.87 |5.53E+07 |2.12E+04 |0.0079 26.37 42.11 17.16}22.44]19.94]105.34 |132.08 59.33 63.06 64.40 |29.07 0.87 |5.56E+07 |2.14E+04 |0.0079 25.84 41.78 17.12 }22.21 19.87 |104.17 |129.96 59.24 61.55 62.83 |28.53 0.87 |5.48E+07 |2.10E+04 |0.0079 290 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure Water Water Gas Gas GasIn GasIn Total Heat Gas Side Nu Pr Gr Re Friction Flow (bar)In(°C)Out Out Out (°C)Density Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)Coefficient Transfer (Ib/hr)(kg/m3)(VU)Coefficient W/m2K (W/m2K) 25.34 41.55 |17.12]21.92]19.87 |103.29 |125.89 59.68 59.80 61.01 |27.93 0.88 |5.46E+07 |2.07E+04 |0.0080 26,23 42.00}16.91 |22.29]19.78 |105.11 |131.80 59,23 62.23 63.55 |28.71 0.87 |5.55E+07 |2.13E+04 |0.0079 Red data is an average of all data points. Run 3: Heat Exchanger Composition -Pure Carbon Dioxide Front Page - Water Flow Rate -1.3 kg/min (0.021667 kg/s) Pressure Gauge -525 psi Pressure Transducer -562 psi Gas Inlet Temperature -258°C (500°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater-0.000282474 Total Volume of System -0.00334 m2 291 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Gas In |GasIn |Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In (°C)|Out Out Out (°C)Density |Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)|Coefficient |Transfer (lb/hr)(kg/m3)(U)Coefficient W/m2K (W/m2K) 23.55 38.80 |15.76]25.70}18.13 94.86 |258.50 39.41 65.31 66.76 |25.48 0.78 |7.29E-1.67E+04 |0.0059 23.55 38.80 |15.72}25.63 |18.05 94.92 |258.40 39.42 65.57 67.03 |25.59 0.78 733 E-1.67E+04 |0.0059 23.55 38.80 |15.80]25.71 18.09 94.91 |259.24 39.36 65.87 67.35 |25.68 0.78 TE:1.67E+04 |0.0059 23.55 38.80 |15.81 |25.79]18.16 94.85 |259.51 39.34 65.44 66.90 |25.50 0.78 TE:1.67E+04 |0.0059 23.54 38.81 15.82 |25.86]18.17 94.86 |259.63 39.33 65.50 66.95 |25.52 0.78 TEE.1.67E+04 |0.0059 23.54 38.80 |15.78 |25.88]18.26 94.77 |259.70 39.32 64.78 66.20 |25.23 0.78 BE.1.67E+04 |0.0059 23.54 38.79 |15.77 |25.81 18.13 94.83 |259.50 39.32 65.40 66.85 |25.48 0.78 730E-1.67E+04 |0.0059 23.53 38.80 |15.84]25.91 18.28 94.72 |259.87 39.30 64.95 66.38 |25.29 0.78 aE:1.66E+04 |0.0059 23.53 38.78 |15.77]25.79 |18.23 94.72 |259.44 39.32 64.78 66.20 |25.24 0.78 aE.1.67E+04 |0.0059 23.53 38.79 |15.84]25.864 18.24 94.73 |259.43 39.33 65.19 66.64 |25.40 0.78 TIE.1.67E+04 |0.0059 23.53 38.79 |15.79 |25.87]18.19 94.76 |259.13 39.35 65.09 66.53 |25.38 0.78 T35E-1.67E+04 |0.0059 23.52 38.77 |15.79]25.85]18.16 94.74 |258.54 39.38 65.27 66.71 |25.47 0.78 TIE.1.67E+04 |0.0059 23.52 38.77 |15.79]25.85]18.21 94.68 |258.59 39.38 64.95 66.38 |25.34 0.78 TE.1.67E+04 |0.0059 23.50 38.77 |15.83 |25.83]18.31 94.59 |258.84 39.35 64.54 65.95 |25.17 0.78 TATE.1.66E+04 |0.0059 23.51 38.76 |15.81 |25.83 |18.24 94.63 |258.37 39.39 64.84 66.27 |25.30 0.78 THE 1.67E+04 |0.0059 292 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas -Gas In |GasIn |Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In (CC)|Out Out Out (°C)Density |Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)|Coefficient |Transfer (lb/hr)(kg/m3)(U)Coefficient W/m2K (W/m2K) 23.50 38.76 |15.83}25.88]18.25 94.61 |258.22 39.40 64.92 66.35 |25.34 0.78 |7.36E-1.67E+04 |0.0059 23.50 38.74 |15.71 |25.77]18.19 94.62 |257.97 39.40 64.56 65.97 |25.21 0.78 TE.1.67E+04 |0.0059 23.50 38.76 |15.89]25.78)18.18 94.66 |258.47 39.37 65.61 67.07 |25.61 0.78 TIE.1.67E+04 |0.0059 23.50 38.76 |15.85]25.83 |18.34 94.55 |258.21 39.40 64.43 65.84 |25.15 0.78 VTE.1.67E+04 |0.0059 23.49 38.79 |16.08}25.90]18.63 94.41 |258.59 39.40 64.02 65.41 |24.97 0.78 TSE 1.66E+04 |0.0059 23.49 38.81 |16.10}26.03 |18.71 94.40 |258.69 39.41 63.74 65.11}24.85 0.78 7 OE.1.66E+04 |0.0059 23.49 38.80 |15.91 |25.94]18.60 94.46 |258.54 39.41 63.37 64.73 |24.71 0.78 TE.1.66E+04 |0.0059 23.49 38.79 |16.00]25.91]18.53 94.48 |258.05 39.44 64.19 65.59 |25.05 0.78 73E-1.66E+04 |0.0059 23.49 38.79 |16.01]25.95 |18.64 94.39 |258.31 39.42 63.61 64.98 |24.81 0.78 7 OTE.1.66E+04 |0.0059 23.49 38.79 |16.03 |25.96]18.58 94.45 |258.31 39.42 64.04 65.43 |24.98 0.78 7SE-1.66E+04 |0.0059 23.49 38.79 |16.05 |25.97]18.59 94.42 |258.63 39.39 64.09 65.49 |25.00 0.78 7 TE.1.66E+04 |0.0059 23.48 38.79 |16.02}25.93]18.74 94.31 |259.00 39.36 63.15 64.51 |24.61 0.78 7 DE 1.66E+04 |0.0059 23.49 38.78 |15.95 |25.88}18.69 94.33 |258.91 39.37 63.10 64.45 |24.59 0.78 TBE.1.66E+04 |0.0059 23.49 38.78 |15.96 |25.83]18.55 94.42 |259.20 39.34 63.87 65.25 |24.89 0.78 7 GE.1.66E+04 |0.0059 09 293 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Gas In |GasIn_|Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In °C)|Out Out Out (°C)Density |Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)|Coefficient |Transfer (lb/hr)(kg/m3)(VU)Coefficient W/m2K (W/m2K) 23.49 38.78 |16.01 |25.89]18.62 94.35 |259.02 39.35 63.74 65.12 |24.84 0.78 |7.67E-09 1.66E+04 |0.0059 23.49 38.78 |16.00 |25.87]18.64 94.34 |259.16 39.34 63.60 64.97 |24.78 0.78 |7.71E-1.66E+04 |0.0059 23.49 38.77 |16.02}25.94]18.64 94.33 |259.06 39.34 63.72 65.10 |24.84 0.78 OTE 1.66E+04 |0.0059 23.50 38.77 |15.90 {25.91 18.62 94.33 |259.10 39.33 63.21 64.57 |24.63 0.78 THE:1.66E+04 |0.0059 23.48 38.77 |16.00}25.94]18.63 94.32 |259.17 39.33 63.64 65.02 |24.80 0.78 770E-1.66E+04 |0.0059 23.48 38.78 |16.05 |26.01 18.68 94.31 |259.24 39.33 63.66 65.04 |24.81 0.78 7 OE:1.66E+04 |0.0059 23.47 38.80 |16.19}26.08 |18.88 94.23 |259.68 39.32 63.23 64.59 |24.62 0.78 TIE 1.66E+04 |0.0059 23.48 38.81 16.13 |26.10]18.81 94.32 |259.51 39.34 63.34 64.70 |24.66 0.78 aE 1.66E+04 |0.0059 23.47 38.81 16.14 |26.08 |18.87 94.25 |259.51 39.34 63.08 64.43 |24.56 0.78 TE.1.66E+04 |0.0059 23.47 38.80 |16.10]26.03 |18.79 94.29 |259.38 39.34 63.30 64.66 |24.65 0.78 775E.1.66E+04 |0.0059 23.47 38.80 |16.14]26.08]18.84 94.26 |259.34 39.35 63.20 64.55 |24.61 0.78 7aIE-1.66E+04 |0.0059 23.47 38.79 |16.09]26.06]18.77 94.29 |259.38 39.34 63.32 64.68 |24.66 0.78 775E:1.66E+04 |0.0059 23.47 38.79 |16.05 |26.09]18.83 94,23 |259.52 39,32 62.84 64.18 |24.47 0.78 751 E-1.66E+04 |0.0059 23.46 38.78 |15.98]26.11 18.78 94.24 |259.20 39.34 62.68 64.01 |24.42 0.78 79E-1.66E+04 |0.0059 23.46 38.78 |15.99]26.07]18.79 94,23 |259.43 39.32 62.70 64.03 |24.42 0.78 7O4E.1.66E+04 |0.0059 23.45 38.78 |16.06}26.13 |18.84 94.17 |258.97 39.35 62.77 64.10 |24.46 0.78 SE 1.66E+04 |0.0059 294 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Gas In |GasIn |Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In CC)|Out Out Out (°C)Density |Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)|Coefficient |Transfer (lb/hr)(kg/m3)(U)Coefficient W/m2K (W/m2K) 23.45 38.76 |15.92]26.08]18.84 94.12 |258.77 39.35 62.08 63.38 |24.19 0.78 |8.08E-1.66E+04 |0.0059 23.44 38.77 |15.98]26.02 |18.97 94.03 |258.81 39.36 61.71 63.00 |24.05 0.78 a 8E-1.66E+04 |0.0059 23.44 38.77 |16.06}26.11]18.95 94.04 |258.70 39.37 62.11 63.42}24.21 0.78 37E-1.66E+04 |0.0059 23.44 38.77 |16.09}26.10}19.06 93.98 |258.96 39.35 61.80 63.10 |24.08 0.78 *6E-1.66E+04 |0.0059 23.44 38.75 |15.87]26.02 |18.80 94.10 |258.40 39.37 61.97 63.27 |24.17 0.78 3 10E-1.66E+04 |0.0059 23.43 38.75 |15.94}26.00]18.80 94.10 |258.49 39.36 62.33 63.64 |24.30 0.78 S00 1.66E+04 |0.0059 23.43 38.76 |16.03]26.09]18.82 94.12 |259.06 39.33 62.67 64.00 |24.42 0.78 73.1.66E+04 |0.0059 23.44 38.79 |16.10]26.08)18.84 94.22 |258.66 39.39 62.86 64.20 |24.51 0.78 TE.1.66E+04 |0.0059 23.43 38.79 |16.08]26.13 |18.95 94.14 |258.16 39.44 62.24 63.55 |24.27 0.78 SOE:1.66E+04 |0.0059 23.43 38.78 |16.05 |26.08]19.06 94.00 |258.22 39.42 61.51 62.79 |23.99 0.78 321E-1.66E+04 |0.0059 23.43 38.77 |16.00]25.98 |19.06 93.96 |258.16 39.41 61.25 62.53 |23.89 0.78 325E-1.66E+04 |0.0059 23.43 38.76 |15.92 |25.89]19.04 93.93 |257.74 39.43 61.00 62.26 |23.80 0.78 3uE-1.66E+04 |0.0059 23.49 38.78 |15.95]25.94}18.58 94.41 |258.89 39.37 63.68 65.06 |24.82 0.78 TOE.1.66E+04 |0.0059 09 Red data is an average of all data points. 295 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Run 4: Heat Exchanger Composition -Pure Carbon Dioxide Front Page - Water Flow Rate -0.438 kg/min (0.0073 kg/s) Pressure Gauge -475 psi Pressure Transducer -507 psi Gas Inlet Temperature -140°C (280°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 296 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Gas In |GasIn |Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In CC)|Out Out Out (°C)Density |Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)|Coefficient |Transfer (lb/hr)(kg/m3)(VU)Coefficient W/m2K (W/m2K) 19.66 35.04]16.63}2859]18.06 82.20 |138.76 47.74 55.18 56.21 |26.28 0.84 |4.35E-1.60E+04 |0.0068 19.71 35.04 |16.54}29.07]18.14 82.18 |142.94 47.16 54.21 $5.20 |25.63 0.84 1OTE.1.60E+04 |0.0068 19.67 35.00 |]16.44]29.08]18.12 82.06 |144.54 46.88 53.60 54.57 |25.28 0.84 TUE 1.59E+04 |0.0068 19.59 34.91 16.54 |29.07]18.09 81.79 |144.60 46.74 54.34 55.34 |25.64 0.84 770E-L.58E+04 |0.0067 19.23 34.67 |16.46]28.91 |18.07 81.01 |141.31 46.84 52.59 53.53 |24.97 0.84 TE.1.56E+04 |0.0068 19.14 34.72 |16.41 |28.29]18.06 81.20 |134.99 47.82 51.67 52.57 |24.79 0.84 TE.1.57E+04 |0.0069 19.43 34.89 |16.54]2841]18.02 81.76 |134.40 48.16 53.89 54.87 |25.87 0.84 13EE 1.59E+04 |0.0069 19.56 34.94]16.69}28.95]18.10 81.89 |137.97 47.72 55.06 56.09 |26.28 0.84 73 1E-1.59E+04 |0.0068 19.35 34.77 |16.77}29.11 |18.22 81.27 |139.99 47.18 54.21 $5.21 |25.80 0.84 G 1E-1.57E+04 |0.0068 19,22 34.79 |16.67 |28.77)18.27 81.28 |136.87 47.65 52.41 53.33 |25.05 0.84 TE 1.57E+04 |0.0069 19.48 34.94 |16.47]28.85]18.22 81.80 |136.52 47.93 52.14 53.06 }24.92 0.84 aE.1.59E+04 |0.0069 19.62 34.99 |16.54]29.14}18.16 81.99 |139.83 47.52 53.75 $4.73 |25.55 0.84 TOE.1.59E+04 |0.0068 19.59 34.97 |16.69 |29.44]18.18 81.92 |142.37 47.13 54.82 55.83 |25.96 0.84 aSIE.1.59E+04 |0.0068 19.64 35.00 |16.78 |29.69]18.26 81.96 |143.89 46.96 55.25 56.28 |26.09 0.84 1 1.59E+04 |0.0068 297 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Gas In |GasIn |Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In (°C)|Out Out Out (°C)Density |Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)|Coefficient |Transfer (lb/hr)(kg/m3)(U)Coefficient W/m2K (W/m2K) 19.41 34.81 16.81 |29.37 |18.34 81.31 |143.68 46.72 53.90 54.88 |25.48 0.84 |4.71E-1.57E+04 |0.0068 19.26 34.81 16.79 |28.66]18.34 81.31 |139.36 47.33 52.89 53.83 |25.18 0.84 TE 1.57E+04 |0.0068 19.45 34.90 |16.79}28.60]18.36 81.58 |138.17 47.62 53.26 54.22 |25.39 0.84 TOE.1.58E+04 |0.0068 19.25 34.71 16.80 |28.50]18.34 80.98 |138.52 47.30 52.79 53.73 |25.18 0.84 TE:1.57E+04 |0.0068 19.12 34.72 |16.78 |28.06]18.30 81.05 |135.08 47.81 52.31 53.23 |25.09 0.84 TORE.1.56E+04 |0.0069 19.39 34.89 |16.78 |28.32]18.32 81.57 |134.68 48.12 53.09 54.04 |25.47 0.84 T3E.1.59E+04 |0.0069 19.31 34.80 |16.80]28.47]18.31 81.28 |136.92 47.66 53.20 $4.16 |25.43 0.84 7555.1.58E+04 |0.0069 19.45 34.92 |16.791 28.58}18.35 81.66 |137.54 47.75 53.29 $4.25 |25.43 0.84 TOE 1.59E+04 |0.0069 19.53 34.96 |16.83 |28.85]18.35 81.77 |140.16 47.42 53.99 54.98 |25.66 0.84 750.1.59E+04 |0.0068 19.43 34.84 |16.84]29.40]18.38 81.38 |141.74 47.03 53.84 54.81}25.53 0.84 TIE.1.58E+04 |0.0068 19.06 34.59 |16.75 |29.03 |18.40 80.56 |138.54 47.12 51.63 52.53 |24.63 0.84 IIE.1.55E+04 |0.0068 19.42 34.87 |16.68]28.85}18.23 81.55 |139.34 47.41 53.49 54.46 |25.46 0.84 TOE.1.58E+04 |0.0068 09 Red data is an average of all data points. 298 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Run 5: Heat Exchanger Composition -Pure Carbon Dioxide Front Page -- Water Flow Rate -0.49 kg/min (0.008167 kg/s) Pressure Gauge -210 psi Pressure Transducer -220 psi Gas Inlet Temperature -190°C (375°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 299 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Gas In |GasIn |Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In (°C)|Out Out Out (°C)Density |Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)|Coefficient |Transfer (Ib/hr)(kg/m3)(U)Coefficient W/m2K (W/m2K) 6.32 15.13 |16.42)21.73]18.33 30.07 |186.42 17.71 14.95 15.02 6.95 0.77 |6.78E-4.94E+03 |0.0034 6.31 15.15 |16.46)21.63]18.31 30.11 |186.46 17.73 15.02 15.10 6.98 0.77 SE.4.93E+03 |0.0034 6.34 15.16]16.54]21.70]18.34 30.13 |187.22 17.71 15.20 15.27 7.06 0.77 SSE.4.95E+03 |0.0034 6.36 15.16 |16.42]21.86]18.38 30.13 |188.22 17.67 14.98 15.05 6.94 0.77 SE.4.95E+03 |0.0034 6.36 15.17 |16.42]21.83]18.35 30.15 |189.23 17.64 15.07 15.14 6.97 0.77 a 1E-4.95E+03 |0.0034 6.35 15.17 |16.47]21.84]18.33 30.16 |190.31 17.60 15.19 15.27 7.02 0.77 65E-4.94E+03 |0.0034 6.38 15.17 |16.55]21.92 |18.37 30.14 |191.38 17.55 15.36 15.44 7.08 0.77 5 GE.4.96E+03 |0.0034 6.37 15.17 |16.74]21.99]18.38 30.15 |192.12 17.52 15.69 15.77 7.22 0.77 SAE.4.95E+03 |0.0034 6.35 15.18 |16.77}22.02]18.44 30.17 |192.36 17.53 15.57 15.65 7.17 0.77 33 1E-4.93E+03 |0.0034 6.42 15.15 |16.61]22.05]18.49 30.10 |192.66 17.48 15.36 15.44 7.06 0.77 SE:4.98E+03 |0.0034 6.40 15.14]16.45]21.95]18.45 30.07 |192.63 17.46 15.12 15.19 6.95 0.77 SOT:4.97E+03 |0.0034 6.43 15.11 16.42 |21.82]18.44 30.00 |191.72 17.47 15.11 15.19 6.96 0.77 6.50E-4.99E+03 |0.0034 6.47 15.05 |16.40]21.72]18.39 29.89 |190.81 17.44 15.22 15.30 7.02 0.77 S75E-5.03E+03 |0.0033 6.46 14.97 |16.23]21.56]18.35 29.73 |188.97 17.42 14.97 15.04 6.93 0.77 55 5.04E+03 |0.0033 300 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water }|Water |Gas Gas Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In (°C)|Out Out Out (°C)Density |Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)|Coefficient |Transfer (lb/hr)(kg/m3)(U)Coefficient W/m2K (W/m2K) 6.42 14.91 16.17 |21.38}18.27 29.59 |185.45 17.48 14.81 14.88 6.90 0.77 |6.86E-5.02E+03 |0.0033 08 6.32 14.91 16.17 |21.17 18.21 29.60 |181.81 17.64 14.60 14.67 6.85 0.77 |6.87E-4.97E+03 |0.0034 08 6.38 15.11 16.45 21.76 18.36 30.01 |189.24 17.56 15.14 15.21 7.00 0.77 |6.75E-4.97E+03 |0.0034 08 Red data is an average of all data points. Run 6: Heat-Exchanger Composition -Pure Carbon Dioxide Front Page - Water Flow Rate -0.447 kg/min (0.00745 kg/s) Pressure Gauge -210 psi Pressure Transducer -215 psi Gas Inlet Temperature -135°C (275°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 301 Mass Pressure }Water |Water |Gas Gas Gas In |GasIn |Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In (°C)|Out Out Out (°C)Density |Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)|Coefficient |Transfer (Ib/hr)(kg/m3)(U)Coefficient W/m2K (W/m2K) 6.30 14.88 |16.87,20.85]18.82 29.46 |137.24 19.68 13.55 13.61 6.89 0.78 |5.39E-§.24E+03 |0.0036 6.26 14.82 |16.85 |20.89]18.80 29.32 |139.96 19.45 13.54 13.61 6.85 0.78 SHE 5.19E+03 |0.0036 6.18 14.79 |16.76}20.80]18.82 29.26 |140.18 19.40 13.18 13.23 6.66 0.78 SE 5.12E+03 |0.0036 6.15 14.77 |16.68 |20.67]18.83 29.22 |138.65 19.46 12.94 13.00 6.56 0.78 SOE:5.10E+03 |0.0036 6.11 14.75 |16.62]20.60]18.76 29.18 |136.33 19.55 12.79 12.85 6.51 0.78 6.00E-5.08E+03 |0.0036 6.10 14.74 |16.74]20.54]18.78 29.15 |133.94 19.65 12.85 12.91 6.58 0.78 30 5.09E+03 |0.0036 6.06 14.71 16.81 |20.54]18.68 29.11 |131.89 19.73 13.00 13.06 6.68 0.78 SE 5.08E+03 |0.0036 6.05 14.74]16.89 |20.54]18.73 29.17 |130.28 19.86 12.97 13.02 6.68 0.78 SE.5.08E+03 |0.0037 6.05 14.82 |16.95]20.62]18.80 29.33 |129.26 20.02 12.94 12.99 6.68 0.78 SE.5.09E+03 |0.0037 6.13 14.82 |16.87 |20.72]18.85 29.32 |129,33 20.02 12.89 12.95 6.65 0.78 SAE.5.14E+03 |0.0037 6.15 14.78 |16.69 |20.73 |18.79 29.24 |130.14 19.92 12.78 12.83 6.58 0.78 3 OE.§.16E+03 |0.0037 6.14 14.73 |16.72]20.60]18.76 29.13 |131.12 19.79 12.87 12.92 6.62 0.78 ae 5.14E+03 |0.0036 6.09 14.68 |16.73 |20.61 18.83 29.01 |130.90 19.73 12.67 12.73 6.52 0.78 3T7E 5.11E+03 |0.0036 6.02 14.641 16.83 |20.52]18.86 28.94 |129.47 19.76 12.56 12.62 6.48 0.78 SE 5.05E+03 |0.0036 302 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Gas In |GasIn |Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In (°C)|Out Out Out (°C)Density |Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)|Coefficient |Transfer (lb/hr)(kg/m3)(U)Coefficient W/m2K (W/m2K) 5.96 14.72}16.91]20.45 |18.93 29.10 |127.42 19.98 12.39 12.44 6.42 0.78 |5.83E-5.01E+03 |0.0037 5.98 14.80}16.95]20.44]18.98 29.26 |125.78 20.18 12.38 12.43 6.43 0.78 SE -|5.05E+03 |0.0037 6.05 14.83 |16.81 |20.53 |19.09 29.31 |125.88 20.22 12.18 12.23 6.33 0.78 355 $.11E+03 |0.0037 6.13 14.82 |16.74]20.50]19.02 29.31 |127.28 20.14 12.38 12.43 6.41 0.78 SBE 5.16E+03 |0.0037 6.13 14.86 |16.67}20.44]18.96 29.38 |129.46 20.06 12.43 12.48 6.41 0.78 SOE:5.15E+03 |0.0037 6.19 14.83 |16.36]20.52]18.88 29.33 |131.51 19.91 12.35 12.40 6.35 0.78 SIGE 5.19E+03 |0.0037 6.18 14.83 |16.22}20.37]18.74 29.36 |133.55 19.80 12.38 12.43 6.34 0.78 Sa7E-5.16E+03 |0.0036 6.20 14.84]16.24]20.22]18.62 29.39 |134.86 19.74 12.64 12.69 6.45 0.78 SE.5.17E+03 |0.0036 6.20 14.83 |16.32 |20.24]18.62 29.37 |135.91 19.67 12.76 12.82 6.51 0.78 oO:5.17E+03 |0.0036 6.19 14.85 |16.27]20.39}18.62 29.41 .136.60 19.67 12.71 12.77 6.47 0.78 6 DE 5.15E+03 |0.0036 6.20 14.85}16.23}2040]18.56 29.42 |137.41 19.62 12.79 12.84 6.50 0.78 5.10.5.16E+03 |0.0036 6.22 14.84]16.27]20.42]18.53 29.41 |137.92 19.59 12.93 12.99 6.57 0.78 SOE.5.17E+03 |0.0036 6.22 14.80 |16.43]20.47]18.55 29.32 |138.31 19.51 13.15 13.20 6.67 0.78 3 1E-5.16E+03 |0.0036 6.17 14.81 16.44 |20.51 |18.52 29.34 |138.15 19.53 13.09 13.15 6.65 0.78 Sue 5.12E+03 |0.0036 6.16 14.85 |16.34]20.56]18.60 29.42 |137.67 19.61 12.80 12.85 6.50 0.78 3 10E-5.12E+03 |0.0036 08 303 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Gas In |GasIn_|Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In (°C)|Out Out Out (°C)Density |Transfer Heat Factor Meter (°C)(°C)Density (kg/m3)|Coefficient |Transfer (lb/hr)(kg/m3)(U)Coefficient W/m2K (W/m2K) 6.19 14.84]16.36]20.50]18.53 29.40 |137.28 19.62 12.98 13.04 6.60 0.78 |5.90E-5.15E+03 |0.0036 08 6.21 14.84]1641]20.50]18.58 29.39 |137.28 19.61 13.01 13.07 6.61 0.78 |5.87E-5.16E+03 |0.0036 08 6.14 14.80 |16.61}20.54]18.76 29.28 |133.58 19.76 12.80 12.86 6.55 0.78 |5.84E-5.13E+03 |0.0036 08 Red data is an average of all data points. 304 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 B1B:Heat Exchanger Data,Carbon Dioxide,Argon Heat Exchanger Data Components - Argon Carbon Dioxide GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0.31822 |0.31283 |0.31621 0.31635 |0.315903 Carbon Dioxide |96.71808 |96.25893 |96.13338 |96.20953 |96.32998 Argon 1.00853 |0.99191 1.00933 1.00831 1.00452 GC Run 1: Agilent Cerity QA/QC Report Sample name:*Reprocessed:0618-HeatXGRArC0012 Sample note: Submission time:Wednesday,June 18,2008 1:37:17 PM Operator: Injection date:Wednesday,June 18,2008 1:41:14 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:June11Calibration2 Method last saved:Friday,June 13,2008 4:08:30 PM 305 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA min2515 TCDZ2A 05 HEMGFLO tiiiiiaai Aq ong ado o0s- eoseecee + nytenonenaan min2515 TCDOZ A i 15 306 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 ESTD Report Calibration last saved:Wednesday,June 18,2008 2:20:06 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s] 1 0.853 - 1 0.973 - 2 0.292 BP 2.5210e+004 2 0.325 VB 2.1926e+006 2 1.503 - 3 1.341 BB 6177.74887 3 2.618 - Total amount =97.45892 Report summary: Warning(s):Calibrated compound(s)not found . Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 2: Agilent Cerity QA/QC Report Sample name:*Reprocessed:0618-HeatXGRArC0013 Sample note: Submission time:Wednesday,June 18,2008 1:37:18 PM Operator: Injection date:Wednesday,June 18,2008 1:44:46 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A 307 Amt/Area Amount [mass%]Name --Oxygen --Nitrogen 1.25431e-005 0.31621 Oxygen/Nitrogen 4.38439e-005 96.13338 Carbon Dioxide --Sulfur Dioxide 1.63381e-004 1.00933 Argon/Oxygen --Nitrogen_2 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Method:June11Calibration2 Method last saved:Friday,June 13,2008 4:08:30 PM 308 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCD1A min2515 TCD2A 0.6 rae min250.5 TCD3 A Bixkosucbry - Spey eb iae min2615 309 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 ESTD Report Calibration last saved:Wednesday,June 18,2008 2:20:06 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount [mass%] 1 0.853 --- 1 0.973 --- 2 0.292 BP 2.5370e+004 1.25431e-005 0.31822 2 0.324 VB 2.2060e+006 4.38439e-005 96.71808 2 1.503 --- 3 1.343 BB 6172.87286 1.63381e-004 1.00853 3 2.618 --- Total amount =98.04483 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 3: Agilent Cerity QA/QC Report Sample name:*Reprocessed:0618-HeatXGRArCOO11 Sample note: Submission time:Wednesday,June 18,2008 1:37:16 PM Operator: Injection date:Wednesday,June 18,2008 1:37:39 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:June11Calibration2 310 Name Oxygen Nitrogen Oxygen/Nitrogen Carbon Dioxide Sulfur Dioxide Argon/Oxygen Nitrogen_2 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Method last saved:Friday,June 13,2008 4:08:30 PM TCDIA >.,..=a ::>:OQ ... oa os --1 +aa more be ,co!: r :1 "46 ! o 4 : .a, r t TT T T 08 1 15 2 25 min TCD2A poe toy lo,ee [| .4:a :"he 1 'ft {,|ia7| }whe ra ro +4 T T --T 4 15 2 25 mir TCDSA i 1 Ai Zn =+a ne na tema §etc tt ch :c=:Be.+ i QO.ive)| i i ;;/B! :ae i OQ ;i o :°! |7 | T T +T T r 4 15 2 25 min 311 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 ESTD Report Calibration last saved:Wednesday,June 18,2008 2:20:06 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [iV's]Amt/Area Amount [mass%]Name 1 0.853 ---Oxygen 1 0.973 ---Nitrogen 2 0.292 BP 2.5221e+004 1.25431e-005 0.31635 Oxygen/Nitrogen 2 0.324 VB 2.1944e+006 4.38439e-005 96.20953 Carbon Dioxide 2 1.503 ---Sulfur Dioxide 3 1.339 BB 6171.52878 1.63381e-004 1.00831 Argon/Oxygen 3 2.618 ---Nitrogen_2 Total amount =97.53418 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 4: Agilent Cerity QA/QC Report Sample name:*Reprocessed:0618-HeatXGRArCO0O10 Sample note: Submission time:Wednesday,June 18,2008 1:06:58 PM Operator: Injection date:Wednesday,June 18,2008 1:27:18 PM GC Description:Mlcro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:June11Calibration2 Method last 312 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 saved:Friday,June 13,2008 4:08:30 PM 313 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >:+ =i o rs a a TT -T 15 2 25 min TCD2ZA >! [on]i i So ::=-9 -T T T 415 2 25 min TCD3 A 2 n _whe .ks pe eben eect nen eae wcnytnmner meets ok * i oO hl .. :ne ae a re im] < S.: a. a:oan fe) oO: Q :ooaoir .Q 1 eee an -nnfa)::ng : 5 Y T T r T --*TT T mes)1 15 20 25 min 314 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 ESTD Report Calibration last saved:Wednesday,June 18,2008 2:20:06 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area piv's]Amt/Area Amount [mass%]Name 1 0.853 ---Oxygen 1 0.973 ---Nitrogen 2 0.291 BB 2.4940e+004 1.25431e-005 0.31283 Oxygen/Nitrogen 2 0.324 BB 2.1955e+006 4.38439e-005 96.25893 Carbon Dioxide 2 1.503 ---Sulfur Dioxide 3 1.333 BB 6071.15710 1.63381e-004 0.99191 Argon/Oxygen 3 2.618 ---Nitrogen_2 Total amount =97.56367 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated 315 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO?/Argon HX Run 1: Heat Exchanger Composition -1.00 Argon,96.33 Carbon Dioxide,0.32 Air Date -13 June 2008 Notebook Page -162 Front Page - Water Flow Rate -0.7905 kg/min (0.013175 kg/s) Pressure Gauge -1205 psi Pressure Transducer -1294 psi Gas Inlet Temperature -58°C (136.4°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 316 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Gas Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In Out Out |Out In Density |Transfer Heat Factor Meter (°C)(°C)(°C)|Density |(°C)|(kg/m3)|Coefficient |Transfer (lb/hr)(kg/m3)(U)Coefficient W/m2K (W/m2K) 119.89 86.34 |16.57 |35.80 |33.90 |659.46 |60.63 |216.50 460.13 543.05 |110.40 |2.12 |1.10E+09 |7.76E+04 |0.0204 118.06 83.63 |16.18 |31.47 |31.48 |693.80 |54.55 |222.40 502.13 602.54 |119.30 |2.50 |1.38E+09 |7.54E+04 |0.0213 116.91 82.40 |16.10 |30.13 |30.67 |702.46 |50.24 |231.82 526.76 638.36 |124.19 |3.01 |1.72E+09 |7.28E+04 |0.0225 116.02 82.08 |16.11 |29.84 |30.43 |705.14 |48.60 |237.04 535.46 651.17 |125.61 |3.34 |1.95E+09 |7.09E+04 |0.0233 116.14 81.78 |16.09 |29.54 |30.32 |705.68 |48.24 |236.85 538.28 655.35 |126.34 |3.36 |1.96E+09 |7.11E+04 |0.0232 114.70 82.17 |16.06 |29.68 |30.37 |706.84 |48.08 |240.07 530.26 643.50 |123.56 |3.55 |2.12E+09 |6.92E+04 |0.0238 110.53 86.52 |16.21 |35.26 |32.55 |689.83 |49.77 |260.47 496.47 594.41 |113.40 |4.07 |2.43E+09 |6.15E+04 |0.0268 111.61 88.48 |16.54 |38.57 |33.95 |673.99 |53.73 |252.50 484.35 577.11 |112.61 |3.21 |1.79E+09 |6.45E+04 |0.0252 112.28 89.44 |16.69 |40.01 |34.57 |667.54 |56.30 |246.55 474.54 $63.25 |111.22 |2.86 |1.55E+09 |6.61E+04 |0.0244 112.52 89.93 |16.81 |40.90 |34.93 |663.09 |57.64 |243.71 470.06 556.95 |110.66 |2.71 |1.45E+09 |6.69E+04 |0.0240 112.43 90.11 |16.80 |41.28 |35.13 |660.13 |58.14 |242.73 465.65 550.76 |109.74 |2.65 |1.41E+09 |6.70E+04 |0.0238 112.42 90.07 |16.69 |41.30 |35.12 |659.94 |58.15 |242.49 464.76 549.53 |109.53 |2.65 |1.41E+09 |6.71E+04 |0.0238 112.37 90.08 |16.80 |41.30 |35.12 |660.06 |58.15 |242.55 465.92 551.14 |109.84 |2.65 |1.40E+09 |6.71E+04 |0.0238 112.35 90.14 |16.87 |41.40 |35.14 |660.10 |58.25 |242.43 467.03 552.70 |110.17 |2.64 |1.40E+09 |6.70E+04 |0.0238 112.20 90.17 |16.90 |41.45 |35.18 |659.30 |58.23 |242.66 466.04 $51.31 |109.91 |2.64 |1.39E+09 |6.69E+04 |0.0238 112.21 90.21 |16.94 |41.52 |35.18 |659.66 |58.39 |242.26 466.70 $52.23 |110.13 |2.63 |1.39E+09 |6.70E+04 |0.0238 112.15 90.22 |16.97 |41.52 |35.20 |659.35 |58.44 |242.15 465.98 $51.22 |109.97 |2.62 |1.38E+09 |6.70E+04 |0.0238 112.05 90.33 |17.03 |41.60 |35.27 |658.61 |58.58 |242.20 464.29 548.86 |109.55 |2.62 |1.38E+09 |6.69E+04 |0.0238 112.25 90.13 |17.02 |41.36 |35.24 |657.63 |58.60 |241.04 462.56 546.45 |109.21 |2.59 |1.36E+09 |6.73E+04 |0.0236 112.23 89.82 |17.04 |40.94 |35.02 |660.49 |58.26 |240.79 466.64 552.15 |110.17 |2.61 |1.37E+09 |6.74E+04 |0.0236 112.10 89.66 |17.01 |40.82 |34.91 |661.67 |57.93 |241.20 469.40 556.01 |110.80 |2.64 |1.39E+09 |6.72E+04 |0.0237 111.96 89.62 |17.03 |40.76 |34.92 |661.23 |57.77 |241.60 468.89 555.31 |110.62 |2.65 |1.39E+09 |6.71E+04 |0.0237 317 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Gas GasIn {|Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In Out Out Out In Density |Transfer Heat Factor Meter (°C)(°C)(°C)|Density |(°C)|(kg/m3)|Coefficient |Transfer(Ib/hr)(kg/m3)(U)Coefficient W/m2K (W/m2K) 112.01 89.51 |16.87 |40.75 |34.85 |661.99 |57.76 |241.09 469.36 555.96 |110.75 |2.64 |1.39E+09 |6.72E+04 |0.0237 112.05 89.45 |16.72 |40.67 |34.81 |662.33 |57.82 |240.51 467.44 $53.27 |110.25 |2.63 |1.39E+09 |6.73E+04 |0.0236 111.73 89.58 |16.76 |40.83 |34.88 |661.74 |57.82 |241.17 466.49 551.94 |109.97 |2.64 |1.40E+09 |6.70E+04 |0.0237 111.59 89.74 |16.89 |41.24 |34.97 |660.82 |58.03 |241.20 468.73 555.08 |110.67 |2.63 |1.38E+09 |6.69E+04 |0.0237 111.62 89.90 |16.85 |41.43 |35.12 |658.80 |58.31 |241.02 464.61 549.31 |109.68 |2.60 |1.36E+09 |6.70E+04 |0.0236 111.70 89.90 |16.71 |41.61 |35.13 |658.50 |58.53 |240.21 463.98 548.43 |109.61 |2.58 |1.35E+09 |6.72E+04 |0.0235 111.83 89.82 |16.51 |41.52 |35.04 |659.97 |58.67 |239.25 463.02 547.09 |109.36 |2.56 |1.35E+09 |6.74E+04 |0.0235 111.67 89.85 |16.62 |41.50 |34.86 |663.99 |58.73 |239.15 468.77 555.13 |110.77 |2.58 |1.35E+09 |6.72E+04 |0.0235 111.56 89.82 |16.72 |41.49 |34.78 |665.58 |58.71 |239.08 472.31 560.10 |111.68 |2.59 |1.35E+09 |6.71E+04 |0.0236 111.55 89.91 |16.77 |41.68 |34.86 |664.56 |58.92 |238.79 471.67 559.21 |111.61 |2.57 |1.34E+09 |6.72E+04 |0.0235 111.57 90.00 |16.73 |41.76 |34.94 |663.33 |59.14 |238.42 468.49 554.75 |110.84 |2.55 |1.33E+09 |6.73E+04 |0.0235 111.60 90.04 |16.77 |41.80 |34.96 |663.20 |59.35 |237.87 467.79 553.76 |110.73 |2.53 |1.32E+09 |6.74E+04 |0.0234 111.88 90.23 |16.77 |41.96 |35.05 |662.60 |59.80 |237.22 465.67 550.79 |110.27 |2.50 |1.30E+09 |6.76E+04 |0.0233 112.05 90.37 |16.74 |42.31 |35.23 |659.68 |60.45 |235.61 461.39 544.81 |109.43 |2.44 |1.26E+09 |6.81E+04 |0.0231 112.09 90.36 |16.73 |42.45 |35.23 |659.77 |60.69 |234.78 462.23 545.98 |109.76 |2.42 |1.25E+09 |6.82E+04 |0.0230 112.07 90.31 |16.58 |42.32 |35.19 |660.27 |60.68 |234.54 460.01 542.89 |109.13 |2.41 |1.25E+09 |6.83E+04 |0.0230 111.91 90.28 |16.70 |42.29 |35.13 |661.25 |60.60 |234.69 462.57 546.46 |109.77 |2.42 |1.25E+09 |6.81E+04 |0.0230 111.84 90.34 |16.81 |42.35 |35.16 |661.15 |60.66 |234.77 463.34 547.53 |109.99 |2.42 |1.25E+09 |6.81E+04 |0.0230 111.78 90.41 |16.89 |42.52 |35.23 |660.05 |60.78 |234.71 463.29 547.46 |110.05 |2.41 |1.24E+09 |6.81E+04 |0.0230 111.94 90.41 |16.88 |42.52 |35.25 |659.74 |60.99 |234.00 462.26 546.02 |109.86 |2.39 |1.23E+09 |6.83E+04 |0.0229 112.00 90.32 |16.76 |42.60 |35.21 |659.79 |61.16 |232.99 462.15 545.87 |109.92 |2.37 |1.21E+09 |6.85E+04 |0.0228 112.64 88.93 |16.70 |39.86 |34.43 |666.86 |57.54 |239.14 474.14 562.91 |111.88 |2.68 |1.43E+09 |6.79E+04 |0.0235 318 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Red Data is an average of all data points. 319 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO2/Argon HX Run 2: Heat Exchanger Composition -1.00 Argon,96.33 Carbon Dioxide,0.32 Air Date -16 June 2008 Notebook Page -162 Front Page - Water Flow Rate -1.1475 kg/min (0.019125 kg/s) Pressure Gauge -800 psi Pressure Transducer -864 psi Gas Inlet Temperature -152°C (305.6°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 320 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side 'Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(CC)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(U)Coefficient W/m2K (W/m2K) 49.16 59.69 |16.15 |31.71 |19.69 |785.94 |152.07 81.16 266.17 291.96 |61.15 |0.92 |1.30E+08 |3.77E+04 |0.0098 49.08 59.70 |16.08 |31.70 |19.69 |785.98 |151.80 81.24 264.68 290.16 |60.79 |0.92 |2.78E+08 |3.76E+04 |0.0098 49.15 59.69 |16.06 |31.65 |19.69 |786.01 |151.72 81.25 264.81 290.33 |60.83 |0.92 |2.78E+08 |3.77E+04 |0.0098 49.44 59.74 |16.16 |31.72 |19.74 |785.37 |151.62 81.34 267.13 293.12 |61.44 |0.92 |2.78E+08 |3.79E+04 |0.0098 49.45 59.77 |16.21 |31.79 |19.80 |784.69 |151.69 81.38 266.91 292.85 |61.40 |0.92 |2.78E+08 |3.79E+04 |0.0098 49.40 59.78 |16.22 |31.88 |19.81 |784.64 |152.08 81.28 266.47 292.32 |61.27 |0.92 |2.78E+08 |3.79E+04 |0.0098 49.46 59.76 |16.20 |31.83 |19.83 |784.26 |152.14 81.24 265.89 291.62 |61.14 |0.92 |2.77E+08 |3.79E+04 |0.0098 49,58 59.74 |16.21 |31.71 |19.81 |784.49 |152.49 81.12 266.71 292.61 |61.33 |0.92 |2.77E+08 |3.80E+04 |0.0098 49.66 59.75 |16.26 |31.73 |19.85 |784.02 |152.30 81.19 267.42 293.46 |61.53 |0.92 |2.77E+08 |3.81E+04 |0.0098 49.38 59.77 |16.28 |31.76 |19.86 |783.81 |152.43 81.17 265.93 291.67 |}61.16 |0.92 |2.77E+08 |3.78E+04 |0.0098 49.27 59.77 |16.29 |31.79 |19.88 |783.64 |152.58 81.14 265.17 290.76 |60.97 |0.92 |2.77E+08 |3.78E+04 |0.0098 49.34 59.77 |16.31 |31.74 |19.85 |784.03 |152.88 81.05 266.18 291.98 |61.19 |0.92 |2.76E+08 |3.78E+04 |0.0098 49.44 59.78 |16.33 |31.78 |19.87 |783.79 |153.28 80.96 266.46 292.31 |61.26 |0.92 |2.76E+08 |3.79E+04 |0.0098 49.54 59.79 |16.35 |31.79 |19.88 |783.63 |153.14 81.01 267.20 293.20 |61.45 |0.92 |2.76E+08 |3.79E+04 |0.0098 49.27 59.78 |16.37 |31.81 |19.87 |783.79 |153.36 80.95 266.18 291.98 |61.18 |0.92 |2.76E+08 |3.77E+04 |0.0098 49.13 59.80 |16.39 |31.86 |19.92 |783.18 |153.32 80.98 264.98 290.53 |60.90 |0.92 |}2.76E+08 |3.76E+04 |0.0098 49.22 59.81 |16.41 |31.89 |19.92 |783.19 |153.42 80.97 265.67 291.36 |61.07 |0.92 |2.76E+08 |3.77E+04 |0.0098 49.29 59.80 |16.35 |32.07 |19.95 |782.72 |153.68 80.89 264.34 289.76 |60.74 |0.92 |2.75E+08 |3.77E+04 |0.0098 49.40 59.78 |16.32 |32.08 |19.94 |782.82 |153.67 80.87 264.70 290.19 |60.83 |0.92 |2.75E+08 |3.78E+04 |0.0098 49.24 59.80 |16.38 |32.11 |19.97 |782.48 |153.92 80.83 264.08 289.45 |60.68 |0.92 |2.75E+08 |3.77E+04 |0.0098 321 Mass_|Pressure |Water |Water |Gas Gas Out |GasIn ;GasIn_|Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(U)Coefficient W/m2K (W/m2K) 49.13 59.82 |16.39 |32.16 |20.01 |781.90 |154.14 80.80 262.67 287.76 |60.33 |0.92 |2.75E+08 |3.76E+04 |0.0098 49,32 59.82 |16.41 |32.22 |20.02 |781.84 |154.46 80.72 263.70 288.99 |60.58 |0.92 |2.74E+08 |3.77E+04 |0.0098 49,33 59.77 |16.28 |31.85 |19.86 |783.92 |152.83 81.07 265.61 291.29 |61.06 |0.92 |2.70E+08 |3.78E+04 |0.0098 Red Data is an average of all data points. CO,/Argon Run 3: Heat Exchanger Composition -1.00 Argon,96.33 Carbon Dioxide,0.32 Air Date -16 June 2008 Notebook Page -162 Front Page - Water Flow Rate -1.8027 kg/min (0.030044 kg/s) Pressure Gauge -775 psi Pressure Transducer -840 psi Gas Inlet Temperature -122°C (251.64°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwin(Do/Di)-4.93992E-05 (Di/Do)/hwater-0.000282474 Total Volume of System -0.00334 m2 322 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass'|Pressure |Water |Water |Gas Gas Out |GasIn |GasIn |Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(U)Coefficient W/m2K (W/m2K) 49.56 57.88 |15.47 |23.85 |18.05 |802.15 |126.04 85.89 306.47 341.18 |63.91 |0.96 |1.43E+08 |3.92E+04 |0.0102 49.41 57.65 |15.40 |23.26 |17.96 |802.65 |121.98 86.84 309.84 345.35 |64.82 |0.97 |1.45E+08 |3.92E+04 |0.0102 49.45 57.71 |15.36 |23.11 }17.90 |803.53 |118.71 88.04 314.78 351.51 |66.03 |0.98 |1.47E+08 |3.94E+04 |0.0104 49,30 57.74 |15.43 |23.41 |17.96 |802.92 |121.93 87.00 310.74 346.47 |65.01 |0.97 |1.45E+08 |3.91E+04 |0.0103 49.57 57.83 |15.41 |23.47 |18.01 |802.49 |122.19 87.06 309.89 345.41 |64.83 |0.97 |1.46E+08 |3.93E+04 }0.0103 49.40 57.77 |15.44 |23.38 |17.99 |802.58 |121.92 87.05 310.43 346.09 |64.96 |0.97 |1.45E+08 |3.92E+04 |0.0103 49.57 57.90 |15.51 |23.56 |18.08 |801.76 |122.45 87.09 310.28 345.90 |64.96 |0.97 |1.46E+08 |3.93E+04 |0.0103 49.62 57.94 |15.56 |23.56 |18.12 |801.43 |122.08 87.30 311.24 347.09 |65.22 |0.97 |1.46E+08 |3.93E+04 |0.0103 49.51 57.86 |15.51 |23.62 |18.14 |800.94 |122.63 86.97 307.70 342.70 |64.41 |0.97 |1.45E+08 |3.92E+04 |0.0103 49,37 57.61 |15.32 |22.94 |17.90 |803.22 |116.93 88.49 314.85 351.58 |66.14 |0.98 |1.48E+08 |3.94E+04 |0.0104 49.37 57.80 |15.44 |23.36 |18.00 |802.47 |119.20 88.02 313.19 349.52 |65.72 |0.97 |1.47E+08 |3.93E+04 |0.0104 49.53 57.91 |15.53 |23.61 |18.10 |801.51 |122.18 87.20 310.24 345.85 |64.98 |0.97 |1.46E+08 |3.93E+04 |0.0103 49.62 57.93 |15.60 |23.76 |18.16 |800.81 |123.23 86.89 309.95 345.49 |64.92 |0.97 |1.45E+08 |3.93E+04 |0.0103 49.90 58.01 |15.57 |23.71 |18.20 |800.60 |121.95 87.44 311.21 347.06 |65.28 |0.97 |1.46E+08 |3.96E+04 |0.0103 49,49 57.85 |15.53 |23.58 |18.12 |801.10 |121.84 87.21 309.60 345.05 |64.87 |0.97 |1.45E+08 |3.93E+04 |0.0103 49.67 57.87 |15.45 |23.44 |18.08 |801.67 |}120.43 87.73 311.32 347.20 |65.29 |0.97 |1.47E+08 |3.95E+04 |0.0103 49.46 57.80 |15.50 |23.52 |18.08 |801.47 |121.59 87.21 309.96 345.50 |64.94 |0.97 |1.45E+08 |3.93E+04 |0.0103 49,52 57.83 |15.46 |23.42 |18.07 |801.75 |120.57 87.60 310.88 346.64 |65.17 |0.97 |1.46E+08 |3.93E+04 |0.0103 49,52 57.83 }15.47 |23.48 |18.05 |801.95 |121.55 87.28 310.70 346.42 |65.08 |0.97 |1.46E+08 |3.93E+04 |0.0103 Red Data is an average of all data points. 323 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO>2/Argon Run 4: Heat Exchanger Composition -1.00 Argon,96.33 Carbon Dioxide,0.32 Air Date -16 June 2008 Notebook Page -162 Front Page - Water Flow Rate 1.1475 kg/min (0.019125 kg/s) Pressure Gauge -455 psi Pressure Transducer -485 psi Gas Inlet Temperature -205°C (401°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di--0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater 0.000282474 Total Volume of System -0.00334 m2 Mass |Pressure |Water |Water |Gas Gas Out |GasIn |GasIn_|Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(VU)Coefficient W/m2K (W/m2K) 18.93 33.49 |16.33 |23.45 |18.04 77.35 |205,23 38.16 51.90 52.81 |20.95 |0.80 |2.63E+07 |1.43E+04 |0.0058 18.99 33.53 |16.18 |23.36 |17.98 77.52 |205.82 38.16 51.62 52.52 |20.80 |0.80 |2.64E+07 |1.43E+04 |0.0058 18.94 33.35 |16.25 |23.40 |17.87 77.04 |206,32 37.91 52.62 53.55 |21.22 |0.80 |2.61E+07 |1.43E+04 |0.0058 18.70 33.08 |16.27 |23.06 |17.89 76.18 |200.36 38.13 51.46 52.35 |20.96 |0.80 |2.60E+07 |1.42E+04 |0.0058 18.31 32.84 |16.27 |22.45 |17.86 75.48 |188.21 38.99 49.85 50.69 |20.69 |0.80 |2.64E+07 |1.41E+04 |0.0059 324 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |GasIn |GasIn_|Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(CC)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(U)Coefficient W/m2K (W/m2K) 18.23 32.92 |16.27 |22.10 |17.78 75.75 |177.20 40.18 49.62 50.45 |20.93 |0.81 |2.73E+07 |1.42E+04 |0.0061 18.41 33.09 |16.20 |22.11 |17.77 76.28 |175.16 40.61 49.63 50.46 |20.97 |0.81 |2.78E+07 |1.44E+04 |0.0061 18.64 33.28 |16.22 |22.40 |17.81 76.85 |181.57 40.19 50.60 51.47 |21.16 |0.81 |2.77E+07 |1.44E+04 |0.0060 18.80 33.42 |16.31 |22.96 |17.88 77.24 |191.91 39,33 51.81 52.72 |21.33 |0.80 |2.72E+07 |1.44E+04 |0.0059 18.87 33.29 |16.28 |23.16 |17.90 76.82 |199.51 38.45 51.97 52.88 |21.17 |0.80 |2.64E+07 |1.43E+04 |0.0058 18.67 33.09 |16.06 |22.81 |17.83 76.24 |197.64 38.39 50.28 51.13 |20.55 |0.80 |2.63E+07 |1.42E+04 |0.0058 18.58 33.14 |15.92 |22.43 |17.74 76.46 |192.06 38.98 49.52 50.35 |20.40 |0.80 |2.68E+07 |1.42E+04 |0.0059 18.67 33.28 |15.92 |22.42 |17.68 76.91 |191.33 39,21 50.10 50.95 |20.64 |0.80 |2.71E+07 |1.43E+04 |0.0059 18.83 33.37 |15.86 |22.68 |17.66 77.21 |197.02 38.78 50.69 51.55 |20.70 |0.80 |2.69E+07 |1.43E+04 |0.0059 18.84 33.22 |15.76 |22.73 |17.59 76.78 |201.58 38.18 50.74 51.60 |20.60 |0.80 |2.63E+07 |1.43E+04 |0.0058 18.72 33.23 |15.74 |22.58 |17.50 76.86 |199.58 38.37 50.68 $1.55 |20.64 |0.80 |2.65E+07 |1.42E+04 |0.0058 18.81 33.34 |15.81 |22.66 |17.55 77.19 |199.94 38.47 51.11 51.99 |20.79 }0.80 |2.67E+07 |1.43E+04 |0.0059 18.92 33.30 |15.81 |22.80 |17.58 77.03 |203.46 38.10 51.40 52.30 |20.81 |0.80 |2.63E+07 |1.43E+04 |0.0058 18.77 33.06 |15.79 |22.69 |17.54 76.32 |202.35 37.92 50.98 51.86 |20.70 |0.80 |2.60E+07 |1.42E+04 |0.0058 18.53 32.89 |15.89 |22.37 |17.55 75.79 |196.88 38.22 50.54 51.40 |20.70 |0.80 |2.60E+07 |1.41E+04 |0.0058 18.71 33.21 |16.06 |22.73 |17.75 76.67 |195.66 38.74 50.86 51.73 |20.84 |0.80 |2.66E+07 |1.43E+04 |0.0059 Red Data is an average of all data points. 325 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO/Argon Run 5: Heat Exchanger Composition -1.00 Argon,96.33 Carbon Dioxide,0.32 Air Date -17 June 2008 Notebook Page -161 Front Page - Water Flow Rate -1.05 kg/min (0.0175 kg/s) Pressure Gauge -415 psi Pressure Transducer -437 psi Gas Inlet Temperature -120°C (248°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftesR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass_|Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(Ib/hr)(U)Coefficient W/m2K (W/m2K) 15.28 30.30 |16.46 |19.87 |18.01 67.90 |118.54 43.56 37.11 37.57 |18.65 |0.84 |2.46E+07 |1.28E+04 |0.0065 15.49 30.40 |16.53 {|20.00 |18.07 68.16 |118.10 43.77 37.69 38.17 |18.95 |0.84 |4.97E+07 |1.30E+04 |0.0065 15.38 30.27 |16.55 |20.08 |18.12 67.77 |119.41 43.39 37.31 37.78 |18.73 |0.84 |4.91E+07 |1.29E+04 |0.0064 15.30 30.32 |16.50 |20.00 |18.15 67.89 |118.06 43.65 36.61 37.06 |18.41 |0.84 |4.93E+07 |1.29E+04 |0.0065 326 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow -|(bar)In Out Out Density }(°C)Density |Transfer Heat Factor Meter (°C)(°C)(CC)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(U)Coefficient W/m2K (W/m2K) 15.49 30.38 |16.44 |19.82 |18.10 68.09 |118.36 43.70 37.00 37.46 |18.59 |0.84 |4.96E+07 |1.30E+04 |0.0065 15.48 30.38 |16.48 |19.84 |18.08 68.10 |119.84 43.50 37.41 37.88 |18.75 |0.84 |4.96E+07 |1.30E+04 |0.0064 15.55 30.38 |16.39 |19.90 |18.07 68.09 |121.38 43,28 37.26 37.73 |18.63 |0.84 |4.95E+07 |1.30E+04 |0.0064 15.39 30.26 |16.28 |19.72 |18.04 67.76 |121.98 43.02 36.44 36.89 |18.20 |0.84 |4.91E+07 |1.29E+04 |0.0064 15.51 30.37 |16.22 |19.62 |17.98 68.12 |120.75 43.36 36.70 37.15 |18.36 |0.84 |4.96E+07 |1.30E+04 |0.0064 15.47 30.32 |16.25 |19.69 |17.97 67.98 |121.34 43.20 36.87 37.33 |18.44 |0.84 |4.94E+07 |1.29E+04 |0.0064 15.57 30.39 |16.24 |19.72 |17.98 68.17 |122.00 43,22 37.07 37.53 |18.51 |0.84 |4.97E+07 |1.30E+04 |0.0064 15.48 30.30 |16.37 |19.80 |17.98 67.92 |122.56 43.01 37.55 38.03 |18.74 |0.84 |4.93E+07 |1.29E+04 |0.0064 15.56 30.38 |16.34 |19.87 |18.05 68.12 |122.61 43.12 37.23 37.69 |18.57 |0.84 |4.96E+07 |1.30E+04 |0.0064 15.44 30.26 |16.33 |19.96 |18.04 67.78 |122.82 42.91 36.94 37.40 |18.43 |0.84 |4.91E+07 |1.29E+04 |0.0064 15.46 30.35 |16.44 |20.00 |18.09 68.01 |121.82 43.18 37.27 37.73 |18.62 |0.84 |4.94E+07 |1.29E+04 |0.0064 15.46 30.30 |16.45 |20.11 |18.14 67.83 |122.24 43.04 37.08 37.54 |18.51 |0.84 |4.91E+07 |1.29E+04 |0.0064 15.46 30.34 |16.39 |19.87 |18.05 67.98 |120.74 43.31 37.10 37.56 |18.57 |0.84 |4.79E+07 |1.29E+04 |0.0064 Red Data is an average of all data points. 327 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO>/Argon Run 6: Heat Exchanger Composition -1.00 Argon,96.33 Carbon Dioxide,0.32 Air Date -17 June 2008 Notebook Page -161 Front Page -- Water Flow Rate -0.954 kg/min (0.0159 kg/s) Pressure Gauge -235 psi Pressure Transducer -244 psi Gas Inlet Temperature -200°C (392°F) Averaged Data 5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwin(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass Pressure |Water |Water |Gas Gas Out |GasIn |Gas In Total Heat |Gas Side Nu_|Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(U)Coefficient W/m2K (W/m2k) 7.16 16.85 |16.67 |20.00 |18.55 33.84 |201.83 19.07 17.30 17.40 |7.81 |0.77 |5.69E+06 |5.48E+03 |0.0036 7.24 16.79 |16.59 |19.93 |18.50 33.72 |202.51 18.97 17.38 17.48 |7.84 |0.77 |5.65E+06 |5.54E+03 |0.0036 7.27 16.72 |16.62 |19.82 |18.39 33.57 |202.67 18.88 17.73 17.84 |8.00 |0.77 |5.59E+06 |5.57E+03 |0.0036 7.16 16.71 |16.64 |19.71 |18.39 33.56 |200.59 18.96 17.65 17.75 |7.99 |0.77 |5.61E+06 |5.50E+03 |0.0036 328 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |GasIn |GasIn |Total Heat |Gas Side Nu |Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(U)Coefficient W/m2K (W/m2K) 7.10 16.73 |16.61 |19.59 |18.32 33.62 |197.74 19.11 17.82 17.92 |8.10 |0.77 |5.66E+06 |5.47E+03 |0.0036 7.08 16.77 |16.57 |19.56 |18.33 33.70 |195.86 19.24 17.79 17.89 |8.11 |0.77 |5.71E+06 |5.47E+03 |0.0036 7.10 16.79 |16.52 }19.52 |18.31 33.75 |195.46 19.28 17.84 17.94 |8.14 |0.77 |5.73E+06 |5.48E+03 |0.0036 7.22 16.74 |16.41 |19.53 |18.29 33.65 |197.14 19.15 17.79 17.90 |8.10 |0.77 |5.68E+06 |5.56E+03 |0.0036 7.26 16.68 |16.33 |19.41 |18.26 33.50 |198.00 19.03 17.70 17.81 |8.05 |0.77 |5.63E+06 |5.59E+03 |0.0036 7.16 16.66 |16.38 |19.34 |18.25 33.47 |196.99 19.06 17.65 17.75 |8.04 |0.77 |5.63E+06 |5.52E+03 |0.0036 7.08 16.70 |16.48 |19.35 |18.29 33.54 |195.01 19.19 17.75 17.86 |8.11 |0.77 |5.67E+06 |5.47E+03 |0.0036 7.05 16.74 |16.54 |19.41 |18.32 33.63 |193.27 19.31 17.88 17.99 |8.19 |0.77 |5.71E+06 |5.46E+03 |0.0036 7.05 16.78 |16.64 |19.57 |18.43 33.72 |193.11 19.37 17.88 17.99 |8.19 |0.77 |5.74E+06 |5.46E+03 |0.0037 7.14 16.77 |16.75 |19.82 |18.43 33.68 |194.71 19.29 18.23 18.34 |8.33 |0.77 |5.70E+06 |5.52E+03 |0.0036. 7.21 16.71 |16.66 |19.94 |18.47 33.54 |196.86 19.12 17.93 18.04 |8.17 |0.77 |5.64E+06 |5.56E+03 |0.0036 7.22 16.64 |16.56 |19.83 |18.55 33.37 |197.55 19.01 17.54 17.64 |7.98 |0.77 |5.58E+06 |5.56E+03 |0.0036 7.08 16.63 |16.55 |19.72 |18.58 33.35 |195.61 19.09 17.26 17.36 |7.87 |0.77 |5.60E+06 |5.46E+03 |0.0036 7.02 16.67 |16.57 |19.60 |18.55 33.43 |192.77 19.25 17.44 17.54 |7.99 |0.77 |5.66E+06 |5.44E+03 |0.0036 7.02 16.71 |16.64 |19.64 |18.52 33.53 |190.57 19.40 17.80 17.90 |8.19 |0.77 |5.70E+06 |5.45E+03 |0.0037 6.99 16.76 |16.69 |19.74 |18.55 33.64 |190.45 19.46 17.78 17.89 }8.18 |0.77 |5.74E+06 |5.43E+03 |0.0037 7.06 16.77 |16.73 |19.89 |18.55 33.66 |192.01 19.41 17.94 18.05 |8.23 |0.77 |5.73E+06 |5.47E+03 |0.0037 7.13 16.73 |16.58 |19.66 |18.42 33.59 |196.22 19.17 17.72 17.82 |8.08 |0.77 |5.67E+06 |5.50E+03 |0.0036 Red Data is an average of all data points. 329 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO/Argon Run 7: Heat Exchanger Composition -1.00 Argon,96.33 Carbon Dioxide,0.32 Air Date -17 June 2008 Notebook Page -161 Front Page -- Water Flow Rate -0.55 kg/min (0.009167 kg/s) Pressure Gauge -225 psi Pressure Transducer -240 psi Gas Inlet Temperature -120°C (248°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass_|Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu_|Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(Ib/hr)(U)Coefficient W/m2K (W/m2K) 6.84 16.61 |17.63 |21.12 |19.65 33.13 |129.77 22.48 14.42 14.49 |7.39 |0.79 |5.74E+06 |5.73E+03 |0.0040 6.82 16.55 |17.77 |21.23 |19.79 32.99 |130.52 22.36 14.39 14.46 |7.36 |0.79 |5.69E+06 |5.71E+03 |0.0040 6.75 16.48 |17.90 |21.30 |19.90 32.81 |129.82 22.30 14.25 14.32 |7.30 |0.79 |5.62E+06 |5.65E+03 |0.0040 6.64 16.45 |17.90 |21.26 |20.02 32.73 |127.86 22.38 13.76 13.82 |7.08 |0.79 |5.60E+06 |5.57E+03 |0.0040 330 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu |Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(CC)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(U)Coefficient W/m2K (W/m2K) 6.61 16.55 |17.95 |21.24 |20.03 32.94 |125.27 22.68 13.67 13.73 |7.06 |0.79 |5.66E+06 |5.57E+03 |0.0041 6.68 16.58 |17.96 |21.23 |20.00 33.02 |123.78 22.82 13.83 13.90 |7.17 |0.79 |5.67E+06 |5.64E+03 |0.0041 6.74 16.56 |17.90 |21.32 |20.15 32.95 |123.79 22.79 13.62 13.68 |7.06 |0.79 |5.66E+06 |5.68E+03 |0.0041 6.73 16.51 |17.90 |21.27 |20.10 32.84 |124.52 22.67 13.71 13.77 |7.09 |0.79 |5.62E+06 |5.67E+03 |0.0040 6.68 16.45 |17.89 |21.24 |20.14 32.70 |124.55 22.58 13.52 13.58 |6.99 |0.79 |5.58E+06 |5.63E+03 |0.0040 6.58 16.39 |17.96 |21.17 |20.21 32.57 |123.48 22.57 13.27 13.32 |6.88 |0.79 |5.53E+06 |5.55E+03 |0.0040 6.54 16.49 |18.03 |21.16 |20.28 32.76 |121.47 22.83 13.10 13.16 |6.82 |0.79 |5.58E+06 |5.53E+03 |0.0041 6.62 16.53 |18.06 |21.21 |20.41 32.85 |120.33 22.98 13.09 13.14 |6.82 |0.79 |5.61E+06 |5.61E+03 |0.0041 6.67 16.50 |17.95 |21.30 |20.38 32.79 |120.54 22.92 13.11 13.16 |6.83 |0.79 |5.59E+06 |5.65E+03 |0.0041 6.67 16.45 |17.85 |21.09 |20.26 32.69 |121.38 22.79 13.14 13.20 |6.84 |0.79 |5.57E+06 |5.64E+03 |0.0041 6.60 16.40 |17.85 |20.93 |20.19 32.58 |121.54 22.70 13.10 13.16 |6.82 |0.79 |5.54E+06 |5.58E+03 |0.0041 6.54 16.47 |17.91 |20.89 |20.24 32.74 |120.77 22.86 12.97 13.02 |6.76 |0.79 |5.59E+06 |5.54E+03 |0.0041 6.59 16.53 |17.97 |20.99 |20.25 32.86 |120.17 22.98 13.12 13.18 |6.84 |0.79 |5.62E+06 |5.58E+03 |0.0041 6.67 16.50 |17.91 |21.17 |20.12 32.82 |124.09 22.69 13.53 13.59 |7.01 |0.79 |5.62E+06 |5.62E+03 |0.0041 Red Data is an average of all data points. 331 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Components - Argon Carbon Dioxide GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 Carbon Dioxide 98.70593 |98.53375 |98.68004 |98.68004 |98.64994 Argon 3.44338]3.47061]3.49842]3.49842|3.477708 GC Run 5:. Agilent Cerity QA/QC Report Sample name:*Reprocessed:0630-HeatXGRArCOO7 Sample note: Submission time:Monday,June 30,2008 3:41:34 PM Operator: Injection date:Monday,June 30,2008 3:41:54 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July2Calibration2 Method last saved:Wednesday,July 02,2008 11:10:56 AM 332 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCD1A >::|.': a J .ae denn 4 a.fe L +m eee ee LL a i ”" j .i 4 s ,a t .4 .te ot :os :'' |:i re vie ,rote a o ::i ': oy -t soap eapeecmens face ape t Yr Sa age eng boc co ane aie Pe]:!; ro t oy t!: .'; i :zi *Li "qT !u T 05 1 15 2 2.5 min z 4 oben $. . -boo ee oe :nS CS en 4 De ete eeeencesean te omens_:era i.t :_i !Ss ot ; 2..|| Md :i :i°i ; sh,ee eee Lk fe mae 0 :iNi I 4 i o .be ..-. | i So ;'--S 0.5 1 15 2 25 min ii|113272Asgeninmerei3.|if-50000125 minayaere.)NESTD Report Calibration last saved:Wednesday,July 02,2008 11:22:55 AM Multiplier:1.0000 Dilution:1.0000 333 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample amount:0.0000 mass% Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount [mass%]Name 1 1.477 ---Oxygen 1 1.627 ---Nitrogen 2 0.292 BP 7.4815e+004 0.00000e+000 0.00000 2 0.326 VB 2.0639e+006 4.77424e-005 98.53375 Carbon Dioxide 2 1.496 ---Sulfur Dioxide 3 1.272 PB 1.7535e+004 1.97930e-004 3.47061 Argon/Oxygen Total amount =102.00436 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 6: Agilent Cerity QA/QC Report Sample name:*Reprocessed:0630-HeatXGRArCOO6 Sample note: Submission time:Monday,June 30,2008 3:37:35 PM Operator: Injection date:Monday,June 30,2008 3:37:57 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July2Calibration2 Method last saved:Wednesday,July 02,2008 11:10:56 AM 334 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >=wee eo._-.ee nee :7=a z ° : oan oe i . eed rock "+oO Hy Oo +4--a4 on a ont meine oe - 4 *:+ 4 .be SETAE UROL a aes em 0s 2 25 min >(",: =:'i 7 ee pos ee t re so we oora::: c . 'i ae O°a 3 i-4 . . 2 1 .i :1 i '.8 ae3arso7ayt+a t 7 T r is 1 ®Do ||:Seg g .4 i 1 i 'ur '7 :t yo r=):i : i=]oo |Qo poe aeropte tage ene spe Src tehcate cepa seer ==coer nage ee +mee np sin ge©"r T T pe 05 4 15 2 2.5 min >4 1 "woe enwa+ti.i on i i : oie ho.7 i t t i ' .f ;pod8|=|f=)eros :ee.:oe a4TTr+v T T v T r T T +r v T r T T T '4 15 2 2.5 min ESTD Report Calibration last saved:Wednesday,July 02,2008 11:22:55 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 335 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [iV*s]Amt/Area Amount [mass%]Name 1 1.477 ---Oxygen 1 1.627 ---Nitrogen 2 0.292 PV 7.4827e+004 0.00000e+000 0.00000 2 0.326 VB 2.0669e+006 4.77424e-005 98.68004 Carbon Dioxide 2 1.496 ---Sulfur Dioxide 3 1.268 BB _1.7675e+004 1.97930e-004 3.49842 Argon/Oxygen Total amount =102.17846 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 7: Agilent Cerity QA/QC Report Sample name:*Reprocessed:0630-HeatXGRArCOO8 Sample note: Submission time:Monday,June 30,2008 3:45:26 PM Operator: Injection date:Monday,June 30,2008 3:45:50 PM GC Description:Mlcro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July2Calibration2 Method last saved:Wednesday,July 02,2008 11:10:56 AM 336 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA :| 7 ; T T T 15 2 25 min TODZ2A a i 1x .,-tno -ee ee3,; 1 <. i o ., '2r ::i[Sn a ': °| o :i3]'if=): T r T 15 2 25 min TCDZA ae:.:!4 .4 ; aren «ee :=:i in-ne ia:qo | ©:;hm o 4 i :|i i : wo Tem tae ban oan copes oo T T --T | :16 2 25 min ESTD Report Calibration last saved:Wednesday,July 02,2008 11:22:55 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 337 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount [mass%]Name 1 1.477 ---Oxygen 1 1.627 ---Nitrogen 2 0.292 BP 7.4971e+004 0.00000e+000 0.00000 2 0.326 VB =2.0675e+006 4.77424e-005 98.70593 Carbon Dioxide 2 1.496 ---Sulfur Dioxide 3 1.276 BB 1.7397e+004 1.97930e-004 3.44338 Argon/Oxygen Total amount =102.14931 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 8: Agilent Cerity QA/QC Report Sample name:*Reprocessed:0630-HeatXGRArCOO5 Sample note: Submission time:Monday,June 30,2008 3:33:38 PM Operator: Injection date:Monday,June 30,2008 3:34:00 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July2Calibration2 Method last saved:Wednesday,July 02,2008 11:10:56 AM 338 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA Tl T 2 25 min v : 13 Le A ie ae ares a _rene S t c- oOo 2 |=.:iOo:f o || o ;i i wee ae Jo abe 'cas :i ; +mena ---> 2 25 min i ee oe 2.28 nin ESTD Report Calibration last saved:Wednesday,July 02,2008 11:22:55 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 339 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [iV*s]Amt/Area Amount [mass%]Name 1 1.477 ---Oxygen 1 1.627 ---Nitrogen 2 0.292 BP 7.4921e+004 0.00000e+000 0.00000 2 0.326 VB =2.0662e+006 4.77424e-005 98.64679 Carbon Dioxide 2 1.496 ---Sulfur Dioxide 3 1.263 BB 1.7861e+004 1.97930e-004 3.53532 Argon/Oxygen Total amount =102.18210 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated CO?/Argon Run 8: Heat Exchanger Composition -3.48 Argon,98.65 Carbon Dioxide Date -24 June 2008 Notebook Page -160 Front Page - Water Flow Rate -0.776 kg/min (0.012933 kg/s) Pressure Gauge -1290 psi Pressure Transducer -1386 psi Gas Inlet Temperature -59°C (138.2°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 340 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Out |Gas GasIn_|Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In Out Out Density |In Density |Transfer Heat Factor Meter (°C)(°C)CC)|(kg/m3)|CC)|(kg/m3)|Coefficient |Transfer (ib/hr)(U)Coefficient W/m2K (W/m2K) 115.63 95.64 |17.59 |42.42 |35.48 |686.75 |59.06 |269.06 477.25 567.06 |109.08 |3.35 |1.97E+09 |6.10E+04 |0.0280 115.39 95.62 |17.64 |42.28 |35.55 |685.53 |58.94 |269.51 473.56 561.86 |108.11 |3.36 |1.97E+09 |6.08E+04 |0.0281 115.34 95.58 |17.69 |42.28 |35.48 |686.43 |58.96 |269.18 475.98 565.27 |108.73 |3.36 |1.97E+09 |6.08E+04 |0.0281 115,22 95.48 |17.72 |42.27 |35.40 |687.19 |58.95 |268.68 478.46 568.78 |109.39 |3.36 |1.96E+09 |6.08E+04 |0.0280 115.57 95.18 |17.77 |42.06 |35.31 |687.22 |58.95 |266.95 481.29 572.77 |110.32 |3.33 |1.94E+09 |6.14E+04 |0.0278 115.41 94.86 |17.69 |41.59 |35.20 |687.55 |58.68 |266.38 478.73 569.16 |109.62 |3.34 |1.97E+09 |6.15E+04 |0.0277 115.35 94.76 |17.67 |41.29 |35.11 |688.54 |58.35 |267.42 478.23 568.45 {109.27 |3.40 |2.01E+09 |6.12E+04 |0.0279 115.37 94.61 |17.54 |41.23 |34.96 |690.24 |58.23 |267.12 481.18 572.62 |109.95 |3.42 |2.03E+09 |6.12E+04 |0.0279 115.56 94.49 |17.46 |41.06 |34.93 |690.09 |58.33 |265.95 479.27 569.92 |109.56 |3.38 |2.02E+09 |6.16E+04 |0.0277 115.53 94.37 |}17.47 |41.08 |34.86 |690.81 |58.29 |265.47 482.53 574.53 |110.43 |3.39 |2.01E+09 |6.16E+04 |0.0277 115.04 94.64 |17.52 |41.46 |35.02 |689.43 |58.29 |267.03 480.54 571.72 |109.86 |3.40 |2.01E+09 |6.11E+04 |0.0279 114.95 95.07 |17.62 |42.11 |35.26 |687.52 |58.68 |267.58 480.59 571.79 |110.01 |3.36 |1.96E+09 |6.10E+04 |0.0279 115.11 95.32 |17.66 |42.45 |35.39 |686.54 |59.33 |265.93 478.84 $69.32 |109.85 |3.27 |1.90E+09 |6.15E+04 |0.0276 115.13 95.37 |17.60 |42.51 |35.43 |686.22 |59.64 |264.78 476.44 565.92 |109.36 |3.22 |1.88E+09 |6.17E+04 |0.0275 114.95 95.36 |17.66 |42.51 |35.40 |686.55 |59.64 |264.69 477.31 567.14 |109.58 |3.22 |1.88E+09 |6.17E+04 |0.0275 114.96 95.39 |17.73 |42.59 |35.41 |686.64 |59.75 |264.42 478.76 569.20 |110.01 |3.21 |1.86E+09 |6.17E+04 |0.0274 114.79 95.36 |17.76 |42.70 |35.45 |685.88 |59.80 |264.02 478.69 569.10 |110.09 |3.19 |1.84E+09 |6.18E+04 |0.0274 114.68 95.31 |17.71 |42.62 |35.41 |686.13 |59.65 |264.38 478.10 568.27 |109.86 |3.21 |1.86E+09 |6.16E+04 |0.0274 114.59 95.12 |17.54 |42.37 |35.35 |686.34 |59.46 |264.22 475.45 $64.52 |109.11 |3.22 |1.88E+09 |6.16E+04 |0.0274 114.62 95.13 |17.61 |42.24 |35.31 |687.08 |59.38 |264.67 476.17 565.54 |109.20 |3.24 |1.90E+09 |6.15SE+04 |0.0275 341 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Out |Gas Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In Out Out Density |In Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)|CC)|(kg/m3)|Coefficient |Transfer(lb/hr)(VU)Coefficient W/m2K (W/m2K) 114.77 95.31 |17.65 |42.60 |35.43 |685.87 |59.89 |263.25 475.99 565.29 |109.43 |3.17 |1.84E+09 |6.19E+04 |0.0273 114.66 95.44 |17.70 |42.84 |35.46 |686.03 |60.27 |262.31 476.53 566.05 |109.69 |3.13 |1.81E+09 |6.20E+04 |0.0271 114.56 95.43 |17.75 |42.84 |35.53 |684.73 |60.30 |262.11 474.50 563.19 |109.26 |3.11 |1.80E+09 |6.21E+04 |0.0271 114.51 95.52 |17.83 |42.97 |35.63 |683.51 |60.44 |261.97 473.31 561.51 |109.05 |3.08 |1.78E+09 |6.22E+04 |0.0270 114.50 95.52 |17.79 |43.08 |35.62 |683.67 |60.65 |261.06 473.56 561.86 |109.21 |3.06 |1.76E+09 |6.24E+04 |0.0269 114.48 95.25 |17.58 |42.87 |35.48 |684.74 |60.40 |260.71 473.88 562.31 |109.22 |3.07 |1.78E+09 |6.24E+04 |0.0269 114.18 95.05 |17.57 |42.79 |35.40 |685.12 |60.13 |260.83 475.60 564.74 |109.62 |3.10 |1.79E+09 |6.22E+04 |0.0269 114.21 95.06 |17.61 |42.91 |35.49 |683.62 |60.04 |261.23 475.73 564.91 |109.72 |3.10 |1.78E+09 |6.22E+04 |0.0269 114.56 94.58 |17.56 |41.81 |35.27 |684.80 |59.99 |258.87 469.64 556.36 |108.17 |3.06 |1.80E+09 |6.29E+04 |0.0266 114.57 94.39 |17.50 |41.77 |35.01 |688.38 |59.74 |258.95 477.60 567.57 |110.05 |3.11 |1.82E+09 |6.28E+04 |0.0267 114.70 94.32 |17.55 |41.65 |34.91 |689.63 |59.68 |258.82 480.54 571.71 |110.76 |3.12 |1.83E+09 |6.28E+04 |0.0268 114.93 95.11 |17.64 |42.23 |35.32 |686.73 |59.42 |264.44 477.23 567.05 |109.53 |3.24 |1.89E+09 |6.17E+04 |0.0274 Red Data an average of all data points CO,/Argon Run 9: Heat Exchanger Composition -3.48 Argon,98.65 Carbon Dioxide Date -24 June 2008 Notebook Page -160 Front Page - Water Flow Rate -0.776 kg/min (0.012933 kg/s) Pressure Gauge -805 psi 342 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Pressure Transducer -868 psi Gas Inlet Temperature -120°C (248°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass |Pressure |Water |Water {Gas Gas Out |GasIn |GasIn_|Total Heat |Gas Side Nu |Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(U)Coefficient W/m2K (W/m2K) 5.89 15.69 |19.13 |22.14 |20.93 30.92 |119.79 21.80 12.35 12.40 |6.45 |0.79 |4.88E+06 |4.99£+03 |0.0040 5.93 15.64 |19.14 |22.26 |21.01 30.82 |122.28 21.58 12.39 12.44 |6.44 |0.79 |4.86E+06 |5.01E+03 |0.0040 5.90 15.58 |19.08 |22.18 |21.03 30.67 |123.97 21.39 12.25 12.30 |6.35 |0.79 |4.83E+06 |4.97E+03 |0.0039 5.81 15.50 |18.92 |22.06 |20.97 30.50 |124.08 21.27 11.91 11.96 |6.17 |0.79 |4.79E+06 |4.90E+03 |0.0039 5.64 15.41 |18.91 |21.86 |20.95 30.33 |122.92 21.22 11.53 11.57 |5.99 |0.79 |4.74E+06 |4.77E+03 |0.0039 5.34 15.34 |18.94 |21.72 |20.92 30.16 |120.47 21.25 10.91 10.95 |5.70 |0.79 |4.67E+06 |4.52E+03 |0.0040 5.21 15.38 |18.98 |21.63 |20.89 30.27 |117.25 21.52 10.64 10.68 |5.59 |0.79 |4.68E+06 |4.43E+03 |0.0041 5.55 15.49 |19.01 |21.61 |20.92 30.49 |114.32 21.85 11.26 11.31 |5.95 |0.79 |4.73E+06 |4.74E+03 |0.0040 5.66 15.59 |18.95 |21.86 |20.93 30.72 |113.11 22.08 11.38 11.43 |6.03 |0.79 |4.78E+06 |4.84E+03 |0.0041 5.84 15.61 |18.95 |22.00 |20.91 30.75 |114.39 22.02 11.82 11.87 |6.24 |0.79 |4.79E+06 |4.99E+03 |0.0040 5.88 15.58 |19.07 |22.13 |20.91 30.69 |117.44 21.78 12.20 12.24 |6.40 |0.79 |4.79E+06 |5.00E+03 |0.0040 343 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Out |GasIn |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(Ib/hr)(VU)Coefficient W/m2K (W/m2K) 5.89 15.53 |19.14 |22.32 |20.94 30.57 |120.75 21.51 12.38 12.43 |6.46 |0.79 |4.77E+06 |4.99E+03 |0.0039 5.85 15.46 |19.20 |22.41 |20.98 30.42 |122.72 21.29 12.37 12.42 |6.43 |0.79 |4.73E+06 |4.94E+03 |0.0039 5.78 15.40 |19.22 |22.40 |20.98 30.30 |122.98 21.20 12.27 12.32 |6.37 |0.79 |4.69E+06 |4.88E+03 |0.0039 5.73 15.51 |19.05 |22.04 |20.95 30.54 |119.75 21.55 11.83 11.88 |6.18 |0.79 |4.77E+06 |4.85E+03 |0.0040 Red Data an average of all data points 344 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO,/Argon Run 10: Heat Exchanger Composition -3.48 Argon,98.65 Carbon Dioxide Date -25 June 2008 Notebook Page -160 Front Page - Water Flow Rate -0.985 kg/min (0.016417 kg/s) Pressure Gauge -730 psi Pressure Transducer -788 psi Gas Inlet Temperature -190°C (374°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass Pressure |Water |Water }Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)CC)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(VU)Coefficient W/m2K (W/m2K) 38.79 54.64 |17.57 |33.18 |20.07 |169.83 |190.46 65.90 119.89 124.86 |44.51 |0.86 |8.63E+07 |2.89E+04 |0.0086 38.80 54.58 |17.43 |33.21 |19.98 |169.76 |190.58 65.81 119.54 124.48 |44.37 |0.85 |8.61E+07 |2.89E+04 |0.0086 38.85 54.56 |17.49 |33.12 |19.95 |169.69 |190.67 65.76 120.53 125.55 |44.75 |0.85 |8.60E+07 |2.89E+04 |0.0085 39.02 54.54 |17.51 |33.24 |19.96 |169.49 |190.81 65.71 121.21 126.29 |45.04 |0.85 |8.58E+07 |2.91E+04 |0.0085 39.03 $4.52 |17.52 |33.28 |19.98 |169.30 |190.91 65.67 121.08 126.15 |45.01 |0.85 |8.57E+07 |2.91E+04 |0.0085 345 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow -|(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(U)Coefficient W/m2K (W/m2K) 38.91 54.49 |17.44 |33.26 |19.99 |169.06 |190.94 65.63 119.76 124.71 |44.53 |0.85 |8.56E+07 |2.90E+04 |0.0085 38.88 54.48 |17.45 |33.64 |19.94 |169.12 |191.12 65.58 120.53 125.55 |44.80 |0.85 |8.53E+07 |2.90E+04 |0.0085 38.79 54.48 |17.53 |34.02 |20.07 |168.65 |191.16 65.58 119.68 124.63 |44.54 |0.85 |8.50E+07 |2.89E+04 |0.0085 38.64 54.47 |17.55 |34.05 |20.11 |168.40 |191.12 65.57 118.96 123.85 |44.30 |0.85 |8.49E+07 |2.88E+04 |0.0085 38.58 54.43 |17.45 |33.97 |20.08 |168.19 |191.04 65.53 117.98 122.79 |43.95 |0.85 |8.49E+07 |2.87E+04 |0.0085 38.60 54.40 |17.50 |33.93 |20.06 |168.07 |190.93 65.52 118.67 123.53 |44.24 |0.85 |8.48E+07 |2.88E+04 |0.0085 38.64 54.39 |17.55 |33.98 |20.10 |167.84 |190.81 65.52 118.92 123.80 |44.37 |0.85 |8.47E+07 |2.88E+04 |0.0085 38.62 54.38 |17.57 |33.93 |20.13 |167.63 |190.82 65.51 118.58 123.44 |44.27 |0.85 |8.47E+07 |2.88E+04 |0.0085 38.78 54.49 |17.50 |33.60 |20.03 |168.85 |190.88 65.64 119.64 124.59 |44.51 |0.85 |8.53E+07 |2.89E+04 |0.0085 Red Data an average of all data points CO 2/Argon Run 11: Heat Exchanger Composition -3.48 Argon,98.65 Carbon Dioxide Date -25 June 2008 Notebook Page -160 Front Page - Water Flow Rate -0.985 kg/min (0.016417 kg/s) Pressure Gauge -500 psi Pressure Transducer -535 psi Gas Inlet Temperature -210°C (410°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftesR (3066.27 W/m2K) 346 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater-0.000282474 Total Volume of System -0.00334 m2 347 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(VU)Coefficient W/m2K (W/m2K) 20.79 36.88 |17.78 |27.83 |19.49 87.21 |210.64 41.61 58.94 60.11 |24.82 |0.80 |3.15E+07 |1.55E+04 |0.0062 20.77 36.89 |17.78 |27.87 |19.51 87.23 |211.72 41.52 58.84 60.01 |24.74 |0.80 |3.14E+07 |1.55E+04 |0.0062 20.70 36.79 |17.76 |27.88 |19.52 86.90 |212.64 41.31 58.45 59.61 |24.55 |0.80 |3.11E+07 |1.54E+04 |0.0062 20.70 36.79 |17.67 |27.76 |19.47 86.92 |212.20 41.35 58.15 59.30 |24.44 |0.80 |3.12E+07 |1.54E+04 |0.0062 20.66 36.73 |17.71 |27.40 |19.44 86.77 |212.59 41.25 58.43 59.59 |24.55 |0.80 |3.11E+07 |1.54E+04 |0.0062 20.62 36.64 |17.72 |27.37 |19.44 86.46 |212.80 41.12 58.44 59.60 |24.56 |0.80 |3.09E+07 |1.54E+04 |0.0062 20.54 36.50 |17.71 |27.10 |19.48 85.96 |209.83 41.24 57.49 58.61 |24.27 |0.80 |3.09E+07 |1.53E+04 |0.0062 20.46 36.52 |17.62 |26.91 |19.47 86.06 |206.51 41.60 56.59 57.67 |24.00 |0.80 |3.13E+07 |1.53E+04 |0.0062 20.47 36.52 |17.64 |27.00 |19.40 86.11 |207.72 41.48 57.32 58.43 |24.27 |0.80 |3.12E+07 |1.53E+04 |0.0062 20.41 36.43 |17.56 |27.01 |19.41 85.79 |208.99 41.25 56.57 57.66 |23.92 |0.80 |3.09E+07 |1.53E+04 |0.0062 20.40 36.46 |17.60 |26.89 |19.40 85.89 |209.11 41.27 56.88 57.97 |24.04 |0.80 |3.10E+07 |1.52E+04 |0.0062 20.38 36.38 |17.60 |26.95 |19.36 85.68 |210.39 41.06 57.11 58.21 |24.10 |0.80 |3.07E+07 |1.52E+04 |0.0062 20.33 36.38 |17.57 |26.90 |19.32 85.69 |210.66 41.03 57.10 $8.21 |24.09 |0.80 |3.07E+07 |1.52E+04 |0.0062 20.32 36.20 |17.62 |26.87 |19.41 85.06 |210.89 40.80 56.69 57.78 |23.93 |0.80 |3.03E+07 |1.52E+04 |0.0061 20.45 36.16 |17.65 |26.72 |19.40 84.91 |208.33 40.99 57.16 58.26 |24.23 |0.80 |3.04E+07 |1.53E+04 |0.0062 20.53 36.55 |17.67 |27.23 |19.44 86.18 |210.34 41.26 57.61 58.73 |24.30 |0.80 |3.10E+07 |1.53E+04 |0.0062 Red Data an average of all data points CO>/Argon Run 12: Heat Exchanger Composition -3.48 Argon,98.65 Carbon Dioxide Date -26 June 2008 Notebook Page -159 348 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Front Page - Water Flow Rate -0.465 kg/min (0.0775 kg/s) Pressure Gauge -375 psi Pressure Transducer -389 psi Gas Inlet Temperature -120°C (248°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(U)Coefficient W/m2K (W/m2K) 13.11 27.90 |18.55 |24.88 |20.07 60.40 |121.24 39.56 32.07 32.41 |16.15 |0.83 |1.86E+07 |1.10E+04 |0.0061 12.95 27.74 |18.55 |24.78 |20.04 60.00 |121.84 39.26 31.82 32.16 |16.02 |0.83 |1.84E+07 |1.08E+04 |0.0060 12.91 27.79 |18.52 |24.57 |20.02 60.13 |120.36 39.51 31.54 31.87 |15.91 |0.83 |1.85E+07 |1.08E+04 |0.0061 13.05 27.83 |18.57 |24.41 |20.01 60.23 |120.40 39.56 32.11 32.46 |16.21 |0.83 |1.86E+07 |1.09E+04 |0.0061 13.01 27.71 |18.60 |24.43 |20.03 59.91 |121.40 39.26 32.16 32.51 |16.21 |0.83 |1.84E+07 |1.09E+04 |0.0060 12.94 27.78 |18.65 |24.41 |20.04 60.10 }120.94 39.43 32.10 32.45 |16.18 |0.83 |1.85E+07 |1.08E+04 |0.0061 13.03 27.75 |18.69 |24.57 |20.10 59.99 |121.74 39.28 32.32 32.67 |16.27 |0.83 |1.84E+07 |1.09E+04 |0.0060 12.90 27.60 |18.72 |24.60 |20.14 59.59 |122.17 39.01 31.93 32.27 |16.07 |0.83 |1.82E+07 |1.08E+04 |0.0060 12.72 27.59 |18.57 |24.95 |20.16 59.55 |120.13 39.23 30.68 30.99 |15.49 |0.83 |1.81E+07 |1.07E+04 |0.0061 349 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(1b/hr)(VU)Coefficient W/m2K (W/m2K) 12.89 27.69 |18.56 |24.96 |20.11 59.84 |119.20 39.51 31.22 31.55 |15.79 |0.83 |1.82E+07 |1.08E+04 |0.0061 12.91 27.58 |18.68 |25.07 |20.13 59.55 |120.49 39.18 31.83 32.17 |16.07 |0.83 |1.80E+07 |1.08E+04 |0.0060 12.70 27.48 |18.67 |25.00 |20.16 59.27 |120.11 39.08 31.07 31.40 |15.70 |0.83 |1.79E+07 |1.07E+04 |0.0060 12.78 27.61 |18.69 |24.95 |20.18 59.61 |118.90 39.42 31.20 31.53 |15.79 |0.83 |1.81E+07 |1.07E+04 |0.0061 12.84 27.56 |18.68 |25.11 |20.19 59.47 |119.85 39.23 31.30 31.63 |15.82 |0.83 |1.80E+07 |1.08E+04 |0.0060 12.77 27.53 |18.73 |25.15 |20.18 59.39 |120.65 39.08 31.49 31.82 |15.89 |0.83 |1.79E+07 |1.07E+04 |0.0060 12.85 27.58 |18.77 |25.23 |20.23 59.50 |121.36 39.07 31.70 32.04 |15.98 |0.83 |1.80E+07 |1.08E+04 |0.0060 12.83 27.50 |18.72 |25.31 |20.20 59.30 |122.22 38.85 31.58 31.92 |15.90 |0.83 |1.79E+07 |1.07E+04 |0.0060 12.89 27.66 |18.64 |24.85 |20.12 59.75 |120.77 39.27 31.65 31.99 |15.97 |0.83 |1.82E+07 |1.08E+04 |0.0060 Red Data an average of all data points CO/Argon Run 13: Heat Exchanger Composition -3.48 Argon,98.65 Carbon Dioxide Date -26 June 2008 Notebook Page -159 Front Page - Water Flow Rate -0.465 kg/min (0.0775 kg/s) Pressure Gauge -220 psi Pressure Transducer -223 psi Gas Inlet Temperature -120°C (248°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/mK) Thermal Conductivity for SS,Kw-16.0 W/mK Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 350 Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 351 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass_|Pressure |Water |Water |Gas Gas Out |GasIn |GasIn {|Total Heat |Gas Side Nu_|Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(Ib/hr)(VU)Coefficient W/m2K (W/m2K) 5.89 15.69 |19.13 |22.14 |20.93 30.92 |119.79 21.80 12.35 12.40 |6.45 |0.79 |4.88E+06 |4.99E+03 |0.0040 5.93 15.64 }|19.14 |22.26 |21.01 30.82 |122.28 21.58 12.39 12.44 |6.44 |0.79 |4.86E+06 |5.01E+03 |0.0040 5.90 15.58 |19.08 |22.18 |21.03 30.67 |123.97 21.39 12.25 12.30 |6.35 |0.79 |4.83E+06 |4.97E+03 |0.0039 5.81 15.50 |18.92 |22.06 |20.97 30.50 |124.08 21.27 11.9]11.96 |6.17 |0.79 |4.79E+06 |4.90E+03 |0.0039 5.64 15.41 |18.91 |21.86 |20.95 30.33 |122.92 21.22 11.53 11.57 |5.99 |0.79 |4.74E+06 |4.77E+03 |0.0039 5.34 15.34 |18.94 |21.72 |20.92 30.16 |120.47 21.25 10.91 10.95 |5.70 |0.79 |4.67E+06 |4.52E+03 |0.0040 5.21 15.38 |18.98 |21.63 |20.89 30.27 |117.25 21.52 10.64 10.68 |5.59 |0.79 |4.68E+06 |4.43E+03 |0.0041 5.55 15.49 {|19.01 |21.61 |20.92 30.49 |114.32 21.85 11.26 11.31 |5.95 |0.79 |4.73E+06 |4.74E+03 |0.0040 5.66 15.59 |18.95 |21.86 |20.93 30.72 |113.11 22.08 11.38 11.43 |6.03 |0.79 |4.78E+06 |4.84E+03 |0.0041 5.84 15.61 |18.95 |22.00 |20.91 30.75 |114.39 22.02 11.82 11.87 |6.24 |0.79 |4.79E+06 |4.99E+03 |0.0040 5.88 15.58 |19.07 |22.13 |20.91 30.69 |117.44 21.78 12.20 12.24 |6.40 |0.79 |4.79E+06 |5.00E+03 |0.0040 5.89 15.53 |19.14 |22.32 |20.94 30.57 |120.75 21.51 12.38 12.43 |6.46 |0.79 |4.77E+06 |4.99E+03 |0.0039 5.85 15.46 |19.20 |22.41 |20.98 30.42 |122.72 21.29 12.37 12.42 |6.43 |0.79 |4.73E+06 |4.94E+03 |0.0039 5.78 15.40 |19.22 |22.40 |20.98 30.30 |122.98 21.20 12.27 12.32 |6.37 |0.79 |4.69E+06 |4.88E+03 |0.0039 5.73 15.51 |19.05 |22.04 |20.95 30.54 |119.75 21.55 11.83 11.88 |6.18 |0.79 |4.77E+06 |4.85E+03 |0.0040 Red Data an average of all data points 352 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Heat Exchanger Data Components - Argon Carbon Dioxide GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0.99778 0.99744 0.99815 0.9939 |0.996818 Carbon Dioxide 97.49901 |97.46502 |97.54221 |97.15582 |97.41552 Argon 3.4 3.39745 3.39918 3.39796 |3.398648 GC Run 9: Agilent Cerity QA/QC Report Sample name:0613-HeatXGRArCO08 Sample note: Submission time:Friday,June 13,2008 9:53:27 AM Operator: Injection date:Friday,June 13,2008 10:01:00 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:June11Calibration Method last saved:Thursday,June 12,2008 9:41:15 AM 353 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >7 '... | j i - i 7 i 2 | ; , o =.cee bees aay t 7©: T T T T T 05 4 15 2 25 min TCDZA >4 oe.ky weed bce :aan a 7 a .- ifsBR =]'a '-eee ere --e-eeee ero 05 1 14 2 25 min TCD3A o-oo *oe?: 2 ;g |i Q i i.3. |2 | !3 : A wr i .7 .,_ 05 1 AS 2 25 min ESTD Report Calibration last saved:Thursday,June 12,2008 9:28:52 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 354 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Inlet Signal 1 WWNNDN=Total amount GC Run 10: Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 0.853 0.973 0.290 0.324 1.503 1.490 2.618 Oxygen ---Nitrogen BP 7.9548e+004 1.25431e-005 0.99778 |Oxygen/NitrogenVB=.2..2238e+006 4.38439e-005 97.49901 Carbon Dioxide ---Sulfur Dioxide BB =2.0810e+004 1.63381e-004 3.40000 Argon/Oxygen ---Nitrogen_2 =101.89680 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated Agilent Cerity QA/QC Report Sample name:0613-HeatXGRArCOO9 Sample note: Submission time:Friday,June 13,2008 9:53:30 AM Operator: Injection date:Friday,June 13,2008 10:04:34 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:June11Calibration Method last saved:Thursday,June 12,2008 9:41:15 AM 355 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >:3 4 --h - ' 1 4 i=]:Oo 4 _,®: 0 SEE En nS ee ee ee een eee lene ann nee ee 05 4 15 2 25 min TCDZA _a Lt ee T T 15 2 25 min TCD3A a7 ots 15 »|; i +=cej:: :Qo i|i 3 ;-fo ane "opty T _-1 ;7 i Eg i'::Pq i4+° +.L o i i «j8|z | 4:Se , i ay Of 1 a AS _2 25 min ESTD Report Calibration last saved:Thursday,June 12,2008 9:28:52 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 356 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area ['iV*s]Amt/Area Amount[]Name 1 0.853 ---Oxygen 1 0.973 ---Nitrogen 2 0.290 BP 7.9577e+004 1.25431e-005 0.99815 Oxygen/Nitrogen 2 0.324 VB =.2.2248e+006 4.38439e-005 97.54221 Carbon Dioxide 2 1.503 ---Sulfur Dioxide 3 1.491 BB 2.0805e+004 1.63381e-004 3.39918 |Argon/Oxygen 3 2.618 ---Nitrogen_2 Total amount =101.93954 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 11: Agilent Cerity QA/QC Report Sample name:0613-HeatXGRArCO010 Sample note: Submission time:Friday,June 13,2008 9:53:30 AM Operator: Injection date:Friday,June 13,2008 10:08:07 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:June11 Calibration Method last saved:Thursday,June 12,2008 9:41:15 AM 357 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >7 |=: ' H ' 2 |oO '. a i any 0.6 4 416 2 25 min TCD2A ey 3 Cc-GO.,ao7!aee oa : ao :No.:i o. .T T T eee ns 1 15 2 25 min TCD3ZA it Senr eens @ 5 ! 9 i¢ 3 2 iete<x.i aea -- T ,-,a --+ 1 15 -2 ee 25 _min ESTD Report Calibration last saved:Thursday,June 12,2008 9:28:52 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 358 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [\iV's]Amt/Area Amount[]Name 1 0.853 ---Oxygen 1 0.973 ---Nitrogen 2 0.290 BP 7.9239e+004 1.25431e-005 0.99390 Oxygen/Nitrogen 2 0.324 VB 2.2160e+006 4.38439e-005 97.15582 Carbon Dioxide 2 1.503 ---Sulfur Dioxide 3 1.491 BB 2.0798e+004 1.63381e-004 3.39796 §Argon/Oxygen 3 2.618 ---Nitrogen_2 Total amount =101.54768 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 12: Agilent Cerity QA/QC Report Sample name:0613-HeatXGRArCOO7 Sample note: Submission time:Friday,June 13,2008 9:53:27 AM Operator: Injection date:Friday,June 13,2008 9:57:26 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:June11Calibration Method last saved:Thursday,June 12,2008 9:41:15 AM 359 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA ' a 15 2 28 min TCDZA -T T 15 2 245 min TCDSA 2 <aed i a 4 = i G !<."9 i 2 i a ae o j Py 8 b 3.. 8 < AEA na SR4152_-26 min ESTD Report Calibration last saved:Thursday,June 12,2008 9:28:52 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 360 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 1 0.853 ---Oxygen 1 0.973 . ---Nitrogen 2 0.290 BP 7.9521e+004 1.25431e-005 0.99744 Oxygen/Nitrogen 2 0.324 VB 2.2230e+006 4.38439e-005 97.46502 Carbon Dioxide 2 1.503 ---Sulfur Dioxide 3 1.491 BB 2.0795e+004 1.63381e-004 3.39745 Argon/Oxygen 3 2.618 ---Nitrogen_2 Total amount =101.85991 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated CO,/Argon Run 14: Heat Exchanger Composition -3.40 Argon,97.42 Carbon Dioxide,1.00 Air Date -11 June 2008 Notebook Page -N/A Front Page - Water Flow Rate -1.016 kg/min (0.01693 kg/s) Pressure Gauge -570 psi Pressure Transducer -608 psi Gas Inlet Temperature -258°C (500°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 361 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(@C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(Ib/hr)(U)Coefficient W/m2K (W/m2K) 25.78 41.87 |16.78 |27.78 |19.29 |105.12 |208.94 47.63 69.74 71.39 |28.71 |0.81 |4.32E+07 |1.92E+04 |0.0068 25.79 41.88 |16.62 |27.77 |19.24 |105.21 |209.67 47.56 69.14 70.76 |28.42 |0.81 |4.32E+07 |1.92E+04 |0.0068 25.79 41.83 |16.59 |27.68 |19.18 |105.08 |210.37 47,42 69.31 70.94 |28.47 |0.81 |4.30E+07 |1.92E+04 |0.0068 25.76 41.80 |16.46 |27.50 |19.09 |105.03 |209.32 47.50 68.92 70.54 |28.36 |0.81 |4.32E+07 |1.92E+04 |0.0068 25.79 41.83 |16.60 |27.59 |19.06 |105.20 |209.49 47.52 70.08 71.75 |28.83 |0.81 |4.32E+07 |1.92E+04 |0.0068 25.79 41.79 |16.55 |27.67 |19.11 |105.01 |210.44 47.37 69.47 TL.A1 |28.54 |0.81 |4.29E+07 |1.92E+04 |0.0068 25.76 41.81 |16.54 |27.51 |19.09 |105.07 |209.78 47.46 69.47 71.11 |28.57 |0.81 |4.31E+07 |1.91E+04 |0.0068 25.79 41.82 |16.63 |27.64 |19.09 |105.11 |210.10 47.43 70.11 71.78 |28.82 |0.81 |4.30E+07 |1.92E+04 |0.0068 25.74 41.81 |16.69 |27.69 |19.16 |105.02 |209.80 47.46 69.90 71.56 |28.75 |0.81 |4.30E+07 |1.91E+04 |0.0068 25.76 41.82 |16.73 |27.75 |19.21 |104.98 |210.24 47.41 69.92 71.58 |28.74 |0.81 |4.29E+07 |1.91E+04 |0.0068 25.72 41.80 |16.74 |27.72 |19.26 |104.86 |209.81 47.44 69.48 71.12 |28.58 |0.81 |4.30E+07 |1.91E+04 |0.0068 25.75 41.82 |16.61 |27.67 |19.22 |105.00 |209.42 47.51 69.07 70.69 |28.41 |0.81 |4.31E+07 |1.91E+04 |0.0068 25.74 41.75 |16.66 |27.60 |19.17 |104.78 |209.61 47.Al 69.56 71.21 |28.62 |0.81 |4.29E+07 |1.91E+04 |0.0068 25.71 41.79 |16.71 |27.61 |19.19 |104.89 |209.01 47.52 69.67 71.32 |28.69 |0.81 |4.31E+07 |1.91E+04 |0.0068 25.74 41.77 |16.72 |27.70 |19.24 |104.78 |209.61 47.43 69.55 71.19 |28.62 |0.81 |4.29E+07 |1.91E+04 |0.0068 25.66 41.75 |16.75 |27.61 |19.26 1 104.67 |208.69 47.51 69.26 70.89 |28.54 |0.81 |4.30E+07 |1.91E+04 |0.0068 25.75 41.81 |16.65 |27.66 |19.18 |104.99 |209.64 47.47 69.54 71.18 |28.60 |0.81 |4.31E+07 |1.91E+04 |0.0068 Red Data an average of all data points 362 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO,/Argon Run 15: Heat Exchanger Composition -3.40 Argon,97.42 Carbon Dioxide,1.00 Air Date -10 June 2008 Notebook Page -N/A Front Page - Water Flow Rate -1.275 kg/min (0.02125 kg/s) Pressure Gauge -570 psi Pressure Transducer -N/A Gas Inlet Temperature -126°C Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater-0.000282474 Total Volume of System -0.00334 m2 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)CC)|CC)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(VU)Coefficient W/m2K (W/m2K) 25.15 41.92 |16.90 |22.01 |19.59 |104.96 |124.92 60.44 60.05 61.27 |28.00 |0.88 |5.61E+07 |2.06E+04 |0.0081 24.88 41.67 |16.82 |22.11 |19.60 |104.00 |130.73 58.91 59.25 60.44 |27.42 |0.87 |5.46E+07 |2.02E+04 |0.0080 24.23 41.35 |16.90 |21.72 |19.61 |102.80 |126.53 59.24 57.44 58.56 |26.81 |0.88 |5.40E+07 |1.98E+04 |0.0080 24.37 41.54 |16.91 |21.56 |19.65 |103.49 |120.34 60.80 57.18 58.29 |26.91 |0.88 |5.54E+07 |2.00E+04 |0.0082 25.02 41.88 |16.93 |21.94 |19.64 |104.78 |123.50 60.68 59.45 60.65 |27.79 |0.88 |5.61E+07 |2.05E+04 |0.0082 363 Mass_|Pressure |Water |Water |Gas Gas Out |GasIn |GasIn_|Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out |Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(Ib/hr)(VU)Coefficient W/m2K (W/m2K) 25.02 41.76 |16.98 |22.28 |19.65 |104.30 |130.69 59.06 60.26 61.49 |27.88 |0.87 |5.47E+07 |2.03E+04 |0.0080 24.39 41.41 |17.02 |22.01 |19.66 |102.99 |129.15 58.83 58.49 59.64 |27.19 |0.87 |5.38E+07 |1.98E+04 |0.0080 24.20 41.41 |16.89 |21.54 |19.65 |102.96 |121.88 60.26 56.66 57.75 |26.63 |0.88 |5.48E+07 |}1.99E+04 |0.0081 24.80 41.78 |16.95 |21.80 |19.62 |104.43 |}121.50 60.94 $8.90 60.08 |27.64 |0.88 |5.60E+07 |2.04E+04 |0.0082 25.11 41.84 |16.99 |22.33 |19.68 |104.58 |129.06 $9.50 60.28 61.51 |27.95 |0.87 |5.52E+07 |2.04E+04 |0.0080 24.62 41.53 |16.97 |22.24 |19.68 |103.41 |130.93 58.67 58.98 60.16 |27.32 |0.87 |5.39E+07 |2.00E+04 |0.0080 24.20 41.38 |17.00 |21.82 |19.73 |102.80 |124.45 59.70 57.07 58.17 |26.72 |0.88 |5.42E+07 |1.98E+04 |0.0081 24.69 41.73 |16.97 |21.84 |19.73 |104.11 |122.04 60.74 58.05 59.19 |27.22 |0.88 |5.57E+07 |2.02E+04 |0.0082 25.12 41.83 |16.85 |22.21 |19.66}104.58 |128.47 59.61 59.59 60.79 |27.65 |0.88 |5.53E+07 |2.04E+04 |0.0080 24.68 41.54 |16.85 |22.12 |19.62 |103.50 |131.34 58.60 58.84 60.01 |27.23 |0.87 |5.40E+07 |2.00E+04 |0.0080 24.18 41.30 |16.73 |21.61 |19.60 |102.62 |125.36 59.39 56.34 57.41 |26.35 |0.88 |5.41E+07 |1.98E+04 |0.0081 24.58 41.61 |16.79 |21.54 |19.52 |103.86 |121.42 60.67 57.92 59.06 |27.21 |0.88 |5.56E+07 |2.02E+04 |0.0082 25.10 41.81 |16.79 |22.03 |19.60 |104.55 |127.10 59.84 59.41 60.60 |27.63 |0.88 |5.55E+07 |2.05E+04 |0.0081 24.87 41.60 |16.81 |22.10 |19.58 |103.79 |131.64 58.65 59.33 60.53 |27.44 |0.87 |5.43E+07 |2.02E+04 |0.0080 24.69 41.63 |16.90 |21.94 |19.63 |103.82 |126.37 59.71 58.61 59.77 |27.31 |0.88 |5.49E+07 |2.02E+04 |0.0081 Red Data an average of all data points CO?/Argon Run 16: Heat Exchanger Composition -3.40 Argon,97.42 Carbon Dioxide,1.00 Air Date -12 June 2008 Notebook Page -N/A Front Page - Water Flow Rate -0.9475 kg/min (0.015792 kg/s) Pressure Gauge -250 psi Pressure Transducer - Gas Inlet Temperature -185°C 364 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwin(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 365 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(VU)Coefficient W/m2K (W/m2K) 7.66 17.37 |16.74 |20.02 |19.53 34.84 |186.08 20.39 16.56 16.65 |11.95 |0.77 |6.23E+06 |5.97E+03 |0.0037 7.61 17.41 |16.60 |19.92 |19.51 34.93 |185.40 20.47 16.29 16.38 |11.77 |0.77 |6.27E+06 |5.94E+03 |0.0038 7.67 17.39 |16.62 |19.86 |19.47 34.90 |185.09 20.46 16.48 16.57 |11.92 |0.77 |6.26E+06 |5.99E+03 |0.0038 7.65 17.38 |16.70 |19.90 |19.50 34.88 |185.11 20.46 16.50 16.59 |11.94 |0.77 |6.25E+06 |5.97E+03 |0.0038 7.60 17.43 |16.75 |19.90 |19.47 35.00 |184.52 20.54 16.48 16.57 |11.94 |0.77 |6.30E+06 |5.93E+03 |0.0038 7.64 17.44 |16.79 |20.00 |19.53 35.01 |184.58 20.55 16.56 16.66 |12.00 |0.77 |6.30E+06 |5.97E+03 |0.0038 7.70 17.39 |16.83 |20.07 |19.56 34.89 |185.60 20.44 16.72 16.81 |12.08 |0.77 |6.25E+06 |6.00E+03 |0.0037 7.63 17.40 |16.86 |20.09 |19.58 34.91 |185.77 20.45 16.60 16.69 |11.99 |0.77 |6.25E+06 |5.95E+03 |0.0038 7.60 17.44 |16.89 |20.13 |19.68 34.98 |185.25 20.52 16.42 16.51 |11.87 |0.77 |6.28E+06 |5.93E+03 |0.0038 7.67 17.41 |16.83 |20.21 |19.73 34.91 |185.59 20.47 16.42 16.51 |11.86 |0.77 |6.25E+06 |5.98E+03 |0.0038 7.71 17.34 }16.80 |20.09 |19.71 34,75 |186.14 20.35 16.51 16.60 |11.91 |0.77 |6.20E+06 |6.01E+03 |0.0037 7.67 17.31 |16.89 |20.08 |19.69 34.68 |185.00 20.37 16.53 16.62 |11.96 |0.77 |6.18E+06 |5.99E+03 |0.0037 7.60 17.34 |16.80 |20.09 |19.71 34.75 |183.20 20.50 16.19 16.28 |11.77 |0.77 |6.22E+06 |5.94E+03 |0.0038 7.65 17.39 |16.78 |20.03 |19.59 34.88 |185.18 20.46 16.48 16.57 |11.92 |0.77 |6.25E+06 |5.97E+03 |0.0038 Red Data an average of all data points CO,/Argon Run 17: Heat Exchanger Composition -3.40 Argon,97.42 Carbon Dioxide,1.00 Air Date -12 June 2008 Notebook Page -N/A Front Page - Water Flow Rate -0.9475 kg/min (0.015792 kg/s) 366 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 ES 6€-_ -_x Pressure Gauge -235 psi Pressure Transducer -243 psi Gas Inlet Temperature -130°C (266°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu_|Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer (tb/hr)(U)Coefficient W/m2K (W/m2K) 7.23 16.77 |16.64 |18.74 |19.22 33.55 |129.02 22.75 14.19 14.26 |7.29 |0.79 |6.05E+06 |6.06E+03 |0.0040 7.27 16.83 |16.66 |18.74 |19.26 33.68 |128.79 22.85 14.24 14.31 |7.31 |0.79 |6.09E+06 |6.10E+03 |0.0040 7.33 16.80 |16.67 |18.81 |19.27 33.62 |129.5]22.76 14.37 14.44 |7.37 |0.79 |6.07E+06 |6.14E+03 |0.0040 7.30 16.74 |16.68 |18.84 |19.31 33.49 |130.40 22.63 14.32 14.39 |7.33 |0.79 |6.02E+06 |6.11E+03 |0.0040 7.23 16.69 |16.68 |18.81 |19.34 33.35 |130.30 22.55 14.13 14.20 |7.24 |0.79 |5.98E+06 |6.05E+03 |0.0040 7.19 16.75 |16.63 |18.78 |19.34 |33.51]129.18]22.72 13.93 14.00 |7.15 |0.79 |6.04E+06 |6.02E+03 |0.0040 7.24 16.80 |16.52 |18.68 |19.26 33.62 |128.42 22.83 13.99 14.05 |7.19 |0.79 |6.08E+06 |6.08E+03 |0.0040 7.29 16.76 |16.51 |18.68 |19.28 33.54 |128.69 22.76 14.03 14.10 |7.21 |0.79 |6.05E+06 |6.11E+03 |0.0040 7.27 16.70 |16.33 |18.56 |19.17 33.42 |129.27 22.64 13.94 14.00 |7.16 |0.79 |6.02E+06 |6.09E+03 |0.0040 7.21 16.65 |16.34 |18.43 |19.03 33.33 |129.05 22.59 14.01 14.08 |7.20 |0.79 |5.98E+06 |6.05E+03 |0.0040 TAT 16.74 |16.39 |18.45 |18.97 33.53 |127.83 22.78 14.05 14.12 |7.24 |0.79 |6.05E+06 |6.03E+03 |0.0040 367 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass_|Pressure |Water |Water |Gas Gas Out |GasIn |Gas In Total Heat |Gas Side Nu |Pr Gr Re Friction Flow j;(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(Ib/hr)(U)Coefficient W/m2K (W/m2K) 7.25 16.78 |16.44 |18.49 |18.99 33.61 |127.42 22.86 14.23 14.30 |7.33 |0.79 |6.07E+06 |6.09E+03 |0.0040 7.29 16.74 |16.37 |18.56 |19.02 33.53 |127.88 22.78 14.18 14.25 |7.30 |0.79 |6.04E+06 |6.12E+03 |0.0040 7.27 16.68 |16.35 |18.48 |18.97 33.40 |128.56 22.66 14,21 14.27 |7.30 |0.79 |6.00E+06 |6.10E+03 |0.0040 7.21 16.68 |16.42 |18.49 |18.93 33.40 |128.46 22.66 14,25 14.31 |7.33 |0.79 |5.99E+06 |6.05E+03 |0.0040 7.25 16.74 |16.51 |18.64 |19.16 33.50 |128.85 22.72 14.14 14.21 |7.26 |0.79 |6.04E+06 |6.08E+03 |0.0040 Red Data an average of all data points Heat Exchanger Data Components- Argon Carbon Dioxide GC Analysis- Trial 1 Trial 2 Trial 3 Trial 4 Average Carbon Dioxide 96.69519 96.53057 96.5423 1 96.64613 96.60355 Argon 3.49418 3.4899 3.48547 3.48039 3.487485 GC Run 13: Agilent Cerity QA/QC Report Sample name:0708-HeatXGRArCOO5 Sample note: Submission time:Tuesday,July 08,2008 3:50:44 PM Operator: 368 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Injection date:Tuesday,July 08,2008 3:51:08 PM GC Description:Micro GC Signal description:TCD1 A;TCD2 A;TCD3 A Method:July2Calibration2 Method last saved:Thursday,July 03,2008 12:58:01 PM TCDIA >..: =a 4 es ca 7 : ae oo |.'Sheedceedeeb=4 :: 6 +=aa t 1rs]':' 4 t Oo 4 nee en a |ae .------r 06 41 15 2 25 min TCD2A >J .....j ot2::i i[=]°°2 apron Soe >--a "a i 5 oO ot t +? 2 ::.: md :,te .: oO.i :: 8 fe :. 3 <a A.oe ame Ae oe on r ro .9 a.a o i.t Tr 'T T Tr _* 05 4 15 2 25 min TCD3A >:".a4aA | i i : a .Ss +: ELBe F ! ; :a |i ' "Be : 9 :°oR , °:Mf,|: :b=4 aan nh os a 7 oan ona oho a "pt | T T T T +T r v T 7 05 4 15 2 25 min 369 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 ESTD Report Calibration last saved:Thursday,July 03,2008 12:58:01 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [iV*s]Amt/Area 1 1.477 - 1 1.627 --- 2 0.292 PV 7.5087e+004 0.00000e+000 0.00000 2 0.325 VB 2.0243e+006 4.77424e-005 96.64613 2 1.496 --- 3 1.376 PB =1.7584e+004 1.97930e-004 3.48039 Total amount =100.12652 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 14: Agilent Cerity QA/QC Report Sample name:0708-HeatXGRArCOO6 Sample note: Submission time:Tuesday,July 08,2008 3:50:44 PM Operator: Injection date:Tuesday,July 08,2008 3:54:42 PM GC Description:Micro GC Signal description:TCD1 A;TCD2 A;TCD3 A Method:July2Calibration2 Method last saved:Thursday,July 03,2008 12:58:01 PM 370 Amount [mass%]Name Oxygen Nitrogen Carbon Dioxide Sulfur Dioxide Argon/Oxygen Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCOTA ae | 16 2 Bm TCD2A yon Cp ; it |as 45 2 25 min TCD3A >.a 4 _i-AL |! =e : 8 Re o ee + en yee re a ee eee ESTD Report Calibration last saved:Thursday,July 03,2008 12:58:01 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 371 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount [mass%]Name 1 1.477 ---Oxygen 1 1.627 ---Nitrogen 2 0.292 PV 7.4995e+004 0.00000e+000 0.00000 2 0.325 VB =.2.0222e+006 4.77424e-005 96.54231 Carbon Dioxide 2 1.496 ---Sulfur Dioxide 3 1.377 PB =1.7610e+004 1.97930e-004 3.48547 Argon/Oxygen Total amount =100.02777 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 15: Agilent Cerity QA/QC Report Sample name:0708-HeatXGRArCOO7 Sample note: Submission time:Tuesday,July 08,2008 3:50:45 PM Operator: Injection date:Tuesday,July 08,2008 3:58:16 PM GC Description:Micro GC Signal description:TCD1 A;TCD2 A;TCD3 A Method:July2Calibration2 Method last saved:Thursday,July 03,2008 12:58:01 PM 372 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >I=a 7 |: ° : =]rt ae '-a ro oa'.1-a i - ,; o -_- *LU J LJ hd 14 2 25 min TCDZA >le |=Co +_ oe a a =a o !:|- 2 'i ' o 3 .4 :i a 5 ovat i :a ia roe :a cao L °OL,,Lo,i oNi|* QO._-i . ;fay |;a . see 1 "|oe >fe ' T ees |T T ee r 08 1 15 2 25 min TCDZA >j ::It :a !a A Ee..j } ooSi tc;.{.=a i t 'ed ;iaae; ..&:;: + _a nee.a as ey eee --ns en: T-T -T =7 0.6 4 15 2 2.5 min ESTD Report Calibration last saved:Thursday,July 03,2008 12:58:01 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 373 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount [mass%]Name 1 1.477 ---Oxygen 1 1.627 ---Nitrogen 2 0.292 PV 7.4977e+004 0.00000e+000 0.00000 2 0.325 VB 2.0219e+006 4.77424e-005 96.53057 Carbon Dioxide 2 1.496 ---Sulfur Dioxide 3 1.377 PB 1.7632e+004 1.97930e-004 3.48990 Argon/Oxygen Total amount =100.02047 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 16: Agilent Cerity QA/QC Report Sample name:0708-HeatXGRArCOO8 Sample note: Submission time:Tuesday,July 08,2008 3:50:46 PM Operator: Injection date:Tuesday,July 08,2008 4:01:49 PM GC Description:Micro GC Signal description:TCD1 A;TCD2 A;TCD3 A Method:July2Calibration2 Method last saved:Thursday,July 03,2008 12:58:01 PM 374 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDI1A >i 1 : =|:| 1 ! .Poe fe |: -:|i ee .feevcpeenpen te teed ae oei's];i4-fe chee ate i "|hae j i i o -|ee os oo .i --S[---- 0.6 41 16 2 25 min TCD2A 24 .¢4 i 2 3 a ec : i fi.o-4-.i -a 8 -L 8 J ft)-boc 7 -(©.:.{i .wo.I..:{N :H iQo.4 do.k fs "sy ob. °po oe 1 i i yt :T s -S 06 4 15 2 25 min TCD3A >|..' a .!&i :_j : --=€o st * :=i { fF ||3 :;; Sf |:a ::ke -i !8 CO n ot ---+--T-:---7s v r 2 ++7 1 15 2 25 ;min ESTD Report Calibration last saved:Thursday,July 03,2008 12:58:01 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 375 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[mass%]Name 1 1.477 ---Oxygen 1 1.627 ---Nitrogen 2 0.292 PV 7.5142e+004 0.00000e+000 0.00000 2 0.326 VB =.2.0254e+006 4.77424e-005 96.69519 Carbon Dioxide 2 1.496 ---Sulfur Dioxide 3 1.377 PB 1.7654e+004 1.97930e-004 3.49418 Argon/Oxygen Total amount =100.18937 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated CO,/Argon Run 18: Heat Exchanger Composition -3.49 Argon,96.60 Carbon Dioxide Date -01 July 2008 Notebook Page -159 Front Page - Water Flow Rate -0.442 kg/min (0.0073667 kg/s) Pressure Gauge -1350 psi Pressure Transducer -1484 psi Gas Inlet Temperature -73°C (163.4°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 376 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out |Gas GasIn_|Coefficient |Transfer Meter |Pressure |In Out Out Density |In Density |(U)Coefficient Friction (lb/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|CC)|(kg/m3)|W/m2K (W/m2K)Nu Pr Gr Re Factor 103.60 101.02 |19.22 |56.30 |39.42 |647.18 |70.94 |249.09 450.84 530.17 |107.43 |2.27 |1.04E+09 |5.90E+04 |0.0255 103.58 101.33 |19.26 |57.08 |39.70 |643.85 |71.76 |247.83 448.32 526.68 {107.10 |2.23 |1.02E+09 |5.92E+04 |0.0253 103.70 101.42 |19.32 |57.34 |39.77 |643.12 |72.13 |247.09 448.38 526.76 |107.24 |2.21 |1.00E+09 |5.94E+04 |0.0252 103.63 101.59 |19.37 |57.56 |39.90 |641.77 |72.54 |246.53 445,27 522.48 |106.53 |2.19 |9.93E+08 |5.95E+04 |0.0251 103.75 101.60 |19.32 |57.78 |39.91 |641.68 |72.87 |245.56 445.50 522.80 |106.69 |2.17 |9.83E+08 |5.97E+04 |0.0250 103.60 101.49 |19.32 |57.70 |39.91 |640.98 |72.67 |245.75 445.26 522.46 |106.64 |2.17 |9.84E+08 |5.96E+04 |0.0250 103.44 101.53 |19.34 |57.69 |40.20 |635.58 |72.51 |246.36 437.88 512.33 |104.86 |2.17 |9.83E+08 |5.95E+04 |0.0250 103.47 101.58 |19.40 |57.67 |40.08 |638.31 |72.51 |246.58 441.75 517.63 |105.76 |2.18 |9.86E+08 |5.94E+04 |0.0251 103.39 101.63 |19.46 |57.81 |40.08 |638.66 |72.63 |246.45 443.13 519.53 |106.14 |2.18 |9.81E+08 |5.94E+04 |0.0251 103.42 101.69 |19.50 |57.97 |40.13 |638.04 |72.89 |245.91 442.54 518.72 |106.07 |2.16 |9.73E+08 |5.95E+04 |0.0250 103.57 101.76 |19.52 |58.17 |40.21 |637.00 |73.26 |245.10 441,33 517.06 |105.88 |2.14 |9.63E+08 |5.97E+04 |0.0249 103.26 101.81 |19.57 |58.32 |40.15 |638.53 |73.48 |244.61 442.74 519.00 |106.23 |2.14 |9.57E+08 |5.96E+04 |0.0249 103.01 101.83 |19.65 |58.14 |40.37 |634.43 |73.33 |245.15 435.12 508.55 |104.30 |2.14 |9.60E+08 |5.94E+04 |0.0249 103.16 101.74 |19.57 |58.26 |40.21 |636.89 |73.26 |244.99 441.48 $17.27 |105.94 |2.14 |9.58E+08 |5.95E+04 |0.0249 103.20 101.69 |19.55 |58.14 |40.25 |635.62 |73.34 |244.56 437.75 512.15 |105.00 |2.13 |9.58E+08 |5.96E+04 |0.0248 103.22 101.59 |19.55 |58.15 |40.16 |636.88 |73.44 |243.89 440.00 515.24 |105.60 |2.13 |9.53E+08 |5.97E+04 |0.0248 103.34 101.19 |19.44 |57.45 |39.84 |640.26 |73.22 |242.89 439.94 515.16 |105.41 |2.13 |9.64E+08 |5.99E+04 |0.0247 102.27 101.77 |19.38 |58.23 |40.24 |636.45 |73.00 |245.91 436.13 509.94 |104.39 |2.16 |9.70E+08 |5.89E+04 |0.0250 102.18 102.13 |19.46 |58.82 |40.58 |632.21 |73.32 |246.38 433.06 505.75 |103.79 |2.14 |9.57E+08 |5.88E+04 |0.0250 102.35 102.32 |19.55 |59.29 |40.76 |629.95 |73.75 |245.86 433.41 $06.22 |104.10 |2.12 |9.41E+08 |5.90E+04 |0.0249 103.26 101.63 |19.44 |57.89 |40.09 |638.37 |72.84 |245.82 441.49 517.30 |105.76 |2.16 |9.76E+08 |5.94E+04 |0.0250 Red Data an average of all data points 377 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO2/Argon Run 19: Heat Exchanger Composition -3.49 Argon,96.60 Carbon Dioxide Date -02 July 2008 Notebook Page -159 Front Page -- Water Flow Rate -0.641 kg/min (0.0106833 kg/s) Pressure Gauge -1045 psi Pressure Transducer -1131 psi Gas Inlet Temperature -105°C (221 °F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2KwIn(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out Gas In Coefficient |Transfer Meter |Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (b/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|CC)(kg/m3)|W/m2K (W/m2K)Nu Pr Gr Re Factor 73.61 77.87 |18.67 |47.88 |29.13 |706.72 |105.30 |132.80 346.36 391.35 |79.89 |1.15 |2.96E+08 |5.45E+04 |0.0143 73.61 77.83 |18.67 |47.84 |29.07 |707.57 |105.22 |132.78 347.43 392.71 |80.13 |1.15 |2.96E+08 |5.45E+04 |0.0143 73.57 77.85 |18.69 |47.70 |29.08 |707.54 |104.95 |132.99 347.35 392.60 |80.11 }1.15 |2.97E+08 |5.45E+04 |0.0143 73.48 77.90 |18.76 |47.73 |29.23 |704.80 |104.74 |133.24 345.38 390.09 |79.74 |1.15 |2.98E+08 |5.44E+04 |0.0143 73.46 77.94 |18.82 |47.83 |29.32 |703.27 |104.74 |133.34 344.82 389.38 |79.66 |1.15 |2.97E+08 |5.44E+04 |0.0143 73.41 77.99 |18.89 |47.87 |29.43 |701.20 |104.92 |133.32 342.89 386.91 |79.24 |1.15 |2.97E+08 |5.43E+04 |0.0143 378 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas Side Mass Transfer Heat Flow Water |Water |Gas Gas Out Gas In Coefficient |Transfer Meter |Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction(ib/hr)|(bar)eC)}@C)|CC)|(ke/m3)|(°C)___|(kg/m3)|Wim2K (W/m2K)|Nu |Pr |Gr Re Factor 73.36 78.02 |18.91 |47.99 |29.47 |700.67 |105.16 |133.21 342.28 386.15 |79.10 |1.15 |2.97E+08 |5.43E+04 |0.0143 73.53 77.81 |18.76 |47.35 |29.29 |703.09 |105.02 |132.88 342.45 386.35 |79.04 |1.15 |2.98E+08 |5.44E+04 |0.0143 73.54 77.62 |18.73 |46.53 |29.04 |707.05 |104.48 |132.84 344.81 389.36 |79.49 |1.15 |3.00E+08 |5.45E+04 |0.0143 73.55 77.55 |18.61 |46.40 |28.90 |709.34 |104.23 |132.86 346.11 391.02 |79.73 |1.15 |3.00E+08 |5.45E+04 |0.0143 73.50 77.48 |18.63 |46.22 |28.90 |708.93 |104.01 |132.87 345.80 390.63 |79.67 |1.16 |3.00E+08 |5.45E+04 |0.0143 73.42 77.45 |18.69 |46.02 |28.86 |709.73 |103.55 |133.14 347.22 392.44 |80.02 |1.16 |3.02E+08 |5.45E+04 |0.0143 73.39 77.42 |18.68 |45.89 |28.75 |711.60 |103.34 |133.21 348.99 394.70 |80.39 |1.16 |3.02E+08 |5.45E+04 |0.0143 73.36 77.39 |18.66 |45.91 |28.74 |711.65 |103.31 |133.16 348.94 394.65 |80.38 |1.16 |3.02E+08 |5.44E+04 |0.0143 73.28 77.42 |18.68 |46.05 |28.72 |712.12 |103.53 |133.08 349.19 394.96 |80.41 |1.16 |3.01E+08 |5.44E+04 |0.0143 73.23 77.43 |18.71 |46.23 |28.79 |710.82 |103.80 |132.91 348.04 393.50 |80.17 |1.15 |3.00E+08 |5.43E+04 |0.0143 73.24 77.42 |18.70 |46.49 |28.73 |712.04 |104.14 |132.65 349.57 395.45 |80.50 |1.15 |2.98E+08 |5.43E+04 |0.0143 73.21 77.39 |18.56 |46.52 |28.70 |712.49 |104.55 |132.32 347.58 392.90 |79.94 |1.15 |2.98E+08 |5.43E+04 |0.0143 73.19 77.32 |18.50 |46.46 |28.59 |714.07 |104.65 |132.10 348.26 393.77 |80.04 |1.15 |2.97E+08 |5.43E+04 |0.0142 73.14 77.31 |18.54 |46.46 |28.60 |713.87 |104.69 |132.05 348.31 393.84 |80.06 |0.77 |2.97E+08 |5.43E+04 |0.0142 73.41 77.62 |18.69 |46.87 |28.97 |708.43 |104.42 |132.89 346.59 391.64 |79.89 |1.13 |2.99E+08 |5.44E+04 |0.0143 Red Data an average of all data points CO,/Argon Run 20: Heat Exchanger Composition -3.49 Argon,96.60 Carbon Dioxide Date -03 July 2008 Notebook Page -159 Front Page + Water Flow Rate -0.685 kg/min (0.0114167 kg/s) Pressure Gauge -860 psi Pressure Transducer -928 psi Gas Inlet Temperature -152°C (305.6 °F) 379 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwin(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out GasIn_|Coefficient |TransferMeter|Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (ib/hr)|(bar)(°C)(°C)(CC)|(kg/m3)|(°C)(kg/m3)|W/m2K (W/m2K)Nu Pr Gr Re Factor 51.44 63.88 |18.46 |41.98 |23.32 |744.69 |150.54 87.85 263.03 288.18 |56.03 |0.93 |L4IE+08 |3.90E+04 |0.0105 51.41 63.95 |18.47 |42.96 |23.41 |743.40 |151.06 87.80 262.65 287.73 |55.98 |0.93 |1.40E+08 |3.89E+04 |0.0105 51.39 64.01 |18.54 |43.37 |23.53 |741.44 |151.61 87.72 261.67 286.56 |55.80 |0.93 |1.39E+08 |3.89E+04 |0.0105 51.38 64.04 |18.62 |43.57 |23.59 |740.36 |152.06 87.64 261.51 286.36 |55.79 |0.93 |1.39E+08 |3.89E+04 |0.0105 51.35 64.06 |18.68 |43.64 |23.65 |739.43 |152.28 87.61 261.26 286.07 |55.76 |0.93 |1.39E+08 |3.88E+04 |0.0105 51.33 64.08 |18.73 |43.69 |23.69 |738.68 |152.47 87.57 260.94 285.68 |55.71 |0.93 |1.39E+08 |3.88E+04 |0.0105 51.30 64.09 |18.77 |43.71 |23.74 |737.78 |152.45 87.59 260.46 285.11 |55.63 |0.93 |1.39E+08 |3.88E+04 |0.0105 51.29 64.13 |18.90 |43.79 |23.85 |735.66 |152.67 87.59 260.23 284.83 |55.64 |0.93 |1.38E+08 |3.88E+04 |0.0105 51.30 64.12 |18.79 |43.84 |23.84 |735.82 |152.68 87.58 258.85 283.18 |55.31 |0.93 |1.38E+08 |3.88E+04 |0.0105 51.34 64.04 |18.53 |43.72 |23.69 |738.34 |152.91 87.39 257.82 281.94 |54.97 |0.93 |1.38E+08 |3.88E+04 |0.0104 51.37 63.95 |18.33 |43.68 |23.55 |740.62 |153.08 87.20 257.35 281.39 |54.78 |0.93 |1.38E+08 |3.88E+04 |0.0104 51.32 63.90 |18.37 |43.48 |23.46 |742.07 |152.83 87.20 259.10 283.48 |55.14 |0.93 |1.38E+08 |3.88E+04 |0.0104 51.33 63.83 |18.31 |42.72 |23.40 |742.95 |152.82 87.11 258.13 282.31 |54.88 |0.93 |1.39E+08 |3.88E+04 |0.0104 51.34 63.79 |18.35 |42.36 |23.33 |744.14 |152.78 87.06 259,52 283.98 |55.16 |0.93 |1.39E+08 |3.89E+04 |0.0104 51.32 63.80 |18.46 |42.33 |23.35 |743.68 |152.87 87.05 260.33 284.94 |55.36 |0.93 |1.39E+08 |3.88E+04 |0.0104 380 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas Side Mass Transfer Heat Flow Water |Water |Gas Gas Out Gas In Coefficient |Transfer Meter |Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (lb/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|(°C)(kg/m3)|W/m2K (W/m2K)Nu Pr Gr Re Factor 51.30 63.82 |18.53 |42.31 |23.42 |742.47 |152.84 87,08 260.07 284.64 |55.35 |0.93 |1.39E+08 |3.88F+04 |0.0104 Red Data an average of all data points CO,/Argon Run 21: Heat Exchanger Composition -3.49 Argon,96.60 Carbon Dioxide Date -03 July 2008 Notebook Page -159 Front Page - Water Flow Rate -0.685 kg/min (0.0114167 kg/s) Pressure Gauge -845 psi Pressure Transducer -915 psi Gas Inlet Temperature -120°C (248 °F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out Gas In Coefficient |TransferMeter|Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (lb/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|(CC)(kg/m3)|W/m2K (W/m2K)Nu Pr Gr Re Factor 50.08 63.09 |18.39 |37.88 |22.74 |751.53 |121.21 96.45 289.11 319.79 |62.96 |0.99 |1.57E+08 |3.90E+04 |0.0113 381 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out Gas In Coefficient |TransferMeter|Pressure |In Out Out |Density |GasIn |Density |(U)Coefficient Friction (Ib/hr)|(bar)(°C)(°C)(°C){|(kg/m3)|(°C)(kg/m3)|W/m2K (W/m2K)Nu Pr Gr Re Factor 50.11 63.05 |18.35 |38.11 |22.69 |752.14 |123.07 95.67 287.69 318.05 |62.52 |0.99 |1.56E+08 |3.90E+04 |0.0113 50.05 63.06 |18.43 |37.76 |22.66 |752.68 |121.35 96.36 290.95 322.04 |63.34 |0.99 |1.57E+08 |3.90E+04 |0.0113 49.77 63.00 |18.50 |38.33 |22.78 |750.46 |122.11 95.96 288.52 319.07 |62.84 |0.99 |1.55E+08 |3.88E+04 |0.0113 50.00 63.14 |18.57 |38.37 |22.81 |750.45 |121.07 96.60 291.74 323.02 |63.65 |0.99 |1.56E+08 |3.90E+04 |0.0114 49.07 62.75 |18.62 |38.22 |22.85 |747.95 |119.97 96.34 287.44 317.75 |62.78 |1.01 |1.54E+08 |3.83E+04 |0.0114 49.14 62.75 |18.65 |36.60 |22.67 |751.27 |112.68 99.28 299.44 332.48 |65.79 |1.00 |1.61E+08 |3.86E+04 |0.0116 49.88 63.07 |18.66 |37.69 |22.78 |750.74 |117.75 97.77 296.73 329.15 |64.97 |0.99 |1.59E+08 |3.90E+04 |0.0115 49.79 63.05 |18.62 |37.97 |22.87 |749.06 |121.08 96.43 289.13 319,82 |63.09 |0.99 |1.56E+08 |3.88E+04 |0.0113 49.85 62.99 |18.49 |38.11 |22.80 |749.95 |122.62 95.74 286.91 317.10 |62.46 |0.99 |1.55E+08 |3.88E+04 |0.0113 49.90 63.03 |18.54 |37.80 |22.75 |751.03 |121.20 96.35 290.46 321.44 |63.31 |0.99 |1.57E+08 |3.89E+04 |0.0113 49.70 62.94 |18.61 |38.04 }22.82 |749.42 |122.35 95.76 288.11 318.57 |62.78 |0.99 |1.55E+08 |3.87E+04 |0.0113 49.91 63.07 |18.66 |37.99 |22.85 |749.49 |121.83 96.18 290.18 321.10 {63.30 |0.99 |1.56E+08 |3.89E+04 |0.0113 49.41 62.88 |18.66 |37.79 |22.86 |748.40 |121.26 96.06 287.28 317.56 |62.67 |0.99 |1.55E+08 |3.85E+04 |0.0113 49.83 63.03 |18.67 |37.63 |22.85 |749.31 |120.79 96.52 290.41 321.38 |63.40 |0.99 |1.57E+08 |3.88E+04 |0.0113 49.48 62.79 |18.51 |36.94 |22.79 |749.29 |121.15 95.95 284.53 314.20 |61.97 |0.99 |1.56E+08 |3.86E+04 |0.0113 49.74 62.86 |18.50 |36.65 |22.75 |750.21 |119.65 96.66 287.85 318.26 |62.78 |0.77 |1.58E+08 |3.88E+04 |0.0114 49.75 62.97 |18.55 |37.76 |22.78 |750.20 |120.65 96.48 289.79 320.63 |63.21 |0.98 |1.56F+08 |3.88E+04 {|0.0113 Red Data an average of all data points CO,/Argon Run 22: Heat Exchanger Composition -3.49 Argon,96.60 Carbon Dioxide Date -07 July 2008 Notebook Page -158 Front Page - Water Flow Rate -0.793 kg/min (0.013217 kg/s) 382 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 ||--SS =ES |eS _.= Pressure Gauge -400 psi Pressure Transducer -421 psi Gas Inlet Temperature -200°C (392 °F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwin(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass_|Pressure |Water }Water |Gas Gas Out |GasIn |GasIn |Total Heat j|Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(@C)Density |Transfer Heat Factor Meter (°C)(°C)(CC)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(VU)Coefficient W/m2K (W/m2K) 15.12 28.97 |18.68 |26.33 |20.32 63.19 |198.55 15.24 40.43 40.98 |17.81 |0.79 1.17E-08 |1.15E+04 |0.0053 15.11 29.05 |18.63 |26.18 |20.31 63.41 |195.99 15.24 40.10 40.65 |17.73 |0.79 1.17E-08 |1.15E+04 |0.0053 15.19 29.13 |18.39 |26.18 |20.26 63.66 |197.39 15.24 39.53 40.05 |17.43 |0.79 1.22E-08 |1.16E+04 |0.0053 15.28 29.09 |18.49 |26.28 |20.40 63.48 |201.70 15.25 39.75 40.28 |17.41 |0.79 1.24E-08 |1.16E+04 |0.0053 15.18 29.04 |18.71 |26.41 |20.76 63.19 |202.39 15.26 38.86 39.37 |17.00 |0.79 1.31E-08 |1.15E+04 |0.0053 15.14 29.08 |18.49 |26.33 |20.67 63.36 |200.11 15.26 38.17 38.66 |16.75 |0.79 1.34E-08 |1.15E+04 |0.0053 15.18 29.15 |18.48 |25.97 |20.52 63.60 |200.27 15.26 38.82 39.33 |17.03 |0.79 1.30E-08 |1.15E+04 |0.0053 15.27 29.07 |18.51 |26.00 |20.44 63.42 |203.01 15.25 39.60 40.13 |17.31 |0.79 1.26E-08 |1.16E+04 |0.0053 15.17 28.98 |18.37 |25.83 |20.39 63.19 |202.20 15.25 38.88 39,38 |17.02 |0.79 1.31E-08 |1.15E+04 |0.0053 15.13 29.04 |18.40 |25.64 |20.29 63.40 |199.55 15.24 39.25 39.77 |17.25 |0.79 1.26E-08 |1.15SE+04 |0.0053 15.18 29.13 |18.50 |25.78 |20.26 63.65 |199.97 15.24 40.06 40.60 |17.60 |0.79 1.21E-08 |1.15E+04 |0.0053 383 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass_|Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(VU)Coefficient W/m2K (W/m2K) 15.25 29.06 |18.57 |26.02 |20.29 63.46 |202.58 15.24 40.56 41.12 |17.75 |0.79 1.20E-08 |1.16E+04 |0.0053 15.17 29.05 |18.59 |25.98 |20.33 63.40 |202.66 15.25 40.21 40.76 |17.59 |0.79 1.22E-08 |1.15E+04 |0.0053 15.17 29.12 |18.51 |25.96 |20.35 63.59 |202.04 15.25 39.76 40.29 |17.41 |0.79 1.25E-08 }1.15E+04 }0.0053 15.25 29.10 |18.55 |26.38 |20.37 63.52 |203.84 15.25 40.20 40.74 |17.55 |0.79 1.23E-08 |1.15E+04 |0.0053 15.19 29.01 |18.67 |26.44 |20.42 63.25 |203.80 15.25 40.30 40.84 |17.60 |0.79 1.22E-08 |1.15E+04 |0.0053 15.13 29.06 |18.71 |26.41 |20.48 63.38 |201.68 15.25 39.96 40.50 |17.51 |0.79 1.23E-08 |1.1SE+04 |0.0053 15.15 29.12 |18.73 |26.45 |20.50 63.52 |201.34 15.25 40.01 40.55 |17.53 |0.79 1.22E-08 |1.15E+04 |0.0053 15.18 29.07 |18.56 |26.14 |20.41 63.43 |201.06 15.25 39.69 40.22 |17.40 |0.79 1.24E-08 |1.1SE+04 |0.0053 Red Data an average of all data points CO 2/Argon Run 23: Heat Exchanger Composition -3.49 Argon,96.60 Carbon Dioxide Date -07 July 2008 Notebook Page -158 Front Page - Water Flow Rate -0.793 kg/min (0.013217 kg/s) Pressure Gauge -370 psi Pressure Transducer -405 psi Gas Inlet Temperature -120°C (248 °F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 384 |Geel «=Eee a Een |--}aS Ee Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater-0.000282474 Total Volume of System -0.00334 m2 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient }Transfer(lb/hr)(VU)Coefficient W/m2K (W/m2K) 14,92 29.57 |18.58 |22.99 |20.16 64.91 |125.65 15.26 36.30 36.74 |18.03 |0.83 |8.39E-09 |1.24E+04 |0.0062 14.66 29.31 |18.37 |22.90 |20.10 64.20 |128.32 15.24 35.03 35.44 |17.33 |0.83 |9.23E-09 |1.21E+04 |0.0061 14.29 29.01 |18.39 |22.55 |20.00 63.43 |126.28 15.23 34.47 34.87 |17.14 |0.83 |9.31E-09 |1.19E+04 |0.0061 13.95 28.81 |18.46 |22.29 |20.00 62.89 |120.91 15.22 33.59 33.97 |16.87 |0.83 |9.27E-09 |1.17E+04 |0.0062 14.10 28.96 |18.48 |22.23 |20.02 63.28 |116.88 15.23 33.71 34.09 |17.05 |0.84 |8.85E-09 |1.19E+04 |0.0063 14.43 29.07 |18.48 |22.47 |20.01 63.59 |118.68 15.23 34.72 35.13 |17.50 |0.83 |8.50E-09 |1.21E+04 |0.0062 14.47 28.91 |18.50 |22.72 |20.01 63.16 |124.42 15.23 35.32 35.74 |17.63 |0.83 |8.66E-09 |1.21E+04 |0.0061 14.21 28.67 |18.40 |22.82 |20.00 62.49 |127.03 15.22 34.31 34.71 |17.06 |0.83 |9.38E-09 |1.18E+04 |0.0061 13.86 28.38 |18.29 |22.59 |19.95 61.74 |125.09 15.20 33.01 33.37 |16.48 |0.83 |9.92E-09 |1.15E+04 |0.0061 13.73 28.37 |18.37 |22.34 |19.92 61.73 |120.72 15.20 32.92 33.29 |16.57 |0.83 |9.54E-09 |1.15E+04 |0.0061 13.98 28.52 |18.43 |22.48 |19.94 62.13 |119.61 15.21 33.68 34.06 |16.98 |0.83 |9.02E-09 |1.17E+04 |0.0061 14.13 28.44 |18.45 |22.76 |19.96 61.89 |123.60 15.21 34.34 34.73 |17.19 |0.83 |9.00E-09 |1.18E+04 |0.0061 13.94 28.22 |18.43 |22.83 |19.98 61.29 |127.02 15.20 33.86 34.24 |16.86 |0.82 |9.54E-09 |1.16E+04 |0.0060 13.62 27.95 |18.18 |22.58 |19.96 60.58 |126.22 15.19 31.90 32.24 |15.92 |0.82 |1.07E-08 |1.13E+04 |0.0060 13.25 27.66 |18.07 |22.09 |19.82 59.86 |121.98 15.17 30.74 31.06 |15.47 |0.83 |1.10E-08 |1.11E+04 |0.0060 13.11 27.62 |18.11 |21.77 |19.75 59.77 |116.26 15.17 30.47 30.78 |15.50 |0.83 |1.05E-08 |1.11E+04 |0.0061 13.36 27.80 |18.20 |21.85 |19.78 60.25 |113.93 15.18 31.27 31.60 |15.97 |0.83 |9.77E-09 |1.13E+04 |0.0061 13.65 27.98 |18.25 |22.12 |19.82 60.70 |115.77 15.18 32.20 32.55 |16.38 |0.83 |9.41E-09 |1.1SE+04 |0.0061 385 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass_|Pressure |Water |Water |Gas Gas Out |GasIn |GasIn }Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer (Ib/hr)(U)Coefficient W/m2K (W/m2K) 13.98 28.51 |18.36 |22.47 |19.95 62.10 |122.13 15.21 33.44 33.81 |16.77 |0.83 |9.44E-09 |1.17E+04 |0.0061 Red Data an average of all data points CO/Argon Run 24: Heat Exchanger Composition -3.49 Argon,96.60 Carbon Dioxide Date -08 July 2008 Notebook Page -158 Front Page - Water Flow Rate -0.633 kg/min (0.01055 kg/s) Pressure Gauge -235 psi Pressure Transducer -242 psi Gas Inlet Temperature -170°C (338 °F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwin(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 386 |aS es mS SS fe SS =_ Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu |Pr Gr Re Friction Flow |(bar)In Out Out Density |(CC)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(U)Coefficient W/m2K (W/m2K) 7.01 16.65 }18.93 |23.14 |21.30 32.97 |172.73 14.96 15.43 15.51 |7.29 |0.77 5.81E-08 |5.55E+03 |20.8405 6.98 16.70 |18.89 |22.99 |21.24 33.08 |171.27 14.96 15.34 15.42 |7.27 |0.77 5.82E-08 |5.53E+03 |20.6938 7.00 16.73 |18.84 |22.94 |21.29 33.15 |170.92 14.96 15.22 15.30 |7.21 |0.77 5.91E-08 |5.55E+03 |20.7929 7.10 16.69 |18.73 |22.83 |21.29 33.07 |172.32 14.96 15.32 15.39 |7.24 |0.77 5.90E-08 |5.62E+03 |21.3055 7.13 16.63 |18.72 |22.76 |21.20 32.94 |173.83 14.95 15.53 15.61 |7.32 |0.77 5.80E-08 |5.64E+03 |21.4799 7.07 16.63 |18.54 |22.70 |21.15 32.94 |174.08 14.95 15.22 15.30 |7.17 |0.77 6.06E-08 |5.58E+03 |21.1302 7.01 16.66 |18.45 |22.48 |21.10 33.03 |173.12 14.95 15.00 15.07 |7.08 |0.77 6.21E-08 |5.54E+03 |20.8188 6.99 16.71 |18.46 |22.57 |21.03 33.15 |172.24 14.95 15.06 15.14 |7.12 |0.77 6.11E-08 |5.53E+03 |20.7265 7.07 16.71 |18.62 |22.85 |20.98 33.15 |172.69 14.94 15.57 15.65 |7.36 }0.77 5.72E-08 |5.59E+03 |21.1287 7.13 16.66 |18.83 |23.09 |21.04 33.02 |174.16 14.94 15.97 16.06 |7.53 |0.77 5.48E-08 |5.63E+03 |21.4412 7.12 16.60 |18.91 |23.28 |21.11 32.89 |174.71 14.95 15.99 16.08 |7.53 |0.77 5.48E-08 |5.62E+03 |21.3919 7.01 16.62 |18.97 |23.24 |21.17 32.92 |173.70 14.95 15.71 15.80 |7.41 |0.77 5.63E-08 |5.54E+03 |20.8381 6.97 16.66 |18.88 |23.28 |21.18 33.01 |171.47 14.95 15.42 15.50 |7.30 |0.77 5.75E-08 |5.52E+03 |20.6158 6.97 16.71 |18.89 |23.21 |21.16 33.12 |170.67 14.95 15.45 15.53 |7.33 |0.77 5.70E-08 |5.53E+03 |20.6473 7.05 16.71 |18.93 |23.26 |21.17 33.12 |171.21 14.95 15.69 15.78 |7.44 |0.77 5.54E-08 |5.59E+03 |21.0605 7.12 16.66 |18.91 |23.41 |21.17 33.01 |172.61 14.95 15.86 15.94 |7.50 |0.77 5.48E-08 |5.63E+03 |21.3995 711 16.59 |18.80 |23.40 |21.18 32.85 |173.34 14.95 15.68 15.76 |7.40 |0.77 5.64E-08 |5.62E+03 |21.3780 7.09 16.54 |18.78 |23.33 |21.19 32.74 |173.06 14.95 15.56 15.64 |7.35 |0.77 5.72E-08 |5.60E+03 |21.2267 7.05 16.66 |18.78 |23.04 |21.16 33.01 |172.67 14.95 15.50 15.58 |7.33 |0.77 5.77E-08 |5.58E+03 |21.0509 Red Data an average of all data points 387 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO,/Argon Run 25: Heat Exchanger Composition -3.49 Argon,96.60 Carbon Dioxide Date -08 July 2008 Notebook Page -158 Front Page - Water Flow Rate -0.633 kg/min (0.01055 kg/s) Pressure Gauge -225 psi Pressure Transducer -232 psi Gas Inlet Temperature -120°C (248 °F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(U)Coefficient W/m2K (W/m2K) 6.50 16.07 |18.92 |21.37 |21.05 31.73 |119.66 14.93 13.05 13.10 |6.81 0.79 |4.90E-08 |5.51E+03 |18.2759 6.52 16.03 |18.84 |21.43 |21.06 31.64 |119.91 14.93 12.96 13.01 |6.76 0.79 |4.98E-08 |5.52E+03 |18.3577 6.50 15.97 |18.65 |21.31 |21.05 31.51 |119.93 14.93 12.64 12.70 |6.60 0.79 |5.25E-08 |5.51E+03 |18.2473 .6.43 15.97 |18.69 |21.13 |20.99 31.52 |119.12 14.93 12.62 12.67 |6.60 0.79 |5.22E-08 |5.46E+03 |17.9288 6.42 16.05 |18.75 |21.14 |21.01 31.69 |118.12 14.93 12.63 12.68 |6.61 0.79 |5.16E-08 |5.45E+03 |17.8702 388 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 |a fa Ea fn |e -|a = Mass_|Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu_|Pr Gr Re Friction Flow |(bar)In Out Out Density |(@C)Density |Transfer Heat Factor Meter (°C)(°C)(CC)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(U)Coefficient W/m2K (W/m2K) 6.48 16.03 |18.81 }21.21 |20.99 31.66 |117.78 14.93 12.86 12.92 |6.74 |0.79 |4.94E-08 |5.51E+03 |18.1759 6.49 15.98 |18.87 |21.27 |21.01 31.55 |118.15 14.93 12.91 12.97 |6.76 |0.79 |4.91E-08 |5.51E+03 |18.1832 6.47 15.93 |18.91 |21.31 |21.03 31.43 |118.26 14.93 12.92 12.97 |6.77 |0.79 |4.91E-08 |5.49E+03 |18.0873 6.39 15.86 |18.94 |21.31 |21.06 31.29 |117.51 14.93 12.72 12.78 |6.67 |0.79 |5.01E-08 |5.43E+03 |17.6965 6.33 15.92 |18.81 |21.14 |21.06 31.40 |115.89 14.93 12.38 12.43 |6.51 |0.79 |5.22E-08 |5.39E+03 |17.4380 6.36 16.00 |18.44 |20.96 |21.00 31.60 |114.48 14.93 11.98 12.03 |6.32 |0.79 |5.51E-08 |5.43E+03 |17.5575 6.42 16.03 |18.39 |20.73 |20.90 31.68 |114.31 14.93 12.16 12.21 |6.42 |0.79 |5.35E-08 |5.49E+03 |17.8868 6.48 16.05 |18.48 |20.75 |20.83 31.72 |115.53 14.92 12.52 12.57 |6.59 |0.79 |5.11E-08 |5.53E+03 |18.1639 6.52 16.07 |18.47 |20.89 |20.85 31.76 |117.78 14.92 12.63 12.68 |6.62 |0.79 |5.16E-08 |5.54E+03 |18.3294 6.53 16.02 |18.39 |20.94 |20.90 31.65 |120.42 14,93 12.57 12.62 |6.55 |0.79 |5.37E-08 |5.53E+03 |18.3949 6.48 15.96 |18.65 |21.03 |21.27 31.47 |122.16 14.94 12.36 12.41 |6.42 |0.79 |5.66E-08 |5.47E+03 |18.1371 6.41 15.93 |18.87 |21.14 |21.34 31.38 |122.45 14.95 12.42 12.47 |6.45 |0.79 |5.60E-08 |5.41E+03 |17.8217 6.45 15.99 |18.70 |21.12 |21.02 31.57 |118.32 14.93 12.61 12.66 |6.60 |0.79 |5.19E-08 |5.48E+03 |18.0325 Red Data an average of all data points 389 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Heat Exchanger Data Components - Argon Carbon Dioxide GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 2.27454 2.2735 2.27104 2.27458 2.273415 Carbon Dioxide 88.64024 88.59888 88.46479 88.60449 88.5771 Argon 7.30144 7.29846 7.30024 7.29149 7.2979075 GC Run 17: Agilent Cerity QA/QC Report Sample name:0624-HeatXGRArC0010 Sample note: Submission time:Tuesday,June 24,2008 9:16:21 AM Operator: Injection date:Tuesday,June 24,2008 9:41:12 AM GC Description:Mlcro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:June11Calibration2 Method last saved:Monday,June 23,2008 2:58:47 PM 390 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 EDTA a)...7 1 S84....hed Joo 7 t poe |bo "Sy -T-So oO 0.6 4 15 2 25 min TCD2A 27 'ns rn ania 8 wl aan a eee oe°°T T T T 41 415 2 25 min TCD3A >Is Aen mo BS 42| acre :og |' ae :Qo .r H ': 8 a T T TF --T T r 05 4 416 2 25 min ESTD Report Calibration last saved:Monday,June 23,2008 2:58:46 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 391 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount [mass%]Name 1 1.498 ---Oxygen 1 1.658 ---Nitrogen 2 0.292 BP =1.8106e+005 1.25431e-005 2.27104 Oxygen/Nitrogen 2 0.326 VB 2.0177e+006 4.38439e-005 88.46479 Carbon Dioxide 2 1.480 ---Sulfur Dioxide 3 1.405 BB 4.4682e+004 1.63381e-004 7.30024 Argon/Oxygen 3 2.554 ---Nitrogen_2 Total amount =98.03607 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 18: Agilent Cerity QA/QC Report Sample name:0624-HeatXGRArCOO11 Sample note: Submission time:Tuesday,June 24,2008 9:45:50 AM Operator: Injection date:Tuesday,June 24,2008 9:46:13 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:June11Calibration2 Method last saved:Monday,June 23,2008 2:58:47 PM 392 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 nmelUGeelC ElC LrlCU iG |lC rlCUCUrihlCCG |-| TCD1A >.oy ; +]...nn :[=]::i :'a en ee i a 7 od.in . 2 25 min 24 -fre -note -- || 5 :i :i |: oS '::;re4o;; d O..-1 i :j : +:;i o |i2°|an ;QO ee en woe :os.' bee .-oD r T T -r T r T T 05 4 15 2 25 min TCDSA >4 eee ti ee 0 i : q.4 °:r i : 8 +i b a T -T *T T T0.6 4 15 2 25 min ESTD Report Calibration last saved:Monday,June 23,2008 2:58:46 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 393 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[mass%]Name 1 1.498 ---Oxygen 1 1.658 ---Nitrogen 2 0.292 BP =1.8125e+005 1.25431e-005 2.27350 Oxygen/Nitrogen 2 0.326 VB 2.0208e+006 4.38439e-005 88.59888 Carbon Dioxide 2 1.480 ---Sulfur Dioxide 3 1.405 PB 4.4671e+004 1.63381e-004 7.29846 Argon/Oxygen 3 2.554 ---Nitrogen_2 Total amount =98.17083 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 19: Agilent Cerity QA/QC Report Sample name:0624-HeatXGRArCO012 Sample note: Submission time:Tuesday,June 24,2008 9:45:51 AM Operator: Injection date:Tuesday,June 24,2008 9:49:47 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:June11Calibration2 Method last saved:Monday,June 23,2008 2:58:47 PM 394 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 _OlU””lUlCM COC Ge sé a Le SS SS SS fs TCDI1A >.:{:i . ae Cn Lede hee z beds ceed . =.ek cee eeh eed eens we -_-_-oanrsVshoor|oot tot ; a wp :pon bond -fn |a Vo -Re ae ++. 4 :te 2 a.i z eee ;beh tt o7--7 _creed -anne 4 - r r r T r r v T Tr Tv Tv T T uy vr ¥T v 05 4 15 2 25 min TCD2A i :!: 1 :5 i :i i ||| f-:4 + | q LJ qT "UJ 4 14 2 25 min TCD3A ih bo *naee,wv .i i 2 iaQ i c i +:a =1 i bad iaam im i:@ | }r T T T T4115225 mir ESTD Report Calibration last saved:Monday,June 23,2008 2:58:46 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 395 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount [mass%]Name 1 1.498 ---Oxygen 1 1.658 ---Nitrogen 2 0.292 BP =1.8134e+005 1.25431e-005 2.27454 Oxygen/Nitrogen 2 0.326 VB =_.2.0217e+006 4.38439e-005 88.64024 Carbon Dioxide 2 1.480 ---Sulfur Dioxide 3 1.405 PB 4.4690e+004 1.63381e-004 7.30144 Argon/Oxygen 3 2.554 ---Nitrogen_2 Total amount =98.21622 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 20: Agilent Cerity QA/QC Report Sample name:0624-HeatXGRArCOO9 Sample note: Submission time:Tuesday,June 24,2008 9:16:20 AM Operator: Injection date:Tuesday,June 24,2008 9:37:39 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:June11Calibration2 Method last saved:Monday,June 23,2008 2:58:47 PM 396 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >cen -|7 =ro 1.:= 8 J 1.a accra feos wo '}j i . ;beep -f.eke Le. be o.t gee uh 4 ay i Bo "I |Po .pot |" o--Pome armen nope 7 i Trent Lie boo..iz ;4 yr T ¥-T T T r 0.6 4 16 2 25 min TCD2ZA 27 ; °::Qo 4H@-_- ory ---- 4 15 2 25 min TCDSA a 15 -i a |A oy a:ec |:i 4 '--o.'| :>. . Qo | °=oO TI o --ct |a =Oo a ro :eeNTT+T v T T r T r T T T T v T __.5 A 45 _2 25.min ESTD Report Calibration last saved:Monday,June 23,2008 2:58:46 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 397 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[!iV*s]Amt/(Area Amount [mass%]Name 1 1.498 ---Oxygen 1 1.658 ---Nitrogen 2 0.292 BP =1.8134e+005 1.25431e-005 2.27458 Oxygen/Nitrogen 2 0.326 VB =2.0209e+006 4.38439e-005 88.60449 Carbon Dioxide 2 1.480 ---Sulfur Dioxide 3 1.405 BB 4.4629e+004 1.63381e-004 7.29149 Argon/Oxygen 3 2.554 ---Nitrogen_2 Total amount =98.17056 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated CO2/Argon Run 26: Heat Exchanger Composition -7.30 Argon,88.58 Carbon Dioxide,2.27 Air Date -19 June 2008 Notebook Page -161 Front Page - Water Flow Rate -0.652 kg/min (0.0108667 kg/s) Pressure Gauge -860 psi Pressure Transducer -928 psi Gas Inlet Temperature -160°C (320°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 398 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Total Heat |Gas Side Mass Transfer Heat Flow Water |Water |Gas Gas Out Gas In Coefficient |Transfer Meter |Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (lb/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|(CC)(kg/m3)|W/m2K (W/m2K)Nu Pr Gr Re Factor 49.20 64.97 |17.61 |47.96 |22.14 |768.48 |163.23 85.85 260.44 285.09 |53.92 |0.92 |1.36E+08 |3.68E+04 |0.0105 49.13 64.95 |17.66 |48.05 |22.18 |767.80 |163.52 85.74 259.95 284.49 |53.84 |0.92 |1.35E+08 |3.68E+04 |0.0105 49.10 64.85 |17.65 |47.24 |22.08 |768.94 |164.37 85.37 259.40 283.83 |53.63 |0.92 |1.35E+08 |3.67E+04 |0.0104 49.05 64.77 |17.56 |47.03 |21.98 |770.13 |165.34 84.99 258.51 282.77 |53.34 |0.92 |1.35E+08 |3.67E+04 |0.0104 49.00 64.70 |17.54 |46.85 |21.94 |770.48 |166.11 84.68 257.77 281.89 |53.13 |0.91 |1.34E+08 |3.66E+04 |0.0104 48.93 64.65 |17.58 |47.10 |21.95 |770.19 |166.68 84.47 257.97 282.12 |53.17 |0.91 |1.33E+08 |3.65E+04 |0.0104 48.83 64.61 |17.62 |46.95 |21.97 |769.76 |167.07 84.31 257.17 281.17 |53.00 |0.91 |1.33E+08 |3.65E+04 |0.0103 48.75 64.56 |17.65 |47.12 |21.97 |769.60 |167.48 84.13 257.14 281.13 |52.99 |0.91 |1.32E+08 |3.64E+04 |0.0103 48.66 64.52 |17.66 |47.15 |22.00 |769.01 |167.99 83.94 255.94 279.69 |52.73 |0.91 |1.32E+08 |3.63E+04 |0.0103 48.61 64.44 |17.55 |47.12 |21.97 |769.19 |168.17 83.78 254.27 277.71 |52.34 |0.91 |1.31E+08 |3.63E+04 |0.0103 48.54 64.33 |17.39 |47.35 |21.86 |770.41 |168.20 83.63 253.86 277.21 |52.19 |0.91 |1.31E+08 |3.62E+04 |0.0103 48.41 64.31 |17.47 |48.17 |21.92 |769.39 |168.38 83.55 254,30 277.74 |52.33 |0.91 |1.30E+08 |3.61E+04 |0.0103 48.33 64.27 |17.56 |48.31 |21.98 |768.37 |168.45 83.47 254,38 277.84 |52.40 |0.91 |1.29E+08 |3.61E+04 |0.0103 48.23 64.22 |17.61 |48.11 |22.02 |767.69 |168.45 83.41 253.67 276.99 |52.27 |0.91 |1.29E+08 |3.60E+04 |0.0103 48.12 64.17 |17.64 |48.18 |22.02 |767.46 |168.65 83.28 253.34 276.60 |52.20 |0.91 |1.29E+08 |3.59E+04 |0.0103 48.03 64.11 |17.68 |48.35 |22.04 |766.90 |168.77 83.17 253.20 276.42 |52.19 |0.91 |1.28E+08 |3.58E+04 |0.0102 47.93 64.06 |17.72 |48.06 |22.05 |766.56 |168.67 83.11 252.79 275.93 |52.12 |0.91 {1.28E+08 |3.58E+04 |0.0102 47.85 64.00 |17.75 |48.10 |22.07 |766.09 |168.72 83.02 252.59 275.70 |52.10 |0.91 |1.27E+08 |3.57E+04 |0.0102 47.79 63.95 |17.66 |47.97 |22.09 |765.53 |168.25 83.07 250.60 273.33 |51.69 |0.91 |1.28E+08 |3.57E+04 |0.0102 47.73 63.92 |17.58 |48.09 |22.01 |766.67 |167.94 83.11 250.97 273.78 |51.73 |0.91 |1.28E+08 |3.57E+04 |0.0102 399 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out GasIn_|Coefficient |TransferMeter|Pressure |In Out Out |Density |GasIn |Density |(U)Coefficient Friction (tb/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|CC)(kg/m3)|W/m2K (W/m2K)Nu Pr Gr Re Factor 48.51 64.42 {17.61 |47.66 |22.01 |768.43 |167.22 |84.00 255.41 279.07 |52.67 {0.91 |1.31E+08 |3.62E+04 |0.0103RedDataanaverageofalldatapoints 400 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO./Argon Run 27: Heat Exchanger Composition -7.30 Argon,88.58 Carbon Dioxide,2.27 Air Date -19 June 2008 Notebook Page -161 Front Page - Water Flow Rate -0.652 kg/min (0.0108667 kg/s) Pressure Gauge -860 psi Pressure Transducer -928 psi Gas Inlet Temperature -122°C (251.6 °F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwin(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Total Heat |Gas Side Mass Transfer Heat Flow Water |Water |Gas Gas Out Gas In Coefficient |Transfer Meter |Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (Ib/hr)|}(bar)(°C)(°C)(°C)|(kg/m3)|(°C)(kg/m3)|W/m2K (W/m2K)Nu Pr Gr Re Factor 44.37 61.87 |18.03 |}37.86 |21.41 |768.43 |123.30 93.56 277.22 305.31 |59.20 |0.98 |1.48E+08 |3.47E+04 |0.0114 43.84 61.58 |17.97 |37.44 |21.31 |768.92 |122.67 93.30 275.09 302.72 |58.70 |0.98 |1.47E+08 |3.43E+04 |0.0114 44.27 61.75 |17.95 |37.53 |21.25 |770.43 |121.74 93.93 280.32 309.08 |59.87 |0.99 |1.49E+08 |3.47E+04 |0.0114 43.52 61.38 |17.94 |37.25 |21.21 |769.62 |121.27 93.46 276.35 304.25 |59.01 |0.98 |1.46E+08 |3.41E+04 |0.0114 44.01 61.63 |17.99 |36.87 |21.22 |770.46 |118.73 94.84 282.90 312.21 |60.59 |0.99 |1.50E+08 |3.45E+04 |0.0115 43.60 61.44 |18.06 |37.38 |21.37 |767.33 |121.82 93.36 274.63 302.17 |58.71 |0.98 |1.46E+08 |3.41E+04 |0.0114 401 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out GasIn_|Coefficient |TransferMeter|Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (lb/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|(°C)(kg/m3)|W/m2K (W/m2K)Nu Pr Gr Re Factor 43.67 61.49 |17.99 |36.65 |21.35 |767.97 |117.86 94.94 277.88 306.10 |59.57 |0.99 |1.50E+08 |3.43E+04 |0.0115 43.96 61.64 |18.00 |38.45 |21.45 |766.87 |121.82 93.71 276.24 304.12 |59.10 |0.98 |1.46E+08 |3.44E+04 |0.0114 44.00 61.76 |18.11 |39.05 |21.61 |764.77 |122.79 93.56 274.85 302.44 |58.85 |0.98 |1.45E+08 |3.44E+04 |0.0114 43.28 61.42 |18.17 |39.10 |21.66 |762.70 |122.59 93.05 270.79 297.53 |58.02 |0.98 |1.43E+08 |3.39E+04 |0.0113 43.53 61.56 |18.19 |38.12 |21.59 |764.43 |117.91 95.04 278.92 307.37 |60.00 |0.99 |1.47E+08 |3.42E+04 |0.0115 43.64 61.55 |18.23 |38.74 |21.68 |762.89 |121.99 93.48 273.80 301.17 |58.74 |0.98 |1.44E+08 |3.42E+04 |0.0114 43.50 61.53 |18.15 |38.22 |21.69 |762.70 |119.88 94,23 272.62 299.74 |58.54 |0.99 |1.46E+08 |3.41E+04 |0.0114 43.82 61.60 |18.14 |38.73 |21.65 |763.53 |122.69 93.32 272.87 300.05 |58.46 |0.98 |1.44E+08 |3.43E+04 |0.0113 43.94 61.67 |18.15 |38.91 |21.65 |763.77 |124.65 92.73 271.53 298.42 |58.06 |0.98 |1.44E+08 |3.43E+04 |0.0113 44.06 61.73 {|18.10 |39.16 |21.70 |763.27 |126.05 92.34 269.00 295.37 |57.44 |0.97 |1.43E+08 |3.43E+04 |0.0112 43.81 61.60 |18.07 |38.09 |21.49 |766.13 |121.73 93.68 275,31 303.00 }58.93 |0.98 |1.46E+08 |3.43E+04 |0.0114 Red Data an average of all data points CO,/Argon Run 28: Heat Exchanger Composition -7.30 Argon,88.58 Carbon Dioxide,2.27 Air Date -20 June 2008 Notebook Page -160 Front Page - Water Flow Rate -0.680 kg/min (0.0113333 kg/s) Pressure Gauge -485 psi Pressure Transducer -516 psi Gas Inlet Temperature -200°C (392°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 402 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/mK) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Total Heat |Gas Side Mass Transfer Heat Flow Water |Water |Gas Gas Out Gas In Coefficient |Transfer Meter |Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (lb/hr)|(bar)(°C)(°C)|CC)|(kg/m3)|CC)(kg/m3)|W/m2K (W/m2K)|Nu Pr Gr Re Factor 19.69 35.64 |17.56 |29.01 |19.26 83.35 |203.49 40.86 55.65 56.69 |23.81 |0.80 |2.94E+07 |1.48E+04 |0.0062 19.64 35.48 |17.58 |28.99 |19.31 82.81 |204.13 40.61 55.26 56.29 |23.63 |0.80 |2.91E+07 |1.48E+04 |0.0061 19.53 35.48 |17.59 |28.66 |19.35 82.79 |200.20 41.00 54.47 55.48 |23.43 |0.80 |2.94E+07 |1.48E+04 |0.0062 19.57 35.59 |17.65 |28.69 |19.40 83.10 |198.87 41.26 54.59 55.60 |23.52 |0.80 |2.97E+07 |1.48E+04 |0.0062 19.64 35.57 |17.67 |28.93 |19.45 83.01 |200.68 41.06 54.74 55.75 |23.52 |0.80 |2.95E+07 |1.48E+04 |0.0062 19.64 35.62 |17.66 |29.10 |19.43 83.19 |202.38 40.95 54.89 55.90 |23.52 |0.80 |2.95E+07 |1.48E+04 |0.0062 19.66 35.58 |17.65 |29.19 |19.42 83.06 |204.25 40.72 55.09 56.11 |23.54 |0.80 |2.92E+07 |1.48E+04 |0.0061 19.62 35.60 |17.66 |29.17 |19.46 83.10 |204.43 40.72 54.76 55.78 |23.39 |0.80 |2.92E+07 |1.48E+04 |0.0062 19.66 35.57 |17.55 |29.24 |19.41 83.03 |205.34 40.60 54.57 55.57 |23.28 |0.80 |2.91E+07 |1.48E+04 |0.0061 19.54 35.44 |17.53 |28.91 |19.36 82.66 |204.36 40.55 54.30 55.30 |23.21 |0.80 |2.90E+07 |1.47E+04 |0.0061 19.54 35.51 |17.54 |28.20 |19.30 82.90 |201.23 40.93 54.43 55.43 |23.37 |0.80 |2.95E+07 |1.47E+04 |0.0062 19.64 35.54 |17.55 |28.30 |19.30 83.00 |202.19 40.87 54.91 55.93 |23.55 |0.80 |2.95E+07 |1.48E+04 |0.0062 19.56 35.36 |17.59 |28.32 |19.36 82.40 |202.65 40.61 54.45 55.45 |23.35 |0.80 |2.91E+07 }1.47E+04 |0.0061 19.46 35.38 |17.57 |28.02 |19.37 82.46 |198.78 41.02 53.81 54.79 |23.20 |0.80 |2.94E+07 |1.47E+04 |0.0062 19.52 35.48 |17.58 |28.03 |19.32 82.81 |197.94 41.22 54.31 55.31 |23.44 |0.80 |2.97E+07 |1.48E+04 |0.0062 19.60 35.55 |17.52 |28.29 |19.33 83.03 |200.66 41.04 54.31 55.30 |23.33 |0.80 |2.96E+07 |1.48E+04 |0.0062 403 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out Gas In Coefficient |TransferMeter|Pressure |In Out Out |Density |GasIn }Density |(U)Coefficient Friction (lb/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|(°C)(kg/m3)|W/m2K (W/m2K)Nu Pr Gr Re Factor 19.59 35.53 |17.59 |28.69 |19.36 82.92 |201.97 40.88 54.66 55.67 |23.44 |0.80 |2.94F+07 |1.48E+04 |0.0062 Red Data an average of all data points CO,/Argon Run 29: Heat Exchanger Composition -7.30 Argon,88.58 Carbon Dioxide,2.27 Air Date -20 June 2008 Notebook Page -160 Front Page - Water Flow Rate -0.680 kg/min (0.0113333 kg/s) Pressure Gauge -465 psi Pressure Transducer -478 psi Gas Inlet Temperature -120°C (248°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 404 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas Side Mass Transfer Heat Flow Water |Water |Gas Gas Out Gas In Coefficient |Transfer Meter |Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (lb/hr)|(bar)(eC)|(C)|CC)|(kg/m3)|CC)(kg/m3)|W/m2K (W/m2K)|Nu Pr Gr Re Factor 17.36 34.13 |17.25 |22.98 |18.82 78.88 |118.90 49.40 44.12 44.78 |21.77 |0.85 |3.21E+07 |1.45E+04 |0.0071 17.72 34.26 |17.16 |23.12 |18.79 79.31 |118.98 49.59 44.81 45.48 |22.09 |0.85 |3.24E+07 |1.48E+04 |0.0071 17.52 34.11 |17.21 |23.18 |18.79 78.82 |120.94 49.04 44.72 45.40 |21.99 |0.85 |3.20E+07 |1.46E+04 |0.0071 17.50 34.16 |17.26 |23.04 |18.76 79.00 |119.89 49.29 45.10 45.78 |22.21 |0.85 |3.22E+07 |1.46E+04 |0.0071 17.74 34.23 |17.20 |23.23 |18.77 79.22 |120.70 49.27 45.36 46.05 |22.30 |0.85 |3.23E+07 |1.48E+04 |0.0071 17.48 34.05 |17.17 |23.17 |18.72 78.68 |122.06 48.77 44.79 45.46 |21.99 |0.85 |3.19E+07 |1.45E+04 |0.0071 17.24 33.96 |17.22 |22.73 |18.72 78.40 |119.63 49.01 44,22 44.88 |21.81 |0.85 |3.18E+07 |1.44E+04 |0.0071 17.60 34.19 |17.28 |22.70 |18.75 79.10 |118.23 49.60 45.33 46.02 |22.39 |0.86 |3.24E+07 |1.47E+04 |0.0071 17.58 34.10 |17.24 |22.93 |18.81 78.80 |120.46 49.11 44.73 45.40 |22.01 |0.85 |3.21E+07 |1.46E+04 |0.0071 17.43 34.03 |17.12 |22.76 |18.77 78.60 |120.46 49.00 43.80 44.45 |21.56 |0.85 |3.20E+07 |1.45E+04 |0.0071 17.69 34.19 |17.09 |22.79 {18.73 79.12 |120.57 49,23 44.68 45.36 |21.98 |0.85 |3.24E+07 |1.47E+04 |0.0071 17,58 34.04 |16.98 |22.80 |18.66 78.68 |122.21 48.73 44.17 44.82 |21.68 |0.85 |3.20E+07 |1.46E+04 |0.0071 17.33 33.94 |17.03 |22.56 |18.65 78.38 |120.88 48.79 43.70 44.34 |21.50 |0.85 |3.18E+07 |1.44E+04 |0.0071 17.62 34.15 |17.14 |22.76 |18.70 79.00 |119.75 49.29 44.86 45.54 |22.10 |0.85 |3.23E+07 |1.47E+04 |0.0071 17.57 34.04 |17.22 |23.10 |18.73 78.66 |121.53 48.85 45.24 45.93 |22.23 |0.85 |3.19E+07 |1.46E+04 |0.0071 17.20 33.86 |17.28 |23.05 |18.79 78.04 |120.95 48.65 44.17 44.83 |21.75 |0.85 |3.14E+07 |1.43E+04 |0.0071 17.19 33.91 |17.30 |22.86 |18.80 78.22 |118.47 49.14 44.06 44.71 |21.78 |0.85 |3.16E+07 |1.44E+04 |0.0071 17.49 34.08 |17.19 |22.93 |18.75 78.76 |120.27 49.10 44.58 45.25 |21.95 |0.85 |3.20E+07 |1.46E+04 |0.0071 Red Data an average of all data points CO,./Argon Run 30: Heat Exchanger Composition -7.30 Argon,88.58 Carbon Dioxide,2.27 Air 405 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Date -23 June 2008 Notebook Page -160 Front Page - Water Flow Rate -0.514 kg/min (0.0085667 kg/s) Pressure Gauge -215 psi Pressure Transducer -226 psi Gas Inlet Temperature -170°C (338°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out GasIn |Coefficient |TransferMeter|Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (lb/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|(°C)(kg/m3)|W/m2K (W/m2K)Nu_|Pr Gr Re Factor 5.98 15.65 |18.43 |22.46 |20.37 30.93 |170.88 19.02 13.69 13.75 |6.51 |0.77 |4.91E+06 |4.75E+03 |0.0037 6.07 15.62 |18.50 |22.54 |20.42 30.85 |171.33 18.96 13.93 13.99 |6.62 |0.77 |4.88E+06 |4.82E+03 |0.0036 6.11 15.57 |18.58 |22.68 |20.46 30.73 |171.80 18.87 14.08 14.14 |6.68 |0.77 |4.84E+06 |4.85E+03 |0.0036 6.01 15.56 |18.64 |22.73 |20.60 30.70 |171.68 18.87 13.72 13.78 |6.51 |0.77 |4.83E+06 |4.77E+03 |0.0036 5.97 15.59 |18.68 |22.71 |20.64 30.76 |170.46 18.97 13.58 13.65 |6.46 |0.77 |4.85E+06 |4.74E+03 |0.0036 5.96 15.60 |18.72 |22.77 |20.65 30.77 |169.72 19.01 13.60 13.66 |6.48 |0.77 |4.86E+06 |4.74E+03 |0.0037 6.03 15.55 |18.66 |23.00 |20.72 30.65 |169.88 18.94 13.60 13.66 |6.48 |0.77 |4.82E+06 |4.79E+03 |0.0036 6.02 15.48 |18.66 |22.99 |20.70 30.49 |170.00 18.84 13.58 13.64 |6.47 |0.77 |4.77E+06 |4.78E+03 |0.0036 6.03 15.41 |18.50 |22.98 |20.71 30.34 |169.29 18.79 13.34 13.40 |6.36 |0.77 |4.73E+06 |4.80E+03 |0.0036 5.86 15.41 |18.43 |22.74 |}20.67 30.35 |167.08 18.89 12.88 12.94 |6.17 |0.77 |4.75E+06 |4.68E+03 |0.0036 406 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas Side Mass Transfer Heat Flow Water |Water |Gas Gas Out Gas In Coefficient |Transfer Meter |Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (lb/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|CC)(kg/m3)|W/m2K (W/m2K)Nu |Pr Gr Re Factor 5.77 15.45 |18.56 |22.57 |20.67 30.44 |164.37 19.07 12.79 12.84 |6.15 |0.77 |4.78E+06 |4.62E+03 |0.0037 5.73 15.49 |18.66 |22.57 |20.68 30.53 |162.62 19.21 _12.78 12.83 |6.16 |0.77 |4.82E+06 |4.60E+03 |0.0037 5.80 15.49 |18.60 |22.69 |20.68 30.54 |162.29 19.23 12.87 12.93 |6.21 |0.77 |4.82E+06 |4.66E+03 |0.0037 5.94 15.44 |18.42 |22.73 |20.70 30.42 |163.74 19.09 12.93 12.98 |6.23 |0.77 |4.78E+06 |4.76E+03 |0.0036 5.95 15.39 |18.40 |22.69 |20.67 30.32 |165.02 18.97 13.00 13.06 |6.25 |0.77 |4.75E+06 |4.76E+03 |0.0036 5.95 15.51 |18.56 |22.72 |20.62 30.59 |168.01 18.98 13.36 13.42 |6.38 |0.77 |4.81E+06 |4.74E+03 |0.0036 Red Data an average of all data points CO,./Argon Run 31: Heat Exchanger Composition -7.30 Argon,88.58 Carbon Dioxide,2.27 Air Date -23 June 2008 Notebook Page -160 Front Page - Water Flow Rate -0.514 kg/min (0.0085667 kg/s) Pressure Gauge -205 psi Pressure Transducer -212 psi Gas Inlet Temperature -123°C (254.4°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 407 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out GasIn_|Coefficient |TransferMeter|Pressure |In Out Out Density |Gas In |Density |(U)Coefficient Friction (lb/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|(°C)(kg/m3)|W/m2K (W/m2K)Nu_|Pr Gr Re Factor 5.41 14.72 |18.53 |21.46 |20.74 28.87 |120.36 20.38 10.73 10.77 |5.61 |0.79 |4.29E+06 |4.59E+03 |0.0038 5.49 14.67 |18.61 |21.56 |20.81 28.74 |123.17 20.15 10.97 11.01 |5.71 |0.78 |4.26E+06 |4.64E+03 |0.0038 5.39 14.61 |18.72 |21.66 |20.89 28.59 |124.71 19.97 10.84 10.87 |5.62 |0.78 |4.22E+06 |4.54E+03 |0.0038 5.27 14.57 |18.78 |21.69 |20.96 28.51 |124.86 19.9]10.59 10.63 |5.49 |0.78 |4.20E+06 |4.44E+03 }0.0038 5.26 14.63 |18.57 |21.69 |21.01 28.64 |123.81 20.06 10.26 10.30 |5.33 |0.78 |4.24E+06 |4.44E+03 |0.0038 5.26 14.69 |18.19 |21.54 |20.95 28.76 |122.79 20.19 9.92 9.95 |5.16 |0.78 |4.29E+06 |4.44E+03 |0.0038 5.31 14.66 |18.25 |21.27 |20.82 28.73 |122.73 20.17 10.19 10.23 |5.31 |0.78 |4.28E+06 |4.49E+03 |0.0038 5.51 14.62 |18.35 |21.27 |20.72 28.65 |123.49 20.07 10.80 10.84 |5.62 |0.78 |4.26E+06 |4.65E+03 |0.0037 5.45 14.57 |18.38 |21.38 |20.63 28.54 |124.19 19.94 10.84 10.88 |5.63 |0.78 |4.22E+06 |4.59E+03 |0.0037 5.35 14.57 |18.45 |21.42 |20.59 28.56 |124.14 19.96 10.78 10.82 |5.60 |0.78 |4.22E+06 |4.51E+03 |0.0038 5.30 14.64 |18.51 |21.44 |20.63 28.71 }123.90 20.07 10.71 10.75 |5.57 |0.78 |4.26E+06 |4.48E+03 |0.0038 5.36 14.64 |18.47 |21.47 |20.70 28.70 |123.92 20.07 10.70 10.74 }5.56 |0.78 |4.26E+06 |4.52E+03 |0.0038 5.37 14.60 |18.36 |21.45 |20.77 28.60 |124.72 19.96 10.52 10.56 |5.46 |0.78 |4.24E+06 |4.53E+03 |0.0038 5.47 14.54 |18.33 |21.39 |20.81 28.47 |125.66 19.83 10.66 10.70 |5.52 |0.78 |4.21E+06 |4.61E+03 |0.0037 5.43 14.50 |18.34 |21.35 |20.82 28.39 |126.02 19.76 10.58 10.62 {|5.48 |0.78 |4.19E+06 |4.57E+03 |0.0037 5.38 14.62 |18.46 |21.47 |20.79 28.63 |123.90 20.03 10.61 10.64 {5.51 |0.78 |4.24E+06 |4.54E+03 |0.0038 Red Data an average of all data points 408 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Heat Exchanger Data Components - Argon Carbon Dioxide GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 Carbon Dioxide 90.98335 90.84608 90.79584 90.76847 |90.848435 Argon 8.98998 8.98225 8.98398 8.98527 8.98537 GC Run 21: Agilent Cerity QA/QC Report Sample name:0716-HeatXGRArCO0O7 Sample note: Submission time:Thursday,July 17,2008 10:31:49 AM Operator: Injection date:Thursday,July 17,2008 10:45:31 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July16Cal3 Method last saved:Thursday,July 17,2008 10:08:54 AM 409 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA ESTD Report Calibration last saved:Thursday,July 17,2008 10:08:54 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 410 2 ) =':' 4 9 :@ ::rel Hl :i o-oan :itn rs sn T T TF T T 06 1 15 2 25 min TCD2A 27 Ig ee,_x ;- 2 i oo:.4 a ce :: : °i :'2 i i !"1 ::: u,'|:' o !||: oR i.i :- x |;8 4 iar 4 '-:rood%.i ::' ¥rT T T T r T ¥ 05 1 15 2 25 min TCDSA -\ i : T T T --t r ” _1 15 2 . 25 min Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount [mass%]Name 1 1.484 ---Oxygen 1 1.625 ---Nitrogen 2 0.276 BB 1.8591e+006 4.89390e-005 90.98335 Carbon Dioxide 2 1.241 ---Sulfur Dioxide 3 1.361 BB 6.1276e+004 1.46712e-004 8.98998 Argon/Oxygen Total amount =99.97333 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 22: Agilent Cerity QA/QC Report Sample name:0716-HeatXGRArCO08 Sample note: Submission time:Thursday,July 17,2008 10:31:50 AM Operator: Injection date:Thursday,July 17,2008 10:49:04 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July16Cal3 Method last saved:Thursday,July 17,2008 10:08:54 AM 411 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >4 !t=a i ::|| |L 4[=]'i j8Ja..7,-}f{i i:: o 4 b h H o c-.oo -r -T -r -oe -,r 7 05 4 15 2 25 min TCD2A 27 'g ee!! x .,--'i)hee Sees :1 a |$.ia imii: ..;irr)''a4 i"8 4 °:4@. :::--.v or -----T pare 05 1 15 2 25 min TCOZSA 24 =i ;:i |!|| |7 /lL | :|7 i :| : i 'i . o i."fe "+" Qo i 8 -i --"be . ra]:- :i A +t -$+-+----+-T a Sn + _41_AS vee A 2 iin ESTD Report Calibration last saved:Thursday,July 17,2008 10:08:54 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 412 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount [mass%]Name 1 1.484 ---Oxygen 1 1.625 ---Nitrogen 2 0.276 BB =1.8563e+006 4.89390e-005 90.84608 Carbon Dioxide 2 1.241 ---Sulfur Dioxide 3 1.362 BB 6.1224e+004 1.46712e-004 8.98225 Argon/Oxygen Total amount =99.82833 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 23: Agilent Cerity QA/QC Report Sample name:0716-HeatXGRArCOO9 Sample note: Submission time:Thursday,July 17,2008 10:31:50 AM Operator: Injection date:Thursday,July 17,2008 10:52:36 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July16Cal3 Method last saved:Thursday,July 17,2008 10:08:54 AM 413 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA a --,nr ne a - TCD2ZA 27 3 Oe,a Do,- 3 i g.| a |Q °o :eS eee =-are : _wee noe oe chet 05 '18 2 25 min TCOSA 24 - :8 L __ "i oe 068 aA 8B min ESTD Report Calibration last saved:Thursday,July 17,2008 10:08:54 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 414 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount [mass%]Name 1 1.484 ---Oxygen 1 1.625 ---Nitrogen 2 0.276 BB 1.8553e+006 4.89390e-005 90.79584 Carbon Dioxide 2 1.241 ---Sulfur Dioxide 3 1.361 BB 6.1235e+004 1.46712e-004 8.98398 Argon/Oxygen Total amount =99.77982 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 24: Agilent Cerity QA/QC Report Sample name:0716-HeatXGRArCO0010 Sample note: Submission time:Thursday,July 17,2008 10:31:52 AM Operator: Injection date:Thursday,July 17,2008 10:56:07 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July16Cal3 Method last saved:Thursday,July 17,2008 10:08:54 AM 415 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 ESTD Report Calibration last saved:Thursday,July 17,2008 10:08:54 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 416 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCD1A >!2 ;: Oo 4 2 e wi -1rs)i ' ey be -: T T tT T 06 4 15 2 25 min TCDZ2A a7 's a ee Fay i . ; : c ;: °4 4 "+2 ::: a }:oO.ie 4 ': ©:. hb.i i a a.i]o o i i . i : oO ch te tee ee be bee be te -sees vo neennr eek eee aeaoisit? :'T oo T T r 05 1 2 25 min >L.i t : i ; : ;oo, i i!:: T+v T T T 1 15 2 2 __min Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [!iV's]Amt/Area Amount [mass%]Name 1 1.484 ---Oxygen 1 1.625 ---Nitrogen 2 0.276 BB 1.8547e+006 4.89390e-005 90.76847 Carbon Dioxide 2 1.241 ---Sulfur Dioxide 3 1.361 BB 6.1244e+004 1.46712e-004 8.98527 Argon/Oxygen Total amount =99.75374 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated CO2/Argon Run 32: Heat Exchanger Composition -8.99 Argon,90.85 Carbon Dioxide Date -09 July 2008 Notebook Page -158 Front Page - Water Flow Rate -0.831 kg/min (0.01385 kg/s) Pressure Gauge -1240 psi Pressure Transducer - 1343 psi Gas Inlet Temperature -73°C (163.4°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 417 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out |Gas |GasIn_|Coefficient |TransferMeter|Pressure |In Out Out Density |In Density |(U)Coefficient Friction(lb/hr)|(bar)CC)|CC)|eC)|(kg/im3)|CC)_|(kg/m3)|W/m2K (W/m2K)|Nu Pr |Gr Re Factor 94.95 93.16 |18.09 |39.97 |30.45 |748.50 |72.62 |213.79 451.20 530.66 |101.72 |2.15 |1.23E+09 |5.82E+04 |0.0234 94.95 93.28 |18.16 |40.21 |30.52 |747.99 |73.15 |213.06 450.46 529.63 |101.62 |2.13 |1.21E+09 |5.83E+04 |0.0233 94.96 93.27 |18.20 |40.40 |30.51 |748.13 |73.51 |212.25 451.64 531.27 |101.97 |2.11 |1.19E+09 |5.85E+04 |0.0232 95.01 93.12 |18.24 |40.20 |30.48 |747.98 |73.43 |211.88 452.04 531.82 |102.12 |2.10 |1.19E+09 |5.86E+04 |0.0231 95.05 92.77 |18.11 |39.61 |30.23 |749.98 |73.10 |211.36 453.36 533.65 |102.31 |2.11 {1.20E+09 |5.87E+04 |0.0231 95.03 92.61 |18.00 |39.33 |30.10 |751.14 |72.73 |211.58 454.06 534.62 |102.36 |2.13 |1.21E+09 |5.87E+04 |0.0231 94.99 92.68 |18.02 |39.46 |30.13 |750.92 |73.01 |211.22 453.22 533.45 |102.19 |2.12 |1.20E+09 |5.87E+04 |0.0231 95.06 92.58 |17.91 |39.47 |30.10 |751.00 |73.16 |210.53 452.53 532.50 |102.04 |2.10 |1.19E+09 |5.89E+04 |0.0230 94,97 92.42 |17.86 |39.46 |29.91 |752.80 |73.06 |210.18 456.30 537.72 |102.88 |2.11 |1.19E+09 |5.89E+04 |0.0230 94.94 92.30 |17.64 }39.22 |29.91 |752.46 |72.75 |210.41 452.14 531.96 |101.80 |2.11 |1.21E+09 |5.88E+04 |0.0230 94.95 92.27 |17.52 |39.19 |29.93 |752.18 |72.85 |210.08 449.50 528.31 |101.16 |2.11 |1.20E+09 |5.89E+04 |0.0230 95.04 92.19 |17.44 |39.29 |29.77 |753.89 |73.01 |209.48 452.78 $32.84 |101.89 |2.10 |1.20E+09 |5.90E+04 |0.0229 94.69 92.50 |17.61 |40.04 |30.01 |751.94 |73.17 |210.22 452.89 $33.01 |102.07 |2.10 |1.18E+09 |5.87E+04 |0.0230 94.64 92.65 |17.76 |40.27 |30.19 |750.15 |73.39 |210.29 451.34 530.85 |101.83 |2.09 |1.17E+09 |5.87E+04 |0.0230 94.71 92.68 |17.75 |40.42 |30.24 |749.62 |73.77 |209.58 450.14 529.19 |101.61 |2.07 |1.15E+09 |5.88E+04 |0.0229 94.64 92.64 |17.76 |40.50 |30.18 |750.19 |73.97 |209.03 451.41 530.95 |101.93 |2.06 |1.14E+09 |5.89E+04 |}0.0228 94.50 92.60 |17.81 |40.45 |30.24 |749.41 |73.82 |209.18 450.40 529.55 |101.73 |2.06 |1.14E+09 |5.88E+04 {0.0228 94.27 92.63 |18.12 |40.54 |30.44 |746.96 |73.84 |209.24 449.58 $28.43 |101.75 |2.05 |1.13E+09 |5.87E+04 |0.0228 94.85 92.69 |17.89 |39.89 |30.19 |750.29 |73.24 |210.74 451.94 $31.69 |101.94 |2.10 |1.19F+09 |5.87E+04 }0.0230 Red Data is an average of all data points. 418 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO2/Argon Run 33: Heat Exchanger Composition -8.99 Argon,90.85 Carbon Dioxide Date -09 July 2008 Notebook Page -158 Front Page - Water Flow Rate -0.831 kg/min (0.01385 kg/s) Pressure Gauge -1010 psi Pressure Transducer -1089 psi Gas Inlet Temperature -120°C (248°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/mK) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater-0.000282474 Total Volume of System -0.00334 m2 419 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out Gas In Coefficient |TransferMeter|Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (Ib/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|(CC)(kg/m3)|W/m2K (W/m2K)|Nu Pr Gr Re Factor 64.06 74.74 |17.70 |37.64 |23.96 |774.74 |114.28 |120.98 336.11 378.31 |72.75 |1.10 |2.89E+08 |4.80E+04 |0.0137 64.01 74.77 |17.74 |37.72 |24.01 |774.11 |114.35 |121.00 335.42 377.43 |72.62 |1.10 |2.89E+08 |4.80E+04 |0.0137 64.06 74.70 |17.54 |37.74 |23.96 |774.55 |114.69 |120.68 332.93 374.29 |71.98 |1.10 |2.88E+08 |4.81E+04 {0.0137 64.01 74.66 |17.52 |37.67 |23.87 |775.58 |114.79 |120.55 333.95 375.57 |72.15 |1.10 |2.88E+08 |4.80E+04 |0.0137 63.90 74.69 |17.60 |37.77 |23.94 |774.78 |115.05 |120.46 333.10 374.49 |71.99 |1.10 |2.87E+08 |4.79E+04 |0.0137 64.04 74.67 |17.44 |37.81 |23.93 |774.84 |115.68 |120.07 330.59 371.33 |71.36 |1.09 |2.86E+08 |4.80E+04 |0.0136 64.12 74.57 |17.23 |38.06 |23.73 |777.06 {115.89 |119.77 332.17 373.32 |71.57 |1.09 |2.85E+08 |4.81E+04 |0.0136 63.99 74.68 |17.42 |38.67 |23.88 |775.58 |116.11 |119.86 333.02 374.40 |71.88 |1.09 |2.83E+08 |4.80E+04 |0.0136 64.01 74.77 |17.59 |38.92 |24.06 |773.54 |116.72 |119.70 332.04 373.16 |71.77 |1.09 |2.82E+08 |4.80E+04 |0.0136 63.91 74.95 |17.94 |39.20 |24.38 |770.00 |117.48 |119.62 330.21 370.85 |71.55 |1.09 |2.80E+08 |4.78E+04 |0.0136 63.87 74.96 |17.75 |39.34 |24.35 |770.38 |117.88 |119.44 327.37 367.27 |70.82 |1.09 |2.80E+08 |4.78E+04 |0.0136 63.90 74.94 |17.69 |39.48 |24.27 |771.35 |118.36 |119.14 327.90 367.94 |70.87 |1.08 |2.78E+08 |4.78E+04 |0.0135 63.86 74.99 |17.78 |39.50 |24.39 |769.90 |118.49 |119.16 326.57 366.27 |70.64 |1.08 |2.78E+08 |4.78E+04 |0.0135 63.87 74.96 |17.77 |39.52 |24.39 |769.83 |118.57 |119.06 326.35 365.99 |70.59 |1.08 |2.78E+08 |4.78E+04 |0.0135 63.70 74.91 |17.79 |39.35 |24.34 |770.42 |118.54 |118.99 326.59 366.29 |70.61 |1.08 |2.78E+08 |4.77E+04 |0.0135 63.66 74.95 |17.88 |39.44 |24.37 |770.07 |118.69 |118.98 327.12 366.96 |}70.76 |1.08 |2.77E+08 |4.76E+04 |0.0135 63.80 75.01 |17.99 |39.73 |24.50 |768.63 |118.61 |119.14 328.00 368.07 |71.08 |1.08 |2.77E+08 |4.77E+04 |0.0135 63.82 75.06 |18.07 |39.87 |24.58 |767.66 |118.73 |119.17 327.82 367.84 |71.10 |1.08 |2.76E+08 |4.77E+04 |0.0135 63.58 75.08 |18.12 |39.99 |24.60 |767.43 |119.10 |119.00 326.74 366.48 |70.84 |1.08 |2.75E+08 |4.75E+04 |0.0135 63.45 75.12 |18.17 |40.18 |24.67 |766.74 |119.27 |119.00 325.95 365.49 |70.69 |1.08 |2.75E+08 |4.74E+04 |0.0135 63.57 75.13 {|18.23 |40.17 |24.68 |766.52 |119.39 |118.94 326.85 366.61 |70.92 |1.08 |2.75E+08-:|4.75E+04 |0.0135 63.65 75.03 |18.15 |39.57 |24.58 |767.54 |119.55 |118.68 326.06 365.63 |70.65 |1.08 |2.75E+08 |4.76E+04 }0.0135 420 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas Side Mass Transfer Heat Flow Water |Water |Gas |Gas Out GasIn |Coefficient |Transfer Meter |Pressure |In Out Out Density |GasIn |Density |(VU)Coefficient Friction (Ib/hr)|(bar)ec)|ec)|ec)|tke/m3)|°C)|(kg/m3)|W/m2K (W/m2K)|Nu |Pr |Gr Re Factor 63.65 74.91 |18.10 |38.99 |24.43 |769.16 |119.48 |118.49 326.81 366.57 |70.73 |1.08 |2.76E+08 |4.76E+04 |0.0135 63.78 74.90 |18.15 |39.06 |24.41 |769.38 |119.75 |118.32 328.51 368.71 |71.11 |1.08 |2.75E+08 |4.77E+04 |0.0134 63.72 74.90 |18.17 |39.12 |24.43 |769.15 |119.88 |118.27 328.27 368.40 |71.07 |1.08 |2.75E+08 |4.77E+04 |0.0134 63.65 74.84 |18.06 |39.10 |24.38 |769.69 |119.89 |118.15 327.18 367.03 |70.77 |1.08 |2.75E+08 |4.76E+04 |0.0134 63.57 74.83 |18.09 |38.95 |24.37 |769.80 |119.96 |118.09 326.95 366.74 |70.70 |1.08 |2.75E+08 |4.76E+04 |0.0134 63.66 74.81 |18.02 |39.06 |24.37 |769.72 |120.27 |117.90 326.04 365.60 |70.48 |1.07 |2.74E+08 |4.76E+04 |0.0134 63.60 74.75 |17.98 |39.11 |24.28 |770.61 |120.69 |117.57 326.36 366.00 |70.48 |1.07 |2.73E+08 |4.76E+04 |0.0134 63.54 74.77 |18.08 |39.14 |24.33 |770.11 {120.65 |117.63 326.92 366.71 |70.65 |1.07 |2.72E+08 |4.75E+04 |0.0134 63.46 74.82 |18.11 |39.32 |24.34 |770.12 |120.66 |117.72 327.25 367.12 |70.73 |1.07 |2.72E+08 |4.75E+04 |0.0134 63.79 74.87 |17.87 |39.01 |24.28 |770.93 |118.11 119.15 328.94 369.25 |71.16 |1.08 |2.79E+08 |4.78E+04 |0.0135 Red Data is an average of all data points. CO2/Argon Run 34: Heat Exchanger Composition -8.99 Argon,90.85 Carbon Dioxide Date -10 July 2008 Notebook Page -158 Front Page- Water Flow Rate -0.866 kg/min (0.0144333 kg/s) Pressure Gauge -855 psi Pressure Transducer -922 psi Gas Inlet Temperature -160°C (320°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 421 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwin(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Gas Side Mass Total Heat Heat Flow Water |Water |Gas Gas Out Gas In Transfer Transfer Meter |Pressure |In Out Out Density {|GasIn |Density |Coefficient |Coefficient Friction (lb/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|CC)(kg/m3)|(U)W/m2K_|(W/m2K)Nu Pr Gr Re Factor 48.18 63.84 |17.80 |36.32 |21.49 774.05 |160.24 85.03 254.35 277.80 |52.38 |0.92 |1.57E-09 |3.63E+04 0.0104 48.17 63.78 |17.59 |36.32 |21.49 773.81 |161.00 84.74 250.06 272.69 |51.41 |0.92 |1.63E-09 |3.62E+04 0.0104 48.16 63.75 |17.69 |36.29 |21.56 772.76 |161.50 84.57 250.00 272.62 |51.43 |0.92 |1.63E-09 {3.62E+04 0.0104 48.14 63.78 |17.83 |36.38 |21.63 771.79 |161.54 84.59 250.97 273.78 |51.69 |0.92 |1.61E-09 |3.62E+04 0.0104 48.11 63.78 |17.86 |36.39 |21.58 772.61 |161.09 84.71 252.84 276.00 |52.09 |0.92 |1.59E-09 |3.62E+04 0.0104 48.09 63.74 |17.80 |36.37 |21.50 773.53 |160.98 84.69 253.09 276.30 |52.10 |0.92 |.1.59E-09 |3.62E+04 0.0104 48.12 63.70 |17.78 |36.28 |21.42 774.54 |161.07 84.61 254.41 277.87 |52.34 |0.92 |1.57E-09 |3.62E+04 0.0104 48.07 63.69 |17.85 |36.31 |21.39 774.96 |161.08 84.59 256.15 279.94 |52.71 |0.92 |1.55E-09 |3.62E+04 0.0104 48.04 63.69 |17.92 |36.36 |21.44 774.22 |161.43 84.49 255.94 279.70 |52.69 |0.92 |1.55E-09 |3.61E+04 0.0104 48.01 63.68 |17.95 |36.36 |21.48 773.70 |161.40 84.49 255.63 279.33 |52.65 |0.92 |1.55E-09 |3.61E+04 0.0104 48.00 63.64 |17.83 |36.01 |21.44 TIAAT7 |161.17 84.49 253.91 277.27 |52.25 |0.92 |1.58E-09 |3.61E+04 0.0104 48.01 63.58 |17.75 |35.80 |21.34 775.30 |161.43 84.34 254.01 277.39 |52.20 |0.92 |1.59E-09 |3.61E+04 0.0104 47.99 63.55 |17.78 |35.44 |21.32 775.47 |162.10 84.11 253.87 277.23 |52.14 |0.92 |1.60E-09 |3.61E+04 0.0103 48.01 63.44 |17.62 |34.86 |21.15 777.61 |162.34 83.90 253.56 276.86 |51.96 |0.92 |1.61E-09 |3.61E+04 0.0103 47.95 63.37 |17.55 |34.66 |21.09 778.16 |161.53 84.01 253.51 276.79 |51.95 |0.92 |1.61E-09 |3.61E+04 0.0103 47.99 63.21 |16.97 |34.49 |20.83 781.26 |161.20 83.86 248.90 271.31 |50.77 |0.92 |1.69E-09 |3.62E+04 0.0103 48.00 63.10 |16.88 |34.19 |20.59 784.17 |161.14 83.72 251.77 274.73 {51.27 |0.92 |1.66E-09 |3.62E+04 0.0103 422 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Gas Side Mass Total Heat Heat Flow Water |Water |Gas Gas Out Gas In Transfer Transfer Meter J Pressure |In Out Out Density |GasIn |Density |Coefficient |Coefficient Friction (lb/hr)|(bar)(°C)(°C)(°C)(kg/m3)|(°C)(kg/m3)|(U)W/m2K_|(W/m2K)Nu Pr Gr Re Factor 48.06 63.61 |17.67 |35.81 |21.34 775.42 |161.31 84.41 253.12 276.33 |52.00 |0.92 1.60E-09 |3.62E+04 0.0104 Red Data is an average of all data points. CO2/Argon Run 35: Heat Exchanger Composition -8.99 Argon,90.85 Carbon Dioxide Date -10 July 2008 Notebook Page 158 Front Page - Water Flow Rate -0.866 kg/min (0.0144333 kg/s) Pressure Gauge -845 psi Pressure Transducer -912 psi Gas Inlet Temperature -120°C (248°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwin(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 423 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out GasIn_|Coefficient |TransferMeter|Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (lb/hr)|(bar)CC)|CC)|CC)|(kg/m3)|(°C)(kg/m3)|W/m2K (W/m2K)|Nu Pr Gr Re Factor 46.27 62.79 |17.41 |31.30 |20.62 |782.85 |119.66 96.53 285.07 314.86 |60.30 |1.00 |1.71E+08 |3.62E+04 |0.0116 46.29 62.84 |17.56 |31.27 |20.67 |782.28 |119.46 96.69 287.54 317.88 |60.92 |1.00 |1.71E+08 |3.62E+04 |0.0116 46.01 62.79 |17.77 |31.31 |20.83 |779.95 |119.26 96.68 286.83 317.00 |60.90 |1.00 |1.70E+08 |3.60E+04 |0.0116 46.09 62.89 |17.92 |31.61 |20.98 |778.15 |119.83 96.64 286.53 316.64 |60.92 |1.00 |1.70E+08 |3.60E+04 |0.0116 46.10 62.95 |18.03 |31.88 |21.11 |776.59 {|119.97 96.70 286.24 316.28 |60.94 |1.00 |1.69E+08 |3.60E+04 |0.0116 44,78 62.39 |18.11 |31.22 |21.14 |774.19 |115.93 97.29 282.68 311.94 |60.39 |1.01 |1.68E+08 |3.52E+04 |0.0117 45.04 62.51 |18.05 |30.30 |21.03 |776.20 |108.51 |100.63 294.12 325.94 |63.23 |1.03 |1.77E+08 |3.55E+04 |0.0121 45.88 62.81 |17.89 |31.26 |21.03 |777.23 |114.20 98.76 289.83 320.68 |61.95 |1.01 |1.74E+08 |3.60E+04 |0.0118 46.04 62.82 |17.82 |31.71 |21.02 |777.42 |118.79 96.93 284.41 314.05 |60.50 |1.00 |1.70E+08 |3.60E+04 |0.0117 45.79 62.73 |17.90 |31.69 |20.99 |777.58 |119.53 96.48 284.73 314.44 |60.54 |1.00 |1.68E+08 |3.58E+04 |0.0116 45.85 62.74 |17.90 |31.78 |21.02 |777.19 |119.80 96.39 284.13 313.71 |60.42 |1.00 |1.68E+08 |3.58E+04 |0.0116 45.89 62.70 |17.67 |31.51 |20.87 |779.13 |118.54 96.81 283.96 313.51 |60.30 |1.00 |1.70E+08 |3.59E+04 |0.0117 45.82 62.63 |17.73 |31.58 |20.80 |779.85 |119.85 96.18 285,22 315.04 |60.51 |1.00 |1.68E+08 |3.58E+04 |0.0116 45.80 62.65 |17.85 |31.72 |20.92 |778.27 |120.56 95.94 284.11 313.69 |60.33 |1.00 |1.67E+08 |3.58E+04 |0.0116 45.81 62.70 |17.95 |31.68 |20.96 |777.89 |119.58 96.41 286.59 316.72 |60.96 |1.00 |1.68E+08 |3.58E+04 |0.0116 45.60 62.64 |17.99 |31.76 |21.02 |776.85 |120.04 96.13 284.26 313.88 |60.46 |1.00 }1.67E+08 |3.57E+04 |0.0116 45.86 62.79 |18.00 |31.78 |21.03 |777.14 |119.84 96.45 286.16 316.18 |60.89 |1.00 }1.68E+08 |3.58E+04 |0.0116 45.82 62.73 |17.86 |31.49 |20.94 |778.16 |118.43 96.92 286.03 316.03 |60.85 |1.00 |1.70E+08 |3.59E+04 |0.0117 Red Data is an average of all data points. 424 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO2/Argon Run 36: Heat Exchanger Composition -8.99 Argon,90.85 Carbon Dioxide Date -11 July 2008 Notebook Page 157 Front Page - Water Flow Rate -0.546 kg/min (0.0091 kg/s) Pressure Gauge -470 psi Pressure Transducer -499 psi Gas Inlet Temperature -205°C (401°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Total Heat |Gas Side Mass Transfer Heat Flow Water |Water |Gas Gas Out Gas In Coefficient |Transfer Meter |Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (lb/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|(°C)(kg/m3)|W/m2K (W/m2K)Nu Pr Gr Re Factor 18.58 34.41 |18.74 |32.32 |20.35 78.82 |207.65 39.02 53.28 $4.24 |22.75 |0.80 |7.47E-09 |1.39E+04 |0.0060 18.41 34.21 |18.79 |32.02 |20.43 78.18 |205.02 39.03 52.33 53.25 |22.44 |}0.80 |7.61E-09 |1.38E+04 |0.0060 18.31 34.25 |18.84 |32.18 |20.44 78.27 |199.20 39.62 §2.15 53.07 |22.57 |0.80 |7.37E-09 |1.39E+04 |0.0060 18.39 34.35 |18.91 |32.22 |20.43 78.60 |196.88 39.97 52.86 $3.80 |22.95 |0.80 |7.07E-09 |1.40E+04 |0.0061 18.46 34.47 |18.99 |32.68 |20.48 78.95 |199.98 39.82 53.60 $4.57 |23.15 |0.80 |7.01E-09 |1.40E+04 |0.0061 18.56 34.46 |19.07 |33.22 |20.57 78.85 |205.36 39.29 54.05 55.03 |23.16 |0.80 |7.11E-09 |1.39E+04 |0.0060 425 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out Gas In Coefficient |TransferMeter|Pressure |In Out Out |Density |GasIn |Density |(U)Coefficient Friction (b/hr)|(bar)(°C)(°C)(°C)|(kg/m3)|(CC)(kg/m3)|W/m2K (W/m2K)Nu Pr Gr Re Factor 18.46 34.24 |19.15 |33.26 |20.67 78.14 |206.24 38.96 53.56 54.53 |22.93 |0.80 |7.26E-09 |1.39E+04 |0.0060 18.29 34.21 |19.22 |32.72 |20.76 77.97 |200.42 39.46 52.52 53.46 |22.69 }0.80 |7.29E-09 |1.38E+04 |0.0060 18.31 34.29 |19.25 |32.54 |20.82 78.20 |196.56 39.93 52.23 53.15 |22.68 |0.80 |7.21E-09 |1.39E+04 |0.0061 18.37 34.41 |19.29 |32.76 |20.81 78.55 |198.08 39.92 52.81 53.76 |22.88 |0.80 |7.12E-09 |1.39E+04 |0.0061 18.47 34.51 |19.31 |33.31 |20.81 78.87 |202.97 39.58 53.63 54.60 |23.05 |0.80 |7.11E-09 |1.39E+04 |0.0060 18.56 34.49 |19.25 |33.93 |20.77 78.81 |208.61 39.02 54.11 55.10 |23.07 |0.80 |7.21E-09 |1.39E+04 |0.0060 18.46 34.42 |19.13 |33.88 |20.69 78.67 |210.24 38.80 53.63 54.61 |22.81 |0.79 |7.42E-09 |1.38E+04 |0.0060 18.46 34.47 |19.11 |33.71 |20.64 78.85 |209.88 38.89 53.75 54.72 |22.87 |0.80 |7.38E-09 |1.38E+04 |0.0060 18.51 34.49 |18.96 |33.96 |20.71 78.87 |211.78 38.74 52.61 53.54 |22.31 |0.79 |7.80E-09 |1.38E+04 |0.0059 18.53 34.37 |18.88 |33.94 |20.65 78.53 |213.08 38.48 52.54 53.48 |22.25 |0.79 |7.87E-09 |1.38E+04 |0.0059 18.45 34.38 |19.06 |33.04 |20.63 78.57 |204.50 39.28 53.10 54.06 |22.78 |0.80 |7.33E-09 |1.39E+04 |0.0060 Red Data is an average of all data points. CO2/Argon Run 37: Heat Exchanger Composition -8.99 Argon,90.85 Carbon Dioxide Date -11 July 2008 Notebook Page -157 Front Page - Water Flow Rate -0.546 kg/min (0.0091 kg/s) Pressure Gauge -450 psi Pressure Transducer -479 psi Gas Inlet Temperature -120°C (248°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2k) Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 426 Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Gas Side Mass Total Heat |Heat Flow Water |Gas Gas Out Gas In Transfer Transfer Meter |Pressure |Water {Out Out Density |Gas In Density |Coefficient |Coefficient Friction (lb/hr)|}(bar)In (°C)|CC)(°C)|(kg/m3)|CC)(kg/m3)|(U)W/m2K |(W/m2K)Nu Pr Gr Re Factor 15.90 33.06 }18.45 |25.09 |19.92 75.01 122.29 47.23 41.00 41.57 |20.19 |0.85 |6.70E-09 |1.32E+04 0.007( 15.59 32.89 |18.37 |24.84 |19.95 74.48 121.94 47.02 39.41 39.93 |19.42 |0.85 |7.23E-09 |1.30E+04 0.007€ 15.67 33.04 |18.35 |24.67 |19.89 74.96 119.18 47.67 39.69 40.22 |19.64 |0.85 |6.96E-09 |1.31E+04 0.007 15.77 33.02 |18.44 |24.80 |19.92 74.87 120.02 47.50 40.37 40.92 |19.96 |0.85 |6.76E-09 |1.31E+04 0.007( 15.69 33.00 |18.56 |24.85 |19.97 74.80 120.30 47.44 40.64 41.20 |20.08 |0.85 |6.68E-09 |1.31E+04 0.007 15.86 33.08 |18.66 |25.05 |20.07 74.96 120.97 47.45 41.15 41.72 |20.30 |0.85 |6.56E-09 |1.32E+04 0.007€ 15.66 32.91 |18.74 |25.13.|20.17 74.43 121.60 47.10 40.44 40.99 |19.94 |0.85 |6.80E-09 |1.30E+04 0.007C 15.50 32.93 |18.80 |24.96 }20.24 74.44 119,52 47.44 39.78 40.31 |19.68 |0.85 |6.90E-09 1.29E+04 0.007 15.76 33.05 |18.84 |25.13 |20.32 74.75 119.05 47.70 40.22 40.76 |19.90 {0.85 |6.72E-09 |1.31E+04 0.007 15.65 32.94 |18.90 |25.52 |20.37 74.42 120.20 47.37 40.13 40.67 |19.83 |0.85 |6.79E-09 |1.30E+04 0.007C 15.78 33.08 |18.97 |25.63 |20.50 74.74 120.60 47.51 40.13 40.68 |19.80 |0.85 |6.83E-09 |1.31E+04 0.007€ 15.72 32.97 |18.99 |25.77 |20.52 74.42 121.88 47.15 40.09 40.63 |19.75 |0.85 |6.91E-09 1.31E+04 0.007€ 15.50 32.95 |18.90 |25.64 |20.53 74.33 121.11 47.23 38.82 39.33 |19.14 |0.85 |7.33E-09 |1.29E+04 0.007 15.74 33.03 |18.85 |25.67 |20.49 74.61 120.76 47.42 39.44 39.96 |19.45 |0.85 |7.09E-09 |1.31E+04 0.007 15.52 32.89 |18.87 |25.61 |20.45 74.20 121.39 47.09 39.20 39.72 |19.33 |0.85 |7.20E-09 |1.29E+04 0.007 15.59 32.99 |18.83 |25.50 |20.43 74.51 120.24 47,43 39.20 39.71 |19.36 |0.85 |7.14E-09 |1.30E+04 0.007 15.66 32.95 |18.70 |25.60 {20.41 74.40 121.12 47.23 38.84 39.35 |19.15 |0.85 |7.33E-09 |1.30E+04 0.007( 427 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Gas Side Mass Total Heat Heat Flow Water |Gas Gas Out Gas In Transfer Transfer .Meter |Pressure |Water |Out Out |Density |Gas In Density |Coefficient |Coefficient Friction (ib/hr)_|(bar)In °C)|(°C)(°C)|(kg/m3)|(°C)(kg/m3)|(U)W/m2K |(W/m2K)Nu Pr Gr Re Factor 15.46 32.79 |18.64 |25.48 |20.35 73.96 121.24 46.96 38.28 38.77 |18.89 |0.85 |7.55E-09 1.29E+04 0.007 15.67 32.98 |18.71 25.27 |20.25 74.57 120.75 47.33 39.82 40.36 |19.66 |0.85 |6.97E-09 1.30F+04 0.007¢ Red Data is an average of all data points. CO2/Argon Run 38: Heat Exchanger Composition -8.99 Argon,90.85 Carbon Dioxide Date -14 July 2008 Notebook Page -157 Front Page - Water Flow Rate -0.561 kg/min (0.00935 kg/s) Pressure Gauge -220 psi Pressure Transducer -222 psi Gas Inlet Temperature -168°C (334.4°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwin(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 428 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out Gas In Coefficient |TransferMeter|Pressure }In Out Out Density |GasIn |Density |(U)Coefficient Friction (lb/hr)|(bar)(°C)(°C)|CC)|(kg/m3)|CC)(kg/m3)|W/m2K (W/m2K)Nu |Pr Gr Re Factor 6.07 15.52 |19.80 |23.55 |21.55 30.46 |167.94 18.99 14.07 14.13 |6.72 |0.77 |6.58E-08 |4.83E+03 |0.0036 6.13 15.46 |19.82 |23.61 |21.58 30.34 |168.85 18.87 14.22 14.29 |6.78 |0.77 |6.48E-08 |4.87E+03 |0.0036 6.16 15.39 |19.78 |23.71 |21.58 30.18 |169.40 18.76 14,23 14.30 |6.78 |0.77 |6.49E-08 |4.89E+03 |0.0036 6.08 15.36 |19.73 |23.76 |21.56 30.12 |168.68 18.75 14.00 14.06 |6.68 |0.77 |6.67E-08 |4.84E+03 |0.0036 5.99 15.37 |19.75 |23.63 |21.55 30.14 |166.99 18.84 13.80 13.87 |6.60 {|0.77 |6.76E-08 |4.78E+03 |0.0036 5.96 15.38 |19.81 |23.59 |21.55 30.17 |165.35 18.94 13.77 13.84 |6.61 |0.77 |6.70E-08 |4.76E+03 |0.0036 5.95 15.40 |19.86 |23.60 |21.57 30.20 |164.45 19.00 13.81 13.87 |6.63 |0.77 |6.62E-08 |4.76E+03 |0.0036 6.01 15.37 |19.89 |23.69 |21.60 30.14 |164.87 18.94 13.96 14.02 |6.70 |0.77 |6.49E-08 |4.80E+03 |0.0036 5.98 15.38 |19.83 |23.75 |21.62 30.16 |165.87 18.9]13.75 13.81 |6.59 |0.77 |6.75E-08 |4.77E+03 |0.0036 6.00 15.36 |19.79 |23.71 |21.62 30.12 |167.05 18.83 13.77 13.83 |6.59 |0.77 |6.80E-08 |4.78E+03 |0.0036 6.06 15.30 |19.79 |23.73 |21.60 29.99 |168.14 18.70 13.95 14.01 |6.66 |0.77 |6.68E-08 |4.82E+03 |0.0036 6.08 15.22 |19.75 |23.73 |21.56 29.83 |168.79 18.58 14.02 14.08 |6.69 |0.77 |6.64E-08 |4.83E+03 |0.0035 6.06 15.14 |19.71 |23.66 |21.52 29.65 |168.15 18.50 13.96 14.02 |6.67 |0.77 |6.66E-08 |4.83E+03 |0.0035 5.96 15.12 |19.72 |23.51 |21.50 29.62 |165.87 18.59 13.69 13.75 |6.57 |0.77 |6.79E-08 |4.75E+03 |0.0036 5.86 15.13 |19.76 |23.41 {21.52 29.64 |162.75 18.75 13.45 13.51 |6.49 |0.77 |6.86E-08 |4.70E+03 |0.0036 5.82 15.16 |19.79 |23.28 |21.55 29.69 |160.33 18.89 13.29 13.35 |6.44 |0.77 |6.88E-08 |4.68E+03 |0.0036 5.81 15.17 |19.74 |23.26 |21.57 29.72 |159.31 18.96 13.13 13.19 |6.37 |0.77 |7.00E-08 |4.68E+03 |0.0036 6.00 15.31 |19.78 |23.60 |21.57 30.01 |166.05 18.81 13.82 13.88 |6.62 |0.77 |6.70E-08 |4.79E+03 |0.0036 Red Data is an average of all data points. 429 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO2/Argon Run 39: Heat Exchanger Composition -8.99 Argon,90.85 Carbon Dioxide Date -14 July 2008 Notebook Page -157 Front Page - Water Flow Rate -0.561 kg/min (0.00935 kg/s) Pressure Gauge -215 psi Pressure Transducer -220 psi Gas Inlet Temperature -120°C (248°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 430 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Total Heat |Gas SideMassTransferHeat Flow Water |Water |Gas Gas Out Gas In Coefficient |Transfer Meter |Pressure |In Out Out Density |GasIn |Density |(U)Coefficient Friction (lb/hr)|(bar)(°C)(°C)CC)|(kg/m3)|(CC)(kg/m3)|W/m2K (W/m2K)Nu |Pr Gr Re Factor 5.99 15.36 |19.65 |22.23 |21.24 30.17 |118.59 21.40 12.81 12.86 |6.71 |0.79 |4.89E-08 |5.08E+03 |0.0039 5.91 15.32 |19.70 |22.31 |21.31 30.08 |119.20 21.31 12.64 12.70 |6.62 |0.79 |5.05E-08 |5.01E+03 |0.0039 5.84 15.38 |19.71 |22.33 |21.39 30.20 |118.54 21.44 12.35 12.40 |6.47 |0.79 |5.26E-08 |4.96E+03 |0.0039 5.88 15.41 |19.61 |22.31 |21.44 30.26 |117.50 21.55 12.15 12.20 |6.38 |0.79 |5.38E-08 |5.00E+03 |0.0039 5.94 15.37 {19.52 |22.26 |21.43 30.17 |117.66 21.48 12.14 12.19 |6.37 |0.79 |5.41E-08 |5.05E+03 |0.0039 5.96 15.32 |19.38 |22.20 |21.40 30.05 |118.33 21.35 12.03 12.08 |6.31 |0.79 |5.55E-08 |5.06E+03 |0.0039 5.93 15.25 |19.40 |22.08 |21.35 29.91 |118.94 21,22 12.08 12.12 |6.32 |0.79 |5.55E-08 |5.03E+03 |0.0039 5.85 15.24 |19.48 |22.04 |21.35 29.90 |118.71 21.22 12.05 12.09 |6.31 |0.79 |5.56E-08 |4.97E+03 |0.0039 5.82 15.31 |19.57 |22.09 |21.39 30.04 |117.91 21.37 12.01 12.06 |6.30 |0.79 |5.54E-08 |4.94E+03 |0.0039 5.87 15.32 |19.66 }22.12 |21.50 30.04 |117.96 21.38 12.09 12.14 |6.34 |0.79 |5.47E-08 |4.99E+03 |0.0039 5.91 15.27 |19.71 |22.16 |21.58 29.93 |118.74 21.26 12.14 12.19 |6.36 |0.79 |5.47E-08 |5.01E+03 |0.0039 5.90 15.21 |19.72 |22.24 |21.64 29.80 |119.51 21.13 12.06 12.11 |6.31 |0.79 |5.59E-08 |5.00E+03 |0.0039 5.85 15.19 |19.75 |22.25 |21.70 29.73 |119.95 21.07 11.91 11.96 |6.22 |0.79 |5.76E-08 |4.95E+03 |0.0039 5.80 15.24 |19.77 |22.23 |21.71 29.85 |119.91 21.15 11.82 11.87 |6.17 |0.79 |5.85E-08 |4.91E+03 |0.0039 5.84 15.24 |19.79 |22.26 |21.69 29.84 |119.56 21.16 11.96 12.01 |6.25 |0.79 |5.69E-08 |4.95E+03 |0.0039 5.88 15.19 |19.80 |22.30 |21.70 29.74 |120.16 21.06 12.05 12.10 |6.29 |0.79 |5.64E-08 |4.97E+03 |0.0039 5.87 15.13 |19.77 |22.31 |21.68 29.62 |120.81 20.94 12.05 12.10 |6.28 |0.79 |5.67E-08 |4.97E+03 |0.0038 5.88 15.28 |19.65 |22.22 |21.50 29.96 |118.94 21.26 12.14 12.19 |6.35 |0.79 |5.49E-08 |4.99E+03 |0.0039 Red Data is an average of all data points. 431 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Heat Exchanger Data Components - Argon Carbon Dioxide GC Analysis - Trial 1 Trial 2 Average Carbon Dioxide 84.50719 |83.26045 |83.88382 Argon 10.55223 |10.71589 |10.63406 Nitrogen 3.53185 4.66157 4.09671 Note - The presence of nitrogen gas in the GC analysis may be explained by an inadvertent leak in the piping that brought the gas from the heat exchanger to the GC,thus allowing room air into the pipe. Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 432 GC Run 25: Agilent Cerity QA/QC Report Sample name:0807HeatXGRArCOO7 Sample note: Submission time:Thursday,August 07,2008 9:54:42 AM Operator: Injection date:Thursday,August 07,2008 9:55:05 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A Method:Aug4Cal Method last saved:Tuesday,August 05,2008 1:12:36 PM 433 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 <TCDIA >;;34 }:; :i ! !+; || .Ec a dn 1 15 2 25 min TCDOZA t :H i is '_ *oe 4iii --Soo +SEES SE IES SLA SEE A GER RE RR a=2«ESTD Report Calibration last saved:Tuesday,August 05,2008 1:12:36 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 434 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV's]Amt/Area Amount[mass%]Name 1 1.473 BP 8.5422e+004 1.25447e-004 10.71589 Argon/Oxygen 1 1.882 BB 3.4985e+004 1.33244e-004 4.66157 Nitrogen 2 0.276 BB 1.6487e+006 5.05013e-005 83.26045 Carbon Dioxide 2 0.974 PB 1298.81249 0.00000e+000 0.00000 2 1.255 ---Sulfur Dioxide Total amount =98.63791 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 26: Agilent Cerity QA/QC Report Sample name:0807HeatXGRArCO06 Sample note: Submission time:Thursday,August 07,2008 9:49:13 AM Operator: Injection date:Thursday,August 07,2008 9:49:34 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A Method:Aug4Cal Method last saved:Tuesday,August 05,2008 1:12:36 PM 435 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >{: °- 2Qo io7°--1 ++.> .Os 1 15 2 25 min TCDOZA 2 :. , 4 Fy :: =: 5jo : 5ou *©:!|||of fe Ree pen .7 ; °: |7 T oe 1 en nee |T r __ Os 1 _a 15 2 25 min ESTD Report Calibration last saved:Tuesday,August 05,2008 1:12:36 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 436 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Inlet Signal Retention Time [min]Type Area [tiv*s]Amt/Area Amount [mass%]Name 1 1.473 BP 8.4117e+004 1.25447e-004 10.55223 Argon/Oxygen 1 1.882 BB 2.6507e+004 1.33244e-004 3.53185 Nitrogen 2 0.275 BB 1.6734e+006 5.05013e-005 84.50719 Carbon Dioxide 2 0.975 PB 1169.66716 0.00000e+000 0.00000 2 1.255 ---Sulfur Dioxide Total amount =98.59127 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated CO2/Argon Run 40: Heat Exchanger Composition -10.63 Argon,83.88 Carbon Dioxide,4.10 Nitrogen Date -01 August 2008 Notebook Page -154 Front Page - Water Flow Rate -0.588 kg/min (0.0098 kg/s) Pressure Gauge -1085 psi Pressure Transducer -1175 psi Gas Inlet Temperature -143°C (289.4 °F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 437 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass_|Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(Ib/hr)(VU)Coefficient W/m2K (W/m2K) 57.48 80.93 |20.50 |47.05 |25.05 |778.47 |133.35 |122.16 325.11 364.43 |68.92 |1.07 |9.32E-10 |4.18E+04 |0.0146 $7.70 81.02 |20.47 |47.61 |25.09 |778.32 |136.16 |120.92 322.60 361.28 |68.24 |1.06 |9.54E-10 |4.19E+04 |0.0144 57.86 81.07 |20.29 |48.10 |25.10 |778.35 |138.21 |120.00 318.46 356.09 |67.19 |1.05 |9.86E-10 |4.20E+04 |0.0143 57.91 81.03 |20.12 |48.44 |24.96 |779.81 |139.90 |119.14 317.28 354.63 |66.75 |1.05 |1.00E-09 |4.20E+04 |0.0142 58.04 81.02 |20.13 |48.70 |24.89 |780.65 |141.17}118.52 318.88 356.62 |67.03 |1.05 |9.93E-10 |4.21E+04 |0.0142 58.12 81.03 |20.15 |48.89 |24.89 |780.59 |141.98 |118.16 319.09 356.88 |67.05 |1.04 |9.92E-10 |4.21E+04 [|0.0141 38.11 81.04 |20.18 |48.97 |24.93 |780.14 |142.59 |117.90 318.04 355.57 |66.82 |1.04 |1.00E-09 |4.21E+04 |0.0141 58.12 81.06 |20.25 |49.26 |25.00 |779.44 |143.03 |117.73 318.14 355.70 |66.88 |1.04 |9.96E-10 |4.21E+04 |0.0141 57.98 80.98 |20.25 |49.01 |24.96 |779.71 |142.57 1]117.80 318.28 355.86 |66.91 |1.04 |9.95E-10 |4.20E+04 |0.0141 57.85 80.94 |20.25 |48.80 |24.94 |779.86 |141.54 |118.22 318.78 356.49 |67.05 |1.04 |9.90E-10 |4.19E+04 |0.0141 $7.90 80.96 |20.30 |49.00 |24.96 |779.67 |141.69 |118.18 319.89 357.88 |67.32 |1.04 |9.80E-10 |4.20E+04 |0.0141 57.92 81.01 |20.26 |48.53 |24.98 |779.55 |140.20 |118.98 319.50 357.40 |67.29 |1.05 |9.84E-10 |4.20E+04 |0.0142 Red Data is an average of all data points. CO2/Argon Run 41: Heat Exchanger Composition -10.63 Argon,83.88 Carbon Dioxide,4.10 Nitrogen Date -04 August 2008 Notebook Page -154 Front Page - Water Flow Rate -0.598 kg/min (0.009967 kg/s) Pressure Gauge -755 psi Pressure Transducer -815 psi 438 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Gas Inlet Temperature -120°C (248 °F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2KwIn(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(VU)Coefficient W/m2K (W/m2K) 31.96 56.32 |20.23 |33.20 |21.59 |176.55 |120.58 85.04 116.23 120.90 |46.20 |0.96 |1.58E-09 |2.54E+04 |0.0110 32.24 56.51 |20.31 |33.17 |21.66 |177.76 |119.71 85.64 117.75 122.54 |46.70 |0.96 |1.54E-09 |2.56E+04 |0.0111 32.11 56.46 |20.36 |33.32 |21.73 |177.08 |120.47 85.32 116.69 121.40 |46.33 |0.96 |1.57E-09 |2.55E+04 |0.0110 32.07 56.39 |20.40 |33.51 |21.80 |176.22 |121.35 84.91 115.90 120.54 |46.09 |0.95 |1.59E-09 |2.55E+04 |0.0110 31.55 §6.17 |20.44 |32.89 |21.81 |174.46 |117.96 85.65 113.59 118.04 |45.57 |0.96 |1.60E-09 |2.51E+04 |0.0111 32.10 56.47 |20.50 |33.04 |21.89 |176.40 |117.57 86.28 115.89 120.52 |46.28 |0.96 |1.55E-09 |2.56E+04 |0.0111 32.23 56.52 |20.54 |33.62 |21.94 |176.60 |120.56 85.38 116.34 121.01 |46.28 |0.96 |1.57E-09 |2.56E+04 |0.0110 31.84 56.29 |20.55 |33.63 |21.95 |174.81 |121.32 84.75 114.47 118.99 |45.72 |0.95 |1.61E-09 |2.53E+04 |0.0110 32.14 56.45 |20.53 |33.59 |21.95 |176.01 |120.24 85.37 115.59 120.20 |46.07 |0.96 |1.58E-09 |2.55E+04 |0.0110 32.03 56.39 |20.53 |33.71 |21.92 |175.72 |120.80 85.09 115.75 120.38 |46.14 |0.95 |1.58E-09 |2.54E+04 |0.0110 31.94 56.28 |20.52 |33.80 |21.89 |174.94 |121.57 84.64 115.67 120.28 |46.18 |0.95 |1.58E-09 |2.54E+04 |0.0110 31.66 56.20 |20.52 |33.25 |21.87 |174.46 |118.63 85.48 114.63 119.16 |45.97 |0.96 |1.57E-09 |2.52E+04 |0.0111 439 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(U)Coefficient W/m2K (W/m2K) 31.96 56.30 |20.54 |33.53 |21.84 |175.30 |119.31 85.41 117.17 121.91 |46.87 |0.96 |1.51E-09 |2.54E+04 |0.0110 31.59 56.15 |20.62 |33.28 |21.83 |174.26 |118.56 85.41 117.26 122.01 |47.10 |0.96 |1.49E-09 |2.52E+04 |0.0111 31.94 $6.29 |20.58 |33.59 |21.82 |175.34 |119.19 85.44 118.70 123.56 |47.50 |0.96 |1.47E-09 |2.54E+04 [|0.0110 31.89 56.27 |20.53 |33.49 |21.78 |175.31 |119.39 85.33 118.08 122.89 |47.23 |0.96 |1.49E-09 |2.54E+04 |0.0110 31.90 56.21 |20.47 |33.57 |21.81 |174.78 |120.55 84.87 116.08 120.73 |46.42 |0.95 |1.55E-09 |2.54E+04 |0.0110 32.05 56.34 |20.39 |33.21 |21.81 |175.74 |120.14 85.21 115.06 119.63 |45.88 |0.96 |1.60E-09 |2.55E+04 |0.0110 31.96 56.33 |20.48 |33.41 |21.83 |175.65 |119.88 85.29 116.16 120.82 |46.36 |0.96 |1.56E-09 |2.54E+04 |0.0110 Red Data is an average of all data points. CO2/Argon Run 42: Heat Exchanger Composition -10.63 Argon,83.88 Carbon Dioxide,4.10 Nitrogen Date -05 August 2008 Notebook Page -154 Front Page -- Water Flow Rate -0.528 kg/min (0.0088 kg/s) Pressure Gauge -725 psi Pressure Transducer -783 psi Gas Inlet Temperature -205°C (401°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK. Inner Tube Diameter,Di- 0.011 m Inner Tube Outside Diameter,Do-0.0127 m Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 440 Di/2Kwin(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass_|Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(CC)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(VU)Coefficient W/m2K (W/m2K) 13.90 31.04 |19.30 |23.69 |20.57 68.81 |122.99 44.06 35.75 36.18 |17.71 |0.84 |8.60E-09 |1.16E+04 |0.0067 13.66 30.93 |19.34 |23.45 |20.58 68.51 |120.34 44.27 35.11 35.52 |17.48 |0.84 |8.68E-09 |1.14E+04 |0.0067 13.89 31.19 |19.44 |23.46 |20.61 69.22 |117.62 45.04 36.07 36.50 |18.03 |0.84 |8.03E-09 |1.16E+04 |0.0068 14.13 31.27 |19.52 |23.72 |20.67 69.41 |119.26 44,93 37.02 37.48 |18.45 |0.84 |7.74E-09 |1.18E+04 |0.0068 14.06 31.15 |19.58 |23.87 |20.69 69.08 |122.07 44.36 37.21 37.68 |18.47 |0.84 |7.85E-09 |1.17E+04 |0.0067 13.81 30.98 |19.62 |23.83 |20.71 68.59 |122.32 44.07 36.63 37.08 |18.18 |0.84 |8.10E-09 |1.15E+04 |0.0067 13.77 31.06 |19.63 |23.70 |20.73 68.79 |119.89 44.52 36.36 36.80 |18.11 |0.84 |8.04E-09 |1.15E+04 |0.0068 14.07 31.26 |19.58 |23.79 |20.71 69.37 |119.39 44.90 36.96 37.42 |18.42 |0.84 |7.76E-09 |1.17E+04 |0.0068 14.11 31.19 |19.54 |23.91 |20.68 69.19 |122.15 44.40 37.25 37.71 |18.48 |0.84 |7.85E-09 |1.17E+04 |0.0067 13.93 31.03 |19.46 |23.86 |20.64 68.77 |123.43 43.99 36.48 36.93 |18.06 |0.84 |8.27E-09 |1.16E+04 |0.0067 13.71 30.91 |19.28 |23.58 |20.59 68.44 |121.67 44.04 34.91 35.32 |17.34 |0.84 |8.89E-09 |1.14E+04 |0.0067 13.90 31.13 |19.15 |23.39 |20.48 69.10 |119.19 44.72 35.21 35.62 |17.55 |0.84 |8.58E-09 |1.16E+04 |0.0068 14.13 31.19 |19.17 |23.49 |20.39 69.34 |120.52 44.64 36.68 37.13 |18.25 |0.84 |8.00E-09 |1.18E+04 |0.0067 14.06 31.08 |19.27 |23.63 |20.41 69.00 |122.74 44.15 37.12 37.58 |18.41 |0.84 |7.96E-09 |1.17E+04 |0.0067 13.84 30.92 |19.39 |23.62 |20.51 68.50 |122.81 43.90 36.61 37.06 |18.16 |0.84 |8.15E-09 |1.15E+04 |0.0067 13.71 30.91 |19.44 |23.55 |20.60 68.44 |120.57 44.20 35.77 36.20 |17.81 |0.84 |8.36E-09 |1.14E+04 |0.0067 13.92 31.08 |19.42 |23.66 |20.60 68.91 |121.06 44.39 36.32 36.76 |18.06 |0.84 |8.18E-09 |1.16E+04 |0.0067 Red Data is an average of all data points. 441 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO2/Argon Run 43: Heat Exchanger Composition -10.63 Argon,83.88 Carbon Dioxide,4.10 Nitrogen Date -05 August 2008 Notebook Page -154 Front Page - Water Flow Rate -0.722 kg/min (0.012033 kg/s) Pressure Gauge -425 psi Pressure Transducer -453 psi Gas Inlet Temperature -120°C (248°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass Pressure |Water |Water |Gas Gas Out |Gas In }Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)CC)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(U)Coefficient W/m2K (W/m2K) 31.75 53.96 |19.46 |43.55 |21.15 |161.16 |211.44 61.59 109.67 113.81 |40.52 |0.84 |2.59E-09 |2.32E+04 |0.0085 31.46 53.68 |19.44 |42.89 |21.04 |159.63 |207.33 61.89 109.42 113.54 |40.79 |0.84 |2.54E-09 |2.31E+04 |0.0085 31.43 $3.69 |19.55 |42.17 |21.03 |159.80 |201.51 62.84 110.76 114.99 |41.60 |0.84 |2.41E-09 |2.32E+04 |0.0086 31.52 53.78 |19.66 |42.25 |21.10 |160.16 |201.04 63.03 111.93 116.24 |42.04 |0.84 |2.35E-09 |2.32E+04 |0.0087 31.61 53.88 |19.75 |42.88 |21.22 |160.42 |203.66 62.72 111.99 116.31 |]41.91 |0.84 |2.38E-09 |2.32E+04 |0.0086 31.68 $3.96 |19.78 |43.62 |21.30 |160.67 |206.93 62.30 111.66 115.96 |41.58 |0.84 |2.43E-09 |2.32E+04 |0.0086 442 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(U)Coefficient W/m2K (W/m2K) 31.77 53.99 |19.86 |43.99 |21.37 |160.65 |210.07 61.84 112.31 116.66 |41.67 |0.84 |2.43E-09 |2.32E+04 |0.0085 31.69 53.95 |19.90 |44.07 |21.46 |]160.14 |210.48 61.73 111.20 115.46 |41.28 |0.84 |2.48E-09 |2.31E+04 |0.0085 31.66 53.98 |19.91 |44.07 |21.45 |160.34 |210.10 61.83 111.35 115.62 |41.34 |0.84 |2.47E-09 |2.31E+04 |0.0085 31.71 53.98 |19.92 |44.15 |21.45 |160.35 |211.28 61.65 111.68 115.98 |41.40 |0.84 |2.47E-09 |2.31E+04 |0.0085 31.60 53.86 |19.76 |43.99 |21.44 |159.58 |}210.26 61.65 108.94 113.03 |40.48 |0.84 |2.58E-09 |2.31E+04 |0.0085 31.57 53.84 |19.68 |43.65 |21.34 |159.79 |208.28 61.94 109.16 113.26 |40.64 |0.84 |2.55E-09 |2.31E+04 |0.0085 31.59 53.86 |19.70 |43.59 |21.27 |160.13 |208.91 61.87 110.61 114.83 |41.13 |0.84 |2.50E-09 |2.31E+04 |0.0085 31.67 53.89 |19.63 |43.72 |21.27 |160.29 |210.03 61.73 109.80 113.96 |40.74 |0.84 |2.55E-09 |2.31E+04 |0.0085 31.62 53.88 |19.71 |43.47 |21.28 |160.22 |207.95 62.04 110.75 114.98 |41.22 |0.84 |2.48E-09 |2.31E+04 |0.0085 Red Data is an average of all data points. 443 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO2/Argon Run 44: Heat Exchanger Composition -10.63 Argon,83.88 Carbon Dioxide,4.10 Nitrogen Date -06 August 2008 Notebook Page -153 Front Page - Water Flow Rate -0.492 kg/min (0.0082 kg/s) Pressure Gauge -420 psi Pressure Transducer -447 psi Gas Inlet Temperature -209°C (408.2°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwin(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(U)Coefficient W/m2K (W/m2K) 14.58 30.83 |19.68 |31.22 |20.46 68.28 |208.99 34.75 46.86 47.60 |20.21 |0.79 |9.25E-09 |1.09E+04 |0.0056 14.75 30.86 |19.72 |31.18 |20.41 68.38 |209.96 34.70 48.44 49.23 |20.87 |0.79 |8.71E-09 |1.11E+04 |0.0056 14.57 30.83 |19.73 |31.16 |20.45 68.29 }209.82 34.68 47.50 48.26 |20.47 |0.79 |9.05E-09 |1.09E+04 |0.0056 14.59 30.86 |19.71 |31.21 |20.47 68.36 |209.24 34.76 47.00 47.74 |20.26 |0.79 |9.22E-09 |1.09E+04 |0.0056 14.55 30.82 |19.75 |31.15 |20.46 68.26 |209.11 34.73 47.53 48.29 |20.50 |0.79 |9.00E-09 |1.09E+04 |0.0056 444 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass'|Pressure |Water |Water |Gas Gas Out |GasIn |GasIn_|Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(CC)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr),(U)Coefficient W/m2K (W/m2K) 14.56 30.87 |19.82 |31.17 |20.53 68.35 |208.78 34.81 47.57 48.34 |20.53 |0.79 |8.96E-09 |1.09E+04 |0.0056 14.51 30.87 |19.87 |31.34 |20.61 68.33 |209.50 34.76 47.11 47.85 |20.30 |0.79 |9.18E-09 |1.09E+04 |0.0056 14.63 30.81 |19.89 |31.42 |20.59 68:17 |209.63 34.68 47.92 48.70 |20.66 |0.79 |8.86E-09 |1.10E+04 |0.0056 14.50 30.86 |19.92 |31.32 |20.61 68.28 |208.58 34.81 47.55 48.31 |20.52 |0.79 |8.95E-09 |1.09E+04 |0.0056 14.56 30.83 |19.87 |31.38 |20.64 68.21 |208.65 34.78 46.87 47.61 |20.23 |0.79 |9.22E-09 |1.09E+04 |0.0056 14.54 30.83 |19.55 |31.38 |20.55 68.24 |208.86 34.76 44.66 45.33 |19.25 |0.79 |1.02E-08 |1.09E+04 |0.0056 14.55 30.82 |19.40 |31.26 |20.41 68.28 |208.55 34.77 44.57 45.24 |19.23 |0.79 |1.02E-08 }1.09E+04 |0.0056 14.64 30.82 |19.46 |31.09 |20.28 68.34 |208.71 34.76 46.63 47.36 |20.12 |0.79 |9.34E-09 |1.10E+04 |0.0056 14.64 30.74 |19.50 |31.14 |20.29 68.09 |209.19 34.62 46.97 47.71 |20.26 |0.79 |9.22E-09 |1.10E+04 |0.0056 14.47 30.76 |19.50 |31.05 |20.33 68.14 |207.70 34.77 45.90 46.61 |19.84 |0.79 |9.57E-09 |1.09E+04 |0.0056 14.44 30.79 |19.54 |31.06 |20.33 68.23 |207.28 34.84 46.14 46.86 |19.95 |0.79 |9.45E-09 |1.09E+04 |0.0056 14.57 30.83 |19.68 |31.22 |20.46 68.26 |208.91 34.75 46.83 47.57 |20.20 |0.79 |9.28E-09 |1.09E+04 |0.0056 Red Data is an average of all data points. CO2/Argon Run 45: Heat Exchanger Composition -10.63 Argon,83.88 Carbon Dioxide,4.10 Nitrogen Date -06 August 2008 Notebook Page -153 Front Page- Water Flow Rate -0.667 kg/min (0.011117 kg/s) Pressure Gauge -235 psi Pressure Transducer -246 psi Gas Inlet Temperature -126°C (258.8°F) 445 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/mK) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwin(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu |Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(VU)Coefficient W/m2K (W/m2K) 6.32 16.96 |18.99 |21.24 |19.98 33.85 |127.81 23.09 15.48 15.56 |7.96 |0.79 |3.82E-08 |5.30E+03 |0.0042 6.30 16.96 |19.04 |21.33 |20.04 33.84 |127.21 23.13 15.41 15.49 |7.93 |0.79 |3.83E-08 |5.29E+03 |0.0042 6.26 16.97 |19.1 |21.42 |20.10 33.87 |126.40 23.21 15.31 15.39 |7.89 |0.79 |3.84E-08 |5.26E+03 |0.0042 6.18 16.99 |19.12 |21.48 |20.16 33.89 |126.19 23.24 14.95 15.03 |7.71 |0.79 |4.02E-08 |5.19E+03 |0.0043 6.20 16.98 |19.07 |21.40 |20.17 33.86 |126.46 23.20 14.82 14.89 |7.63 |0.79 |4.11E-08 |5.20E+03 |0.0042 6.14 16.96 |19.09 |21.38 |20.17 33.83 |126.61 23.17 14.76 14.83 |7.60 |0.79 |4.1SE-08 |5.1S5SE+03 |0.0042 6.32 16.94 |19.17 |21.45 |20.18 33.78 |126.80 23.13 15.41 15.49 |7.93 |0.79 |3.81E-08 |5.31E+03 |0.0042 6.30 16.90 |19.28 |21.51 |20.20 33.69 |127.05 23.06 15.66 15.74 |8.06 |0.79 |3.69E-08 |5.29E+03 |0.0042 6.24 16.94 |19.40 |21.59 |20.27 33.76 |126.61 23.14 15.67 15.75 |8.07 |0.79 |3.67E-08 |5.24E+03 |0.0042 6.25 16.95 |19.50 |21.66 |20.38 33.78 |125.83 23.21 15.64 15.73 }8.07 |0.79 |3.65E-08 |5.26E+03 |0.0042 6.25 16.98 |19.59 |21.76 |20.52 33.82 |125.56 23.27 15.49 15.57 |7.99 |0.79 |3.71E-08 |5.26E+03 |0.0042 6.25 16.96 |19.22 |21.47 |20.20 33.82 |126.59 23.17 15.33 15.41 |7.89 |0.79 |3.85E-08 |5.25E+03 |0.0042 Red Data is an average of all data points. 446 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Heat Exchanger Data Components - Argon Carbon Dioxide GC Analysis - Trial 1 Trial 2 Trial 3 Average Carbon Dioxide 83.9613 |83.67514 |83.46859 |83.70168 Argon 13.15694 }13.4486 |13.71958 |13.44171 GC Run 27: Agilent Cerity QA/QC Report Sample name:0725ArCOOGasVessel6 Sample note: Submission time:Friday,July 25,2008 2:48:40 PM Operator: Injection date:Friday,July 25,2008 2:52:35 PM GC Description:Mlcro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 447 TCDIA 2 2 , ioO: o7 trs) q : oO +a can :- $e o 15 2 25 min TCD2A >aOe=-epee Gnenn Ceee Cc ° 2 nm oO, © :i 8 a | @ |. : i :ad ry -T os |aed 05 4 16 2 25 min TCD3ZA i anz ,Rk:Oo.; =i :°°: :>;€,: :e. 4 3 Hl :r i i po iSSESaSePRaS|r _AL AS Ye 265 min ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 448 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Unknown Signal Retention Time [min]Type Area [iv*s]Amt/Area Amount [mass%]Name 1 1.500 ---Oxygen 1 1.637 ---Nitrogen 2 0.245 BP 2.4707e+005 0.00000e+000 0.00000 2 0.276 VB 1.6978e+006 4.94521e-005 83.96130 Carbon Dioxide 2 1.220 ---Sulfur Dioxide 3 1.352 BB 9.1023e+004 1.44545e-004 13.15694 Argon/Oxygen 3 2.112 ---Nitrogen_2 Total amount =97.11825 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 28: Agilent Cerity QA/QC Report Sample name:0725ArCOOGasVessel5 Sample note: Submission time:Friday,July 25,2008 2:48:39 PM Operator: Injection date:Friday,July 25,2008 2:49:02 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM 449 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA > =a o o 4 io o +; ry 05 4 15 2 25 min TCDZA 2 ence,1 neogiaiec! o 2 :"i ..oO :; ©nt : 2 N ::oo : r T ed T T -T 05 1 15 2 25 min TCDSA 24 is een,a>::aeoO,:=::So:: 2:f 5 i vel i6::' Nn : :i :: a_06_: 1 15 2.28 min ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 450 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Unknown Signal Retention Time [min]Type Area [tiv*s]Amt/Area Amount [mass%]Name 1 1.500 ---Oxygen 1 1.637 ---Nitrogen 2 0.245 BP 2.5248e+005 0.00000e+000 0.00000 2 0.276 VB 1.6920e+006 4.94521e-005 83.67514 Carbon Dioxide 2 1.220 ---Sulfur Dioxide 3 1.351 BB 9.3041e+004 1.44545e-004 13.44860 Argon/Oxygen 3 2.112 ---Nitrogen_2 Total amount =97.12374 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 29: Agilent Cerity QA/QC Report Sample name:0725ArCOOGasVessel4 Sample note: Submission time:Friday,July 25,2008 2:30:19 PM Operator: Injection date:Friday,July 25,2008 2:41:16 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM 451 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCD1A > = q . °Oo 4 -a 3) o 4 '-asic on T T ba T T T 05 4 15 2 25 min TCD2A >Re=a HlApe Mlo2i: a Heci :; o f a }: "i i.:» o.::!©- 8 9 @ ane o T T aa T T --T 05 1 15 2 25 min TCOZA 24 ic.rater.. :£:- :"6°! :@:: :"Oo::: i 2 :! ae 8,4a:+: :;8 :wr:!iin]ne :.; N :: : T T T T r -T 05 1 15 2 2 min ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 452 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Unknown Signal Retention Time [min]Type Area [iV's]Amt/Area Amount [mass%] 1 1.500 --- 1 1.637 --- 2 0.245 BP 2.5756e+005 0.00000e+000 0.00000 2 0.276 VB =1.6879e+006 4.94521e-005 83.46859 2 1.220 --- 3 1.351 BB 9.4916e+004 1.44545e-004 13.71958 3 2.112 --- Total amount =97.18817 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated CO>/Argon Run 46: Heat Exchanger Composition -10.63 Argon,83.88 Carbon Dioxide,4.10 Nitrogen Date -01 August 2008 Notebook Page -154 Front Page - Water Flow Rate -0.588 kg/min (0.0098 kg/s) Pressure Gauge -1085 psi Pressure Transducer -1175 psi Gas Inlet Temperature -143°C (289.4 °F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwin(Do/Di)-4.93992E-05 453 Name Oxygen Nitrogen Carbon Dioxide Sulfur Dioxide Argon/Oxygen Nitrogen_2 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass_|Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(VU)Coefficient W/m2K (W/m2K) 57.48 80.93 |20.50 |47.05 |25.05 |778.47 |133.35 |122.16 325.11 364.43 |68.92 |1.07 |9.32E-10 |4.18E+04 |0.0146 57.70 81.02 |20.47 |47.61 |25.09 |778.32 |136.16 |120.92 322.60 361.28 |68.24 |1.06 |9.54E-10 |4.19E+04 |0.0144 57.86 81.07 |20.29 |48.10 |25.10 |778.35 |138.21 |120.00 318.46 356.09 |67.19 |1.05 |9.86E-10 |4.20E+04 |0.0143 57.91 81.03 |20.12 |48.44 |24.96 |779.81 |139.90}119.14 317.28 354.63 |66.75 |1.05 |1.00E-09 |4.20E+04 |0.0142 58.04 81.02 |20.13 |48.70 |24.89 |780.65 |141.17 |118.52 318.88 356.62 |67.03 |1.05 |9.93E-10 |4.21E+04 |0.0142 58.12 81.03 |20.15 |48.89 |24.89 |780.59 |141.98 |118.16 319.09 356.88 |67.05 |1.04 |9.92E-10 |4.21E+04 |0.0141 58.11 81.04 |20.18 |48.97 |24.93 |780.14 |142.59 |117.90 318.04 355.57 |66.82 |1.04 |1.00E-09 |4.21E+04 |0.0141 58.12 81.06 |20.25 |49.26 |25.00 |779.44 |143.03 |117.73 318.14 355.70 |66.88 |1.04 |9.96E-10 |4.21E+04 |0.0141 57.98 80.98 |20.25 |49.01 |24.96 |779.71 |142.57 |117.80 318.28 355.86 |66.91 |1.04 |9.95E-10 |4.20E+04 |0.0141 57.85 80.94 |20.25 |48.80 |24.94 |779.86 |141.54 |118.22 318.78 356.49 |67.05 |1.04 |9.90E-10 |4.19E+04 |0.0141 57.90 80.96 |20.30 |49.00 |24.96 |779.67 |141.69 |118.18 319.89 357.88 |67.32 |1.04 |9.80E-10 |4.20E+04 |0.0141 57.92 81.01 |20.26 |48.53 |24.98 |779.55 |140.20 |118.98 319.50 357.40 |67.29 |1.05 |9.84E-10 |4.20E+04 |0.0142 Red Data is an average of all data points. CO,/Argon Run 47: Heat Exchanger Composition -10.63 Argon,83.88 Carbon Dioxide,4.10 Nitrogen Date -04 August 2008 Notebook Page -154 Front Page - 454 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Water Flow Rate -0.598 kg/min (0.009967 kg/s) Pressure Gauge -755 psi Pressure Transducer -815 psi Gas Inlet Temperature -120°C (248 °F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater-0.000282474 Total Volume of System -0.00334 m2 Mass Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(CC)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(VU).Coefficient W/m2K (W/m2K) 31.96 56.32 |20.23 |33.20 |21.59 |176.55 |120.58 85.04 116.23 120.90 |46.20 |0.96 |1.58E-09 |2.54E+04 |0.0110 32.24 56.51 |20.31 |33.17 |21.66 |177.76 |119.71 85.64 117.75 122.54 |46.70 |0.96 |1.54E-09 |2.56E+04 |0.0111 32.11 56.46 |20.36 |33.32 |21.73 |177.08 |120.47 85.32 116.69 121.40 |46.33 |0.96 |1.57E-09 |2.55E+04 |0.0110 32.07 56.39 |20.40 |33.51 |21.80 |176.22 |121.35 84.91 115.90 120.54 |46.09 |0.95 |1.59E-09 |2.55E+04 |0.0110 31.55 56.17 |20.44 |32.89 |21.81 |174.46 |117.96 85.65 113.59 118.04 |45.57 |0.96 |1.60E-09 |2.51E+04 |0.0111 32.10 56.47 |20.50 |33.04 |21.89 |176.40 |117.57 86.28 115.89 120.52 |46.28 |0.96 |1.55E-09 |2.56E+04 |0.0111 32.23 56.52 |20.54 |33.62 |21.94 |176.60 |120.56 85.38 116.34 121.01 |46.28 |0.96 |1.57E-09 |2.56E+04 |0.0110 31.84 56.29 |20.55 |33.63 |21.95 |174.81 |121.32 84.75 114.47 118.99 |45.72 |0.95 |1.61E-09 |2.53E+04 |0.0110 32.14 56.45 |20.53 |33.59 |21.95 |176.01 |120.24 85.37 115.59 120.20 |46.07 |0.96 |1.58E-09 |2.55E+04 |0.0110 32.03 56.39 |20.53 |33.71 |21.92 |175.72 |120.80 85.09 115.75 120.38 |46.14 |0.95 |1.58E-09 |2.54E+04 |0.0110 455 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(VU)Coefficient W/m2K (W/m2K) 31.94 56.28 |20.52 |33.80 |21.89 |174.94 |121.57 84.64 115.67 120.28 |46.18 |0.95 |1.58E-09 |2.54E+04 |0.0110 31.66 56.20 |20.52 |33.25 |21.87 |174.46 |118.63 85.48 114.63 119.16 |45.97 |0.96 |1.57E-09 |2.52E+04 |0.0111 31.96 56.30 |20.54 |33.53 |21.84 |175.30 |119.31 85.41 117.17 121.91 |46.87 |0.96 |1.51E-09 |2.54E+04 |0.0110 31.59 56.15 |20.62 |33.28 |21.83 |174.26 |118.56 85.41 117.26 122.01 |47.10 |0.96 |1.49E-09 |2.52E+04 |0.0111 31.94 56.29 |20.58 |33.59 |21.82 |175.34 |119.19 85.44 118.70 123.56 |47.50 |0.96 |1.47E-09 |2.54E+04 |0.0110 31.89 $6.27 |20.53 |33.49 |21.78 |175.31 |119.39 85.33 118.08 122.89 |47.23 |0.96 |1.49E-09 |2.54E+04 |0.0110 31.90 56.21 |20.47 |33.57 |21.81 |174.78 j 120.55 84.87 116.08 120.73 |46.42 |0.95 |1.55E-09 |2.54E+04 |0.0110 32.05 $6.34 |20.39 |33.21 |21.81 |175.74 |120.14 85.21 115.06 119.63 |45.88 |0.96 |1.60E-09 |2.55E+04 |0.0110 31.96 $6.33 |20.48 |33.41 |21.83 |175.65 |119.88 85.29 116.16 120.82 |46.36 |0.96 |1.56E-09 |2.54E+04 |0.0110 Red Data is an average of all data points. CO/Argon Run 48: Heat Exchanger Composition -10.63 Argon,83.88 Carbon Dioxide,4.10 Nitrogen Date -05 August 2008 Notebook Page -154 Front Page - Water Flow Rate -0.528 kg/min (0.0088 kg/s) Pressure Gauge -725 psi Pressure Transducer 783 psi Gas Inlet Temperature -205°C (401°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) 456 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 457 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass_|Pressure |Water |Water |Gas Gas Out |GasIn |GasIn |Total Heat }Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(U)Coefficient W/m2K (W/m2K) 13.90 31.04 |19.30 |23.69 |20.57 68.81 |122.99 44.06 35.75 36.18 |17.71 |0.84 |8.60E-09 |1.16E+04 |0.0067 13.66 30.93 |19.34 |23.45 |20.58 68.51 |120.34 44.27 35.11 35.52 |17.48 |0.84 |8.68E-09 |1.14E+04 |0.0067 13.89 31.19 |19.44 |23.46 |20.61 69.22 |117.62 45.04 36.07 36.50 |18.03 |0.84 |8.03E-09 |1.16E+04 |0.0068 14.13 31.27 |19.52 |23.72 |20.67 69.41 |119.26 44.93 37.02 37.48 |18.45 |0.84 |7.74E-09 |1.18E+04 |0.0068 14.06 31.15 |19.58 |23.87 |20.69 69.08 |122.07 44.36 37.21 37.68 |18.47 |0.84 |7.85E-09 |1.17E+04 |0.0067 13.81 30.98 |19.62 |23.83 |20.71 68.59 |122.32 44.07 36.63 37.08 |18.18 |0.84 |8.10E-09 |1.15E+04 |0.0067 13.77 31.06 |19.63 |23.70 |20.73 68.79 |119.89 44.52 36.36 36.80 |18.11 |0.84 |8.04E-09 |1.1SE+04 |0.0068 14.07 31.26 |19.58 |23.79 |20.71 69.37 |119.39 44.90 36.96 37.42 |18.42 |0.84 |7.76E-09 |1.17E+04 |0.0068 14.11 31.19 |19.54 |23.91 |20.68 69.19 |122.15 44.40 37.25 37.71 |18.48 |0.84 |7.85E-09 |1.17E+04 |0.0067 13.93 31.03 |19.46 |23.86 |20.64 68.77 |123.43 43.99 36.48 36.93 |18.06 |0.84 |8.27E-09 |1.16E+04 |0.0067 13.71 30.91 |19.28 |23.58 |20.59 68.44 |121.67 44.04 34.91 35.32 |17.34 |0.84 |8.89E-09 |1.14E+04 |0.0067 13.90 31.13 |19.15 |23.39 |20.48 69.10 |119.19 44.72 35.21 35.62 |17.55 |0.84 |8.58E-09 |1.16E+04 |0.0068 14.13 31.19 |19.17 |23.49 |20.39 69.34 |120.52 44.64 36.68 37.13 |18.25 |0.84 |8.00E-09 |1.18E+04 |0.0067 14.06 31.08 |19.27 |23.63 |20.41 69.00 |122.74 44.15 37.12 37.58 |18.41 |0.84 |7.96E-09 |1.17E+04 |0.0067 13.84 30.92 |19.39 |23.62 |20.51 68.50 |122.81 43.90 36.61 37.06 |18.16 |0.84 |8.15E-09 }1.15E+04 |0.0067 13.71 30.91 |19.44 |23.55 |20.60 68.44 |120.57 44,20 35.77 36.20 }17.81 |0.84 |8.36E-09 }1.14E+04 |0.0067 13.92 31.08 |19.42 |23.66 |20.60 68.91 |121.06 44.39 36.32 36.76 |18.06 |0.84 |8.18E-09 |1.16E+04 |0.0067 Red Data is an average of all data points. 458 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO,/Argon Run 49: Heat Exchanger Composition -10.63 Argon,83.88 Carbon Dioxide,4.10 Nitrogen Date -05 August 2008 Notebook Page 154 Front Page - Water Flow Rate -0.722 kg/min (0.012033 kg/s) Pressure Gauge -425 psi Pressure Transducer -453 psi Gas Inlet Temperature -120°C (248°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2KwIn(Do/Di)-4.93992E-05 (Di/Do)/hwater-0.000282474 Total Volume of System -0.00334 m2 Mass Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(U)Coefficient W/m2K (W/m2K) 31.75 53.96 |19.46 |43.55 |21.15 |161.16 |211.44 61.59 109.67 113.81 |40.52 |0.84 |2.59E-09 |2.32E+04 |0.0085 31.46 53.68 |19.44 |42.89 |21.04 |159.63 |207.33 61.89 109.42 113.54 |40.79 |0.84 |2.54E-09 |2.31E+04 |0.0085 31.43 53.69 |19.55 |42.17 |21.03 |159.80 |201.51 62.84 110.76 114.99 |41.60 |0.84 |2.41E-09 |2.32E+04 |0.0086 31.52 53.78 |19.66 |42.25 |21.10 |160.16 |201.04 63.03 111.93 116.24 |42.04 |0.84 |2.35E-09 |2.32E+04 |0.0087 31.61 53.88 |19.75 |42.88 |21.22 |160.42 |203.66 62.72 111.99 116.31 |41.91 |0.84 |2.38E-09 |2.32E+04 |0.0086 459 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |GasIn |GasIn |Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density }|(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(Ib/hr)(VU)Coefficient W/m2K (W/m2K) 31.68 53.96 |19.78 |43.62 |21.30 |160.67 |206.93 62.30 111.66 115.96 |41.58 |0.84 |2.43E-09 |2.32E+04 |0.0086 31.77 53.99 |19.86 |43.99 |21.37]160.65 |210.07]61.84 112.31 116.66 |41.67 |0.84 |2.43E-09 |2.32E+04 |0.0085 31.69 53.95 |19.90 |44.07 |21.46]160.14 |210.48 61.73 111.20 115.46 |41.28 |0.84 |2.48E-09 |2.31E+04 |0.0085 31.66 53.98 |19.91 |44.07 |21.45 |160.34 |210.10 61.83 111.35 115.62 |41.34 |0.84 |2.47E-09 |2.31E+04 |0.0085 31.71 53.98 |19.92 |44.15 |21.45 |160.35 |211.28]61.65 111.68 115.98 |41.40 |0.84 |2.47E-09 |2.31E+04 |0.0085 31.60 53.86 |19.76 |43.99 |21.44 |159.58 |210.26 61.65 108.94 113.03 |40.48 |0.84 |2.58E-09 |2.31E+04 |0.0085 31.57 53.84 |19.68 |43.65 |21.34]159.79 |208.28 61.94 109.16 113.26 |40.64 |0.84 |2.55E-09 |2.31E+04 |0.0085 31.59 53.86 |19.70 |43.59 |21.27 |160.13 |208.91 61.87 110.61 114.83 |41.13 |0.84 |2.50E-09 |2.31E+04 |0.0085 31.67 53.89 |19.63 |43.72 |21.27 |160.29 |210.03 61.73 109.80 113.96 |40.74 |0.84 |2.55E-09 |2.31E+04 |0.0085 31.62 53.88 |19.71 |43.47 |21.28 |160.22 |207.95 |62.04 110.75 114.98 |41.22 |0.84 |2.48E-09 |2.31E+04 |0.0085 Red Data is an average of all data points. CO/Argon Run 50: Heat Exchanger Composition -10.63 Argon,83.88 Carbon Dioxide,4.10 Nitrogen Date -06 August 2008 Notebook Page -153 Front Page- Water Flow Rate -0.492 kg/min (0.0082 kg/s) Pressure Gauge -420 psi Pressure Transducer -447 psi Gas Inlet Temperature -209°C (408.2°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 460 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw--16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass_|Pressure |Water |Water |Gas Gas Out |GasIn |GasIn |Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(CC)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(VU)Coefficient W/m2K (W/m2K) 14.58 30.83 |19.68 |31.22 |20.46 68.28 |208.99 34,75 46.86 47.60 |20.21 |0.79 |9.25E-09 |1.09E+04 |0.0056 14.75 30.86 |19.72 |31.18 |20.41 68.38 |209.96 34.70 48.44 49.23 |20.87 |0.79 |8.71E-09 |1.11E+04 |0.0056 14.57 30.83 |19.73 |31.16 |20.45 68.29 |209.82 34.68 47.50 48.26 |20.47 |0.79 |9.05E-09 }1.09E+04 |0.0056 14.59 30.86 |19.71 |31.21 |20.47 68.36 |209.24 34.76 47.00 47.74 |20.26 |0.79 |9.22E-09 |1.09E+04 |0.0056 14.55 30.82 |19.75 |31.15 |20.46 68.26 |209.11 34.73 47,53 48.29 |20.50 |0.79 |9.00E-09 |1.09E+04 |0.0056 14.56 30.87 }19.82 |31.17 |20.53 68.35 |208.78 34.81 47.57 48.34 |20.53 |0.79 |8.96E-09 |1.09E+04 |0.0056 14.51 30.87 |19.87 |31.34 |20.61 68.33 |209.50 34.76 47.11 47.85 |20.30 |0.79 |9.18E-09 |1.09E+04 |0.0056 14.63 30.81 |19.89 |31.42 |20.59 68.17 |209.63 34.68 47.92 48.70 |20.66 |0.79 |8.86E-09 |1.10E+04 |0.0056 14.50 30.86 |19.92 |31.32 |20.61 68.28 |208.58 34.81 47.55 48.31 |20.52 |0.79 |8.95E-09 |1.09E+04 |0.0056 14.56 30.83 |19.87 |31.38 |20.64 68.21 |208.65 34.78 46.87 47.61 |20.23 |0.79 |9.22E-09 |1.09E+04 |0.0056 14.54 30.83 |19.55 |31.38 |20.55 68.24 |208.86 34.76 44.66 45.33 |19.25 |0.79 |1.02E-08 |1.09E+04 |0.0056 14.55 30.82 |19.40 |31.26 |20.41 68.28 |208.55 34.77 44.57 45.24 |19.23 |0.79 |1.02E-08 |1.09E+04 |0.0056 14.64 30.82 |19.46 |31.09 |20.28 68.34 |208.71 34.76 46.63 47.36 |20.12 |0.79 |9.34E-09 |1.10E+04 |0.0056 14.64 30.74 |19.50 |31.14 |20.29 68.09 |209.19 34.62 46.97 47.71 |20.26 |0.79 |9.22E-09 |1.10E+04 |0.0056 14.47 30.76 |19.50 |31.05 |20.33 68.14 |207.70 34.77 45.90 46.61 |19.84 |0.79 |9.57E-09 |1.09E+04 |0.0056 461 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |GasIn |GasIn |Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(Ib/hr)(U)Coefficient W/m2K (W/m2K) 14.44 30.79 |19.54 {31.06 |20.33 68.23 |207.28 34.84 46.14 46.86 |19.95 |0.79 |9.45E-09 |1.09E+04 |0.0056 14.57 30.83 |19.68 |31.22 |20.46 68.26 |208.91 34.75 46.83 47.57 |20.20 |0.79 |9.28E-09 |1.09E+04 |0.0056 Red Data is an average of all data points. CO>2/Argon Run 51: Heat Exchanger Composition -10.63 Argon,83.88 Carbon Dioxide,4.10 Nitrogen Date -06 August 2008 Notebook Page -153 Front Page - Water Flow Rate -0.667 kg/min (0.011117 kg/s) Pressure Gauge -235 psi Pressure Transducer -246 psi Gas Inlet Temperature -126°C (258.8°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 462 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas |Gas Out |GasIn |GasIn |Total Heat |Gas Side Nu |Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer (Ib/hr)(VU)Coefficient W/m2K (W/m2K) 6.32 16.96 |18.99 |21.24 |19.98 33.85 |127.81 23.09 15.48 15.56 |7.96 |0.79 |3.82E-08 |5.30E+03 |0.0042 6.30 16.96 |19.04 |21.33 |20.04 33.84 |127.21 23.13 15.41 15.49 |7.93 |0.79 |3.83E-08 |5.29E+03 |0.0042 6.26 16.97 |19.11 |21.42 |20.10 33.87 |126.40 23.21 15.31 15.39 |7.89 |0.79 |3.84E-08 |5.26E+03 |0.0042 6.18 16.99 |19.12 |21.48 |20.16 33.89 |126.19 23.24 14.95 15.03 |7.71 |0.79 |4.02E-08 |5.19E+03 |0.0043 6.20 16.98 |19.07 |21.40 |20.17 33.86 |126.46 23.20 14.82 14.89 |7.63 |0.79 |4.11E-08 |5.20E+03 |0.0042 6.14 16.96 |19.09 |21.38 }20.17 33.83 |126.61 23.17 14.76 14.83 |7.60 |0.79 |4.15E-08 |5.1SE+03 |0.0042 6.32 16.94 |19.17 |21.45 |20.18 33.78 |126.80 23.13 15.41 15.49 |7.93 |0.79 |3.81E-08 |5.31E+03 |0.0042 6.30 16.90 |19.28 |21.51 |20.20 33.69 |127.05 23.06 15.66 15.74 |8.06 |0.79 |3.69E-08 |5.29E+03 |0.0042 6.24 16.94 |19.40 |21.59 |20.27 33.76 |126.61 23.14 15.67 15.75 |8.07 |0.79 |3.67E-08 |5.24E+03 |0.0042 6.25 16.95 |19.50 |21.66 |20.38 33.78 |125.83 23.21 15.64 15.73 |8.07 |0.79 |3.65E-08 |5.26E+03 |0.0042 6.25 16.98 |19.59 |21.76 |20.52 33.82 |125.56 23.27 15.49 15.57 |7.99 |0.79 |3.71E-08 |5.26E+03 |0.0042 6.25 16.96 |19.22 |21.47 |20.20 33.82 |126.59 23.17 15.33 15.41 |7.89 |0.79 |3.85E-08 |5.25E+03 |0.0042 Red Data is an average of all data points. Heat Exchanger Data Components - Argon Carbon Dioxide GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Carbon Dioxide |81.89579 |81.74692 |81.83607 |81.61676 |81.77389 Argon 15.81165 |15.8174 |15.81537 |15.81413 |15.81464 463 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 GC Run 30: Agilent Cerity QA/QC Report Sample name:0725-HeatXGRArCOO9 Sample note: Submission time:Friday,July 25,2008 9:04:20 AM Operator: Injection date:Friday,July 25,2008 9:10:01 AM GC Description:Mlcro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM 464 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA 4 beeen 4 _-a -Z 7; : aT 1 t i 1 15 2 25 mir TCOZA i || pos i ' i bo a7 | boo i :pb ee of |i '|{!i |:: i : i |}: "UJ Lj T Lj 1 16 2 25 min jc," :a,ae:se 4 i (O°:i :GZ -_-}iEce:{ eB rede be i 'i i :a:[nen 4 eg ||eo 7 _ ce eee copes oo ey i +T --__-T t 4 18 2 25 mir ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 465 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Unknown Signal Retention Time[min]Type Area[!iV's]Amt/Area Amount[mass%]Name 1 1.500 ---Oxygen 1 1.637 ---Nitrogen 2 0.244 BP 2.9489e+005 0.00000e+000 0.00000 2 0.276 VB =1.6561e+006 4.94521e-005 81.89579 Carbon Dioxide 2 1.220 ---Sulfur Dioxide 3 1.346 BB 1.0939e+005 1.44545e-004 15.81165 Argon/Oxygen 3 2.112 ---Nitrogen_2 Total amount =97.70743 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 31: Agilent Cerity QA/QC Report Sample name:0725-HeatXGRArCO010 Sample note: Submission time:Friday,July 25,2008 9:04:21 AM Operator: Injection date:Friday,July 25,2008 9:13:35 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM 466 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA }i t i _t._a on ee _a |i : :i H .aa .'<b t t:i t L ae "+ !it ,. : 16 2 25 min yornnn cee nee p eon -ce eeeee poo i i!H i a : Booed :i .: i poo : ;ek Beebe es fetehen be eee !i ! i i - 18 2 25 min TCDSA 1c ee. ,oe ::mR.::Bel b,4°O°{iEe:i)ie'! Ord a =on (: ReoOiri anne aaa t 7 - T T T 15 2 2.5 min ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 467 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Unknown Signal Retention Time [min]Type Area [!iV*s]Amt(Area Amount [mass%]Name 1 1.500 ---Oxygen 1 1.637 ---Nitrogen 2 0.244 BP 2.9434e+005 0.00000e+000 0.00000 2 0.276 VB 1.6531e+006 4.94521e-005 81.74692 Carbon Dioxide 2 1.220 ---Sulfur Dioxide 3 1.347 BB 1.0943e+005 1.44545e-004 15.81740 Argon/Oxygen 3 2.112 ---Nitrogen_2 Total amount =97.56432 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 32: Agilent Cerity QA/QC Report Sample name:0725-HeatXGRArCOO11 Sample note: Submission time:Friday,July 25,2008 9:04:23 AM Operator: Injection date:Friday,July 25,2008 9:17:09 AM GC Description:Mlcro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM 468 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 {5 "ew v : 1 :o.j !: i a : :"6 i |: i Ene ]| t ¢;:3:"oe :{cock i 7 i i ioe oO . i ¢|| :a:i , a an bo to 3 A co |a : q T T v T 7 ++ s 1 oe 16.2 25 mini ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 469 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Unknown Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount [mass%]Name 1 1.500 ---Oxygen 1 1.637 ---Nitrogen 2 0.244 BP 2.9465e+005 0.00000e+000 0.00000 2 0.276 VB =1.6549e+006 4.94521e-005 81.83607 Carbon Dioxide 2 1.220 ---Sulfur Dioxide 3 1.346 BB 1.0941e+005 1.44545e-004 15.81537 Argon/Oxygen 3 2.112 ---Nitrogen_2 Total amount =97.65144 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated GC Run 33: Agilent Cerity QA/QC Report Sample name:0725-HeatXGRArCOO8 Sample note: Submission time:Friday,July 25,2008 9:04:20 AM Operator: Injection date:Friday,July 25,2008 9:06:28 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM 470 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCD1A 3 Loe |=a J i =.ade nied a a a ss ras Bee.ak fo.5 .J n :| ..::.4 cot 4 $ od:i.bn caine i 7 "4 i : :-4do.ck eee ren .doe La.fee i L +i T T i -S]>-- 06 4 15 2 25 min TCDZ2A >a aes,a . =a 1 =Nx ::..: 'oe :,.: : -aQa :t at FI L ' c.:::: : °:::: -2 i nos i Cy i :' ! o i yo me é |-| 8 J Fa >ee 4 fee peee = %o :i St sn RE RE SRE A ED NRA oo Os 4 15 2 25 min TCDOSA >4 --_wee nee GF wi eee me ae ee be ee eee ee -a : o4 :-7;ee ; tel Ggykeecee7 oo r My T T i T 06 1 15 2 25 __min ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% 471 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sample type:Sample Sampling source:Unknown Signal Retention Time [min]Type Area [!iV's]Amt/Area Amount [mass%]Name 1 1.500 ---Oxygen 1 1.637 ---Nitrogen 2 0.244 BP 2.9387e+005 0.00000e+000 0.00000 2 0.276 VB 1.6504e+006 4.94521e-005 81.61676 Carbon Dioxide 2 1.220 ---Sulfur Dioxide 3 1.346 BB =1.0941e+005 1.44545e-004 15.81413 Argon/Oxygen 3 2.112 ---Nitrogen_2 Total amount =97.43089 Report summary: Warning(s):Calibrated compound(s)not found Warning(s):Sample amount is zero.Absolute amounts calculated CO>/Argon Run 52: Heat Exchanger Composition -15.81 Argon,81.77 Carbon Dioxide Date -17 July 2008 Notebook Page -157 Front Page - Water Flow Rate -0.653 kg/min (0.010883 kg/s) Pressure Gauge -1080 psi Pressure Transducer -1171 psi Gas Inlet Temperature -125°C (257°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2KwIn(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 472 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(CC)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(U)Coefficient W/m2K (W/m2K) 61.90 80.67 |19.27 |43.50 |24.63 |782.63 |121.37 67.76 342.98 387.03 |73.26 |1.12 |8.43E-10 |4.52E+04 |0.0150 62.05 80.79 |19.31 |44.08 |24.74 |781.76 |123.61 67.62 340.52 383.91 |72.66 |1.11 }|8.56E-10 |4.52E+04 |0.0148 62.10 80.86 |19.32 |44.47 |24.81 |781.05 |125.17 67.50 337.93 380.61 |72.04 |1.10 |8.71E-10 |4.53E+04 |0.0147 62.14 80.90 |19.31 |44.77 |24.86 |780.65 |126.08 67.44 336.58 378.90 |71.72 |1.10 |8.79E-10 |4.53E+04 |0.0147 62.13 80.91 |19.32 |44.85 |24.89 |780.33 |126.66 67.38 335.44 377.46 |71.45 |1.10 |8.86E-10 |4.53E+04 |0.0147 62.15 80.88 |19.25 |44.81 |24.86 |780.56 |127.04 67.42 334.12 375.79 |71.11 |1.10 |8.96E-10 |4.53E+04 |0.0146 62.16 80.87 |19.26 |44.91 |24.84 |780.82 |127.25 67.46 334,93 376.82 |71.28 |1.09 |8.91E-10 |4.53E+04 |0.0146 62.10 80.88 |19.34 |44.97 |24.88 |780.32 |127.50 67.38 334.87 376.74 |71.29 |1.09 |8.90E-10 |4.52E+04 |0.0146 62.08 80.86 |19.42 |44.55 |24.91 |780.01 |127.50 67.33 334,52 376.29 |71.24 |1.09 |8.94E-10 |4.52E+04 |0.0146 62.09 80.80 |19.44 |43.95 |24.83 |780.67 |127.69 67.44 334.60 376.40 |71.20 |1.09 |9.00E-10 |4.52E+04 |0.0146 62.05 80.79 |19.45 |43.90 |24.82 |780.77 |127.72 67.45 334.63 376.44 |71.20 |1.09 |9.01E-10 |4.52E+04 |0.0146 62.02 80.75 |19.42 |43.91 |24.82 |780.74 |127.87 67.45 333.83 375.42 |71.01 |1.09 |9.06E-10 |4.52E+04 |0.0146 62.00 80.72 |19.38 |43.93 |24.78 |781.04 |127.92 67.50 333.77 375.35 |70.97 |1.09 |9.06E-10 |4.52E+04 |0.0146 61.95 80.71 |19.44 |44.03 |24.80 |780.81 |127.92 67.46 334.35 376.07 |71.13 |1.09 |9.01E-10 |4.51E+04 |0.0146 61.95 80.74 |19.49 |44.14 |24.86 |780.22 |127.92 67.37 334.40 376.14 |71.18 |1.09 |8.98E-10 |4.51E+04 |0.0146 61.98 80.77 |19.52 |44.28 |24.88 |780.01 |128.42 67.33 334.24 375.95 |71.15 |1.09 }8.99E-10 |4.51E+04 |0.0145 61.99 80.79 |19.53 |44.39 |24.91 |779.81 |128.92 67.30 333.53 375.05 |70.97 |1.09 |9.03E-10 |4.51E+04 |0.0145 62.01 80.78 |19.54 |44.29 |24.89 |780.03 |129.56 67.34 333.09 374.48 |70.83 |1.08 |9.09E-10 |4.52E+04 |0.0145 62.00 80.82 |19.54 |44.79 |24.91 |779.81 |130.08 67.30 333.09 374.49 |70.83 |1.08 |9.06E-10 |4.51E+04 |0.0145 62.05 80.80 |19.40 |44.34 |24.84 |780.63 |127.17 67.43 335.34 377.33 |71.40 |1.09 |8.91E-10 |4.52E+04 |0.0146 Red Data is an average of all data points. 473 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO /Argon Run 53: Heat Exchanger Composition -15.81 Argon,81.77 Carbon Dioxide Date -18 July 2008 Notebook Page -157 Front Page - Water Flow Rate -0.627 kg/min (0.01045 kg/s) Pressure Gauge -1005 psi Pressure Transducer -1084 psi Gas Inlet Temperature -147°C (296.6°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK. Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow _|(bar)In Out Out |Density |(@C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(U)Coefficient W/m2K (W/m2K) 54.98 75.16 |19.32 |46.20 |23.98 |775.70 |148.29 66.61 293.88 325.64 |61.48 |0.99 |1.15E-09 |4.05E+04 |0.0127 54.96 75.11 |19.27 |46.11 |23.94 |776.06 |148.14 66.67 293.84 325.60 |61.46 |0.99 |1.15E-09 |4.05E+04 |0.0127 55.00 75.10 |19.30 |46.11 |23.92 |776.23 |148.31 66.69 294.73 326.68 |61.65 |0.99 |1.14E-09 |4.05E+04 |0.0127 54.97 75.10 |19.31 |46.38 |23.98 |775.53 |148.45 66.58 293.99 325.77 |61.51 |0.99 |1.1SE-09 |4.05E+04 |0.0127 54.90 75.11 |19.31 |46.34 |24.02 |774.96 |148.47 66.49 292.52 323.98 |61.21 |0.99 |1.16E-09 |4.04E+04 |0.0127 474 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass_|Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(C)Density |Transfer Heat Factor Meter (°C)CC)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer (1b/hr)(U)Coefficient W/m2K (W/m2K) 54.89 75.09 |19.36 |46.42 |24.02 |775.00 |148.58 66.50 293.46 325.12 |61.42 |0.99 |1.15E-09 |4.04E+04 |0.0127 54.89 75.09 |19.44 |46.50 |24.01 |775.03 |148.55 66.50 295.17 327.23 |61.82 |0.99 |1.13E-09 |4.04E+04 |0.0127 54.84 75.11 |]19.52 |46.61 |24.11 |773.91 |148.55 66.32 294.54 326.45 |61.74 |0.99 |1.13E-09 |}4.04E+04 |0.0127 54.81 75.10 |19.56 |46.56 |24.17 |773.17 |148.52 66.21 293.87 325.63 |61.64 |0.99 |1.14E-09 |4.04E+04 |0.0127 $4.79 75.10 |19.59 |46.60 |24.20 |772.68 |148.42 66.13 293.73 325.45 |61.64 |0.99 |1.14E-09 |4.03E+04 |0.0127 54.79 75.09 |19.62 |46.63 |24.20 |772.69 |148.41 66.13 294.28 326.13 |61.77 |0.99 |1.13E-09 |4.03E+04 |0.0127 54.69 75.05 |19.56 |46.49 |24.20 |772.62 |148.23 66.12 292.68 324.17 |61.41 |0.99 |1.14E-09 |4.03E+04 |}0.0127 54.65 74.99 |19.50 |46.38 |24.15 |773.09 |147.78 66.19 292.69 324.18 |61.39 |0.99 |1.14E-09 |4.03E+04 |0.0127 54.62 74.94 |19.50 |46.37 |24.09 |773.63 |147.40 66.28 294.10 325.91 |61.70 |0.99 |1.13E-09 |4.03E+04 |0.0127 54.62 74.92 |19.55 |46.27 |24.12 |773.22 |147.09 66.21 294.43 326.31 |61.82 |0.99 |1.13E-09 |4.03E+04 |0.0127 54.56 74.89 |19.46 |46.23 |24.11 |773.24 |146.95 66.22 292.78 324.30 |61.44 |0.99 |1.14E-09 |4.02E+04 |0.0127 54.53 74.85 |19.40 |46.14 |24.06 |773.75 |146.83 66.30 292.58 324.04 |61.36 |0.99 |1.14E-09 |4.02E+04 |0.0127 54.50 74.80 |19.39 |46.11 |24.00 |774.42 |146.78 66.40 293.59 325.29 |61.56 |0.99 |1.14E-09 |4.02E+04 |0.0127 54.49 74.77 |19.31 |45.94 |23.97 |774.72 |146.79 66.45 292.32 323.73 |61.25 |0.99 |1.15E-09 |4.02E+04 |0.0127 54.76 75.02 |19.44 |46.34 |24.07 |774.19 |147.92 66.37 293.64 325.35 |61.54 |0.99 |1.14E-09 |4.04E+04 |0.0127 Red Data is an average of all data points. CO,/Argon Run 54: Heat Exchanger Composition -15.81 Argon,81.77 Carbon Dioxide Date -18 July 2008 Notebook Page -157 475 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Front Page - Water Flow Rate -0.627 kg/min (0.01045 kg/s) Pressure Gauge -820 psi Pressure Transducer -885 psi Gas Inlet Temperature -190°C (374°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(U)Coefficient W/m2K (W/m2K) 39.62 60.89 |19.34 |43.28 |22.00 |754.63 |187.87 63.26 217.74 234.70 |44.23 |0.87 |2.17E-09 |2.92E+04 |0.0097 39.61 60.90 |19.45 |43.33 |22.07 |753.42 |188.36 63.07 217.90 234.88 |44.29 |0.87 |2.17E-09 |2.92E+04 |0.0097 39.59 60.90 |19.46 |43.43 |22.10 |752.92 |188.54 63.00 217.40 234.31 |44.20 |0.87 |2.18E-09 |2.92E+04 |0.0097 39.59 60.89 |19.43 |43.49 |22.11 |752.72 |188.77 62.97 216.67 233.46 |44.04 |0.87 |2.19E-09 |2.92E+04 |0.0097 39.57 60.88 |19.46 |43.43 |22.11 |752.75 |188.97 62.97 216.97 233.81 |44.10 |0.87 |2.19E-09 |2.92E+04 |0.0096 39.57 60.89 |19.60 |43.56 |22.15 |751.95 |189.10 62.85 218.67 235.78 |44.49 |0.87 |2.15E-09 |2.92E+04 |0.0096 39.54 60.91 |19.67 |43.72 |22.25 |750.30 |189.33 62.61 217.79 234.75 |44.34 |0.87 |2.16E-09 |2.91E+04 |0.0096 39.54 60.93 |19.66 |43.77 |22.31 |749.34 ]189.73 62.46 216.35 233.08 |44.04 |0.87 |2.19E-09 |2.91E+04 |0.0096 39.52 60.98 |19.88 }|44.05 |22.56 |744.85 |190.27 61.80 215.03 231.56 |43.87 |0.87 |2.21E-09 |2.91E+04 |0.0096 476 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer (Ib/hr)(U)Coefficient W/m2K (W/m2K) 39.50 61.05 |20.06 |44.23 |22.70 |742.40 |190.80 61.44 215.20 231.76 |43.96 |0.87 |2.20E-09 |2.90E+04 |0.0096 39.51 61.01 |19.91 |43.65 |22.65 |743.26 |191.20 61.57 212.65 228.80 |43.36 |0.87 |2.27E-09 |2.90E+04 |0.0096 39.53 60.97 |19.88 |43.10 |22.49 |746.09 |191.47 61.98 214.82 231.31 |43.75 |0.87 |2.24E-09 |2.90E+04 |0.0096 39.51 60.95 |19.88 |42.96 |22.48 |746.15 |191.59 61.99 214.71 231.18 |43.72 |0.87 |2.25E-09 |2.90E+04 |0.0096 39.55 60.93 |19.67 |43.54 |22.31 |749.29 |189.69 62.46 216.30 233.03 |44.03 |0.87 |2.20E-09 |2.91E+04 |0.0096 Red Data is an average of all data points. 477 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO./Argon Run 55: Heat Exchanger Composition -15.81 Argon,81.77 Carbon Dioxide Date -21 July 2008 Notebook Page -156 Front Page - Water Flow Rate -0.697 kg/min (0.011617 kg/s) Pressure Gauge -600 psi Pressure Transducer -641 psi Gas Inlet Temperature -120°C (248°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater-0.000282474 Total Volume of System -0.00334 m2 Mass Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(U)Coefficient W/m2K (W/m2K) 22.99 44.10 |19.76 |27.39 |21.26 |111.60 |121.83 16.09 65.63 67.09 |30.33 |0.89 |3.32E-09 |1.87E+04 |0.0089 23.25 44,26 |19.67 |27.49 |21.23 |112.27 |122.48 16.11 65.96 67.43 |30.41 |0.89 |3.32E-09 |1.89E+04 |0.0089 22.94 44.01 |19.63 |27.39 |21.15 |111.37 |123.43 16.08 65.35 66.80 |30.14 |0.89 |3.39E-09 |1.87E+04 |0.0088 22.99 44.12 |19.66 |27.11 |21.10 |111.86 |121.00 16.09 66.20 67.69 |30.62 |0.89 |3.25E-09 |1.88E+04 |0.0089 23.16 44.15 |19.75 |27.37 |21.18 |111.90 |122.29 16.10 66.94 68.47 |30.91 |0.89 |3.21E-09 |1.89E+04 |0.0088 478 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|}(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(U)Coefficient W/m2K (W/m2K) 22.75 43.89 |19.84 |27.30 |21.28 |110.76 |121.95 16.08 65.32 66.77 |30.23 |0.89 |3.33E-09 |1.86E+04 |0.0088 22.97 44.11 |19.89 |27.17 |21.35 |111.56 |119.25 16.10 65.65 67.11 |30.46 |0.89 |3.25E-09 |1.88E+04 |0.0089 23.08 44.10 |19.79 |27.49 |21.36 |111.50 |121.40 16.10 65.15 66.59 |30.12 |0.89 |3.35E-09 |1.88E+04 |0.0089 22.70 43.84 |19.70 |27.19 |21.29 |110.56 |121.09 16.07 63.64 65.01 |29.48 |0.89 |3.49E-09 |1.85E+04 |0.0088 22.99 44.09 |19.77 |27.04 |21.30 |111.53 |118.89 16.09 64.95 66.38 |30.14 |0.89 |3.31E-09 |1.88E+04 |0.0089 23.02 44.04 |19.84 |27.46 |21.34 |111.26 |121.49 16.09 65.55 67.00 |30.32 |0.89 |3.31E-09 |1.88E+04 |0.0088 22.49 43.71 |19.86 |27.36 |21.39 |109.93 {|120.61 16.07 63.41 64.77 |29.43 |0.89 |3.48E-09 |1.84E+04 |0.0088 21.94 43.47 |19.60 |26.66 |21.33 |109.07 |114.48 16.05 59.47 60.66 |27.88 |0.90 |3.76E-09 |1.81E+04 |0.0090 22.61 43.85 |19.58 |26.39 |21.19 |110.72 |110.96 16.07 62.30 63.62 |29.30 |0.91 |3.35E-09 |1.87E+04 |0.0091 22.99 43.97 |19.65 |26.93 |21.17 |111.21 |115.62 16.08 64.84 66.27 |30.27 |0.90 |3.22E-09 |1.89E+04 |0.0090 22.61 43.70 |19.74 |26.89 |21.25 |110.05 |118.77 16.06 63.72 65.10 |29.66 |0.89 |3.40E-09 |1.85E+04 |0.0089 22.08 43.48 |19.73 |26.27 |21.32 |109.11 |115.07 16.05 60.75 62.00 |28.47 |0.90 |3.63E-09 |1.82E+04 |0.0089 22.67 43.85 |19.51 |26.16 |21.38 |110.50 |112.31 16.08 60.17 61.39 |28.22 |0.90 |3.66E-09 |1.87E+04 |0.0090 22.97 43.90 |19.06 |26.54 |21.23 |110.87 |117.21 16.08 59.41 60.60 |27.63 |0.90 |3.94E-09 |1.88E+04 |0.0089 22.80 43.93 |19.69 |27.03 |21.27 |110.93 |118.95 16.08 63.92 65.30 |29.69 |0.89 |3.42E-09 |1.87E+04 |0.0089 Red Data is an average of all data points. CO,/Argon Run 56: Heat Exchanger Composition -15.81 Argon,81.77 Carbon Dioxide Date -22 July 2008 Notebook Page -156 Front Page - Water Flow Rate -0.52 kg/min (0.008667 kg/s) 479 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Pressure Gauge -575 psi Pressure Transducer -615 psi Gas Inlet Temperature -210°C (410°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater-0.000282474 Total Volume of System -0.00334 m2 Mass Pressure |Water |Water |Gas Gas Out |Gas In j Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)(kg/m3)(kg/m3)|Coefficient |Transfer(tb/hr)(U)Coefficient W/m2K (W/m2K) 23.53 42.58 |20.20 |36.68 |21.73 |105.24 |210.70 15.99 72.53 74.32 |29.73 |0.81 |4.57E-09 |1.74E+04 |0.0070 23.55 42.63 |20.05 |36.47 |21.68 |105.49 |206.81 15.99 71.53 73.26 |29.47 |0.81 |4.61E-09 |1.75E+04 |0.0071 23.63 42.72 |20.11 |36.50 |21.64 |105.87 |207.97 16.00 72.83 74.63 |29.95 |0.81 |4.48E-09 |1.75E+04 |0.0071 23.69 42.81 |19.94 |37.02 |21.65 |106.19 |211.64 16.01 71.64 73.39 |29.28 |0.81 |4.73E-09 |1.75E+04 |0.0071 23.79 42.74 |19.36 |37.41 |21.39 |106.21 }215.93 15.99 69.79 71.44 |28.33 |0.81 |5.11E-09 |1.75E+04 |0.0070 23.72 42.64 |19.33 |36.93 ]21.03 |106.20 |216.23 15.98 72.18 73.95 |29.32 |0.81 |4.78E-09 |1.75E+04 |0.0070 23.76 42.67 |19.05 |37.52 |20.92 |106.44 |215.78 15.98 71.14 72.86 |28.90 |0.81 |4.91E-09 |1.75E+04 |0.0070 23.84 42.66 |18.80 |37.71 |20.70 |106.63 |217.18 15.97 71.46 73.20 |28.97 |0.81 |4.90E-09 |1.75E+04 |0.0070 23.72 42.54 |18.93 |37.55 |20.60 |106.27 |217.32 15.96 72.88 74.69 |29.58 |0.81 |4.70E-09 |1.74E+04 |0.0070 23.73 42.58 |19.04 |37.48 |20.66 |106.36 |215.75 15.96 73.39 75.22 |29.85 |0.81 |4.59E-09 |1.75E+04 |0.0070 23.81 42.64 |19.22 |37.69 |20.73 |106.53 |216.59 15.97 74.66 76.56 |30.33 |0.81 |4.45E-09 |1.75E+04 |0.0070 480 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow }(bar)In Out Out Density |(CC)Density |Transfer Heat Factor Meter (°C)(°C)(°C)(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(U)Coefficient W/m2K (W/m2K) 23.74 42.50 |19.44 |37.82 |20.83 |105.89 |217.28 15.96 75.68 77.63 |30.76 |0.81 |4.33E-09 |1.75E+04 |0.0069 23.44 42.23 |19.51 |37.24 |20.97 |104.72 |211.27 15.94 73.42 75.25 |30.13 |0.81 |4.44E-09 |1.74E+04 |0.0070 23.32 42.26 |19.54 }36.51 |21.10 |104.69 }202.79 15.95 71.55 73.29 |29.70 |0.81 |4.47E-09 |1.74E+04 |0.0071 23.39 42.37 1 19.60 |36.45 |21.07 |105.13 |200.55 15.96 72.70 74.50 |30.27 |0.82 |4.28E-09 |1.75E+04 |0.0071 23.46 42.44 |19.62 |36.66 |21.11 |105.36 |201.41 15.96 72.69 74.48 |30.22 |0.82 |4.30E-09 |1.75E+04 |0.0071 23.63 42.56 |19.48 |37.10 |21.11 |105.83 |211.57 15.97 72.50 74.29 |29.68 |0.81 |4.60E-09 |1.75E+04 |0.0070 Red Data is an average of all data points. CO,/Argon Run 57: Heat Exchanger Composition -15.81 Argon,81.77 Carbon Dioxide Date -22 July 2008 Notebook Page -156 Front Page - Water Flow Rate -0.538 kg/min (0.008967 kg/s) Pressure Gauge -410 psi Pressure Transducer -436 psi Gas Inlet Temperature -120°C (248°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 481 Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(VU)Coefficient W/m2K (W/m2K) 13.26 30.00 |19.41 |24.92 |20.91 65.76 |121.40 15.30 32.76 33.12 |16.33 |0.83 |9.77E-09 |1.11E+04 |0.0065 13.67 30.19 |19.52 |25.07 |20.92 66.29 |121.01 15.31 34.36 34.76 |17.14 |0.84 |8.85E-09 |1.14E+04 |0.0065 13.67 30.13 |19.58 |25.37 |20.98 66.10 |123.22 15.31 34.50 34.90 |17.14 |0.83 |8.94E-09 |1.14E+04 |0.0065 13.30 29.98 |19.45 |25.40 |20.99 65.68 |124.33 15.31 32.89 33.26 |16.31 |0.83 |9.94E-09 |1.10E+04 |0.0065 13.04 29.80 |19.49 |25.09 |21.01 65.18 |122.55 15.30 32.16 32.51 |16.01 |0.83 |1.02E-08 |1.09E+04 |0.0065 12.91 29.79 |19.60 |24.84 |21.06 65.12 |118.52 15.30 31.80 32.14 |15.94 |0.84 |1.00E-08 |1.08E+04 |0.0066 13.19 30.07 |19.71 |25.17 |21.10 65.87 |116.14 15.32 32.85 33.21 |16.53 |0.84 |9.16E-09 |1.11E+04 |0.0066 13.40 30.13 |19.80 |25.63 |21.13 66.03 |118.36 15.32 34.01 34.40 |17.04 |0.84 |8.71E-09 |1.12E+04 |0.0066 13.33 30.02 |19.79 |25.91 |21.14 65.73 |121.64 15.32 33.89 34.28 |16.89 |0.83 |9.04E-09 |1.11E+04 |0.0065 13.26 30.03 |19.74 |25.89 |21.20 65.74 |122.39 15.32 33.21 33.58 |16.52 }0.83 |9.51E-09 |1.10E+04 |0.0065 13.60 30.19 |19.78 |25.86 |21.22 66.14 |123.09 15.32 34.20 34.60 |16.99 |0.83 |9.06E-09 |1.13E+04 |0.0065 13.60 30.10 |19.85 |26.03 |21.25 65.88 |125.04 15.32 34.50 34.90 |17.09 |0.83 |9.04E-09 |1.13E+04 |0.0065 13.24 29.94 |19.91 |25.94 |21.30 65.44 |125.26 15.32 33.61 33.99 |16.65 |0.83 |9.53E-09 |1.10E+04 |0.0065 13.00 29.79 |19.90 |25.76 |21.34 65.00 |123.17 15.32 32.47 32.82 |16.14 |0.83 |9.99E-09 |1.08E+04 |0.0065 13.32 30.01 |19.68 |25.49 |21.11 65.71 |121.87 15.31 33.37 33.75 |16.62 |0.83 |9.41E-09 |1.11E+04 |0.0065 Red Data is an average of all data points. 482 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO,/Argon Run 58: Heat Exchanger Composition -15.81 Argon,81.77 Carbon Dioxide Date -23 July 2008 Notebook Page -156 Front Page - Water Flow Rate -0.564 kg/min (0.0094 kg/s) Pressure Gauge -405 psi Pressure Transducer -430 psi Gas Inlet Temperature -210°C (410°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass j Pressure |Water |Water |Gas Gas Out |GasIn |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)|CC)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(VU)Coefficient W/m2K (W/m2K) 14.59 29.66 |19.99 |31.28 |21.06 64.78 |208.63 15.30 43.81 44.46 |18.96 |0.79 |1.04E-08 |1.10E+04 |0.0054 14.54 29.72 |19.85 |31.11 |21.04 64.93 |207.09 15.30 42.67 43.28 |18.50 |0.79 |1.09E-08 |1.09E+04 |0.0054 14.55 29.78 |19.78 |31.08 |20.98 65.14 |208.00 15.30 42.71 43.32 |18.49 |0.79 |1.10E-08 |1.09E+04 j}0.0054 483 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass_|Pressure |Water |Water |Gas Gas Out |GasIn |GasIn |Total Heat |Gas Side Nu Pr Gr Re Friction Flow |(bar)In Out Out Density |(CC)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(Ib/hr)(U)Coefficient W/m2K (W/m2K) 14.62 29.73 |19.70 |31.24 |20.96 65.00 |211.40 15.30 42.65 43.26 |18.36 |0.79 |1.12E-08 |1.09E+04 |0.0054 14.56 29.73 |19.58 |31.20 |20.93 65.03 |212.40 15.30 41.93 42.52 |18.02 |0.79 |1.17E-08 |1.09E+04 |0.0054 14.57 29.79 |19.58 |31.17 |20.91 65.20 |212.75 15.30 42.12 42.72 |18.09 |0.79 |1.16E-08 |1.09E+04 |0.0054 14.63 29.71 |19.63 |31.26 |20.92 64.96 |214.27 15.29 42.59 43.20 |18.26 |0.78 |1.15E-08 |1.09E+04 |0.0054 14.58 29.63 |19.64 |31.23 |20.94 64.73 |213.08 15.29 42.30 42.91 |18.17 |0.78 |1.15E-08 |1.09E+04 |0.0054 14.51 29.69 |19.68 |31.43 |20.99 64.88 |210.49 15.30 42.02 42.61 |18.12 |0.79 |1.1SE-08 |1.09E+04 |0.0054 14,52 29.77 |19.72 |31.50 |21.01 65.09 |210.36 15.30 42.16 42.76 |18.18 |0.79 |1.14E-08 |1.09E+04 |0.0054 14.59 29.70 |19.78 |31.77 |21.04 64.88 |212.68 15.30 42.70 43.31 |18.35 |0.78 |1.12E-08 |1.09E+04 |0.0054 14.56 29.61 |19.82 |31.72 |21.04 64.63 |212.11 15.30 42.83 43.44 |18.43 |0.78 |L.11E-08 |1.09E+04 |0.0054 14.50 29.65 |19.83 |31.59 |21.05 64.75 |209.58 15.30 42,52 43.13 |18.36 |0.79 |1.11E-08 |1.09E+04 |0.0054 14.50 29.73 |19.88 |31.55 |21.05 64.96 |209.12 15.30 42.86 43.48 |18.52 |0.79 |1.09E-08 |1.09E+04 |0.0054 14.57 29.70 |19.92 |31.36 |21.07 64.86 |211.11 15.30 43.16 43.79 |18.60 |0.79 |1.09E-08 |1.09E+04 |0.0054 14.52 29.66 |19.95 |31.36 |21.06 64.75 |211.85 15.30 43,39 44.02 |18.68 |0.79 |1.08E-08 |1.09E+04 |0.0054 14.50 29.72 |19.97 |31.33 }21.06 64.93 }212.13 15.30 43.47 44.11 }18.70 |0.79 |1.08E-08 |1.09E+04 |0.0054 14.55 29.70 |19.78 |31.36 |21.01 64.91 |211.00 15.30 42.70 43.31 |18.40 |0.79 |1.12E-08 |1.09E+04 |0.0054 Red Data is an average of all data points. 484 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 CO,/Argon Run 59: Heat Exchanger Composition -15.81 Argon,81.77 Carbon Dioxide Date -24 July 2008 Notebook Page -156 Front Page - Water Flow Rate -0.602 kg/min (0.010033 kg/s) Pressure Gauge -235 psi Pressure Transducer -245 psi Gas Inlet Temperature -175°C (347°F) Averaged Data -5 Minutes HX Transfer Area -0.24 m2 HX Water-side Heat Transfer Coefficient -0.15 BTU/ftzsR (3066.27 W/m2K) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater -0.000282474 Total Volume of System -0.00334 m2 Mass Pressure Water Water Gas Gas Out Gas In GasIn |Total Heat |Gas Side Nu_|Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(CC)|CC)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(U)Coefficient W/m2K (W/m2K) 6.83 16.84 |19.29 |23.40 |20.85 33.45 |175.73 14.94 16.61 16.70 |7.81 }0.77 |S.11E-08 |5.38E+03 |0.0038 6.74 16.88 |19.39 |23.39 |20.98 33.51 |173.74 14.95 16.27 16.35 |7.67 |0.77 |5.25E-08 |5.33E+03 |0.0038 6.70 16.91 |19.35 |23.36 |20.95 33.60 |171.76 14.95 16.10 16.18 |7.62 |0.77 |5.28E-08 |5.30E+03 |0.0038 6.72 16.94 |19.33 |23.32 |20.94 33.66 |171.15 14.95 16.12 16.20 |7.64 |0.77 |5.24E-08 |5.33E+03 |0.0038 485 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |Gas In }Gas In Total Heat |Gas Side Nu |Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(lb/hr)(VU)Coefficient W/m2K (W/m2K) 6.76 16.93 |19.39 |23.37 |20.95 33.65 |171.59 14.95 16.30 16.39 |7.72 |0.77 |5.14E-08 |5.35E+03 |0.0038 6.76 16.97 |19.48 |23.44 |21.03 33.72 |172.76 14.95 16.39 16.48 |7.74 |0.77 |5.13E-08 |5.34E+03 |0.0038 6.82 16.93 |19.56 |23.55 |21.09 33.63 |173.88 14.95 16.60 16.69 |7.83 |0.77 |5.04E-08 |5.38E+03 |0.0038 6.84 16.87 |19.65 |23.65 |21.15 33.48 |174.79 14.95 16.74 16.83 |7.88 |0.77 |4.99E-08 |5.40E+03 |0.0038 6.75 16.88 |19.64 |23.67 |21.19 33.48 |174.54 14.96 16.40 16.49 |7.72 |0.77 |5.18E-08 |5.33E+03 |0.0038 6.68 16.91 |19.59 |23.61 |21.18 33.55 |173.03 14.96 16.08 16.17 |7.59 |0.77 |5.33E-08 |5.28E+03 |0.0038 6.66 16.93 |19.47 |23.52 |21.13 33.61 |171.82 14,95 15.87 15.96 |7.51 |0.77 |5.43E-08 |5.27E+03 |0.0039 6.75 16.89 |19.27 |23.39 |21.05 33.54 |172.01 14.95 15.85 15.93 |7.50 |0.77 |5.46E-08 |5.34E+03 |0.0038 6.79 16.83 |19.17 |23.17 |20.95 33.41 |172.41 14.94 15.95 16.04 |7.54 |0.77 |5.41E-08 |5.38E+03 |0.0038 6.77 16.76 |19.14 |23.05 |20.86 33.27 |171.98 14.94 16.01 16.09 |7.58 |0.77 |5.35E-08 |5.37E+03 |0.0038 6.67 16.77 |19.23 |22.96 |20.81 33.32 |169.83 14.94 16.01 16.09 |7.61 |0.77 |5.26E-08 |5.30E+03 |0.0038 6.62 16.82 |19.37 |22.98 |20.78 33.42 |168.18 14.94 16.21 16.29 |7.72 |0.77 |5.06E-08 |5.27E+03 |0.0039 6.61 16.86 |19.46 |23.04 |20.83 33.51 |167.45 14.94 16.27 16.36 |7.76 |0.77 |4.98E-08 |5.27E+03 |0.0039 6.73 16.88 |19.40 |23.35 |20.98 33.52 |172.15 14.95 16.22 16.31 |]7.67 |0.77 |5.21E-08 |5.33E+03 |0.0038 Red Data is an average of all data points. CO,/Argon Run 60: Heat Exchanger Composition -15.81 Argon,81.77 Carbon Dioxide Date -24 July 2008 Notebook Page -156 Front Page - Water Flow Rate -0.602 kg/min (0.010033 kg/s) Pressure Gauge -230 psi 486 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Pressure Transducer -236 psi Gas Inlet Temperature -120°C (248°F) Averaged Data-5 Minutes HX Transfer Area-0.24 m2HXWater-side Heat Transfer Coefficient-0.15 BTU/ftzsR (3066.27 WimkK) Thermal Conductivity for SS,Kw-16.0 W/mK Inner Tube Diameter,Di-0.011 m Inner Tube Outside Diameter,Do-0.0127 m Di/2Kwln(Do/Di)-4.93992E-05 (Di/Do)/hwater-0.000282474 Total Volume of System -0.00334 m2 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu_|Pr Gr Re Friction Flow |(bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer (lb/hr)(VU)Coefficient W/m2K (W/m2K) 6.28 16.31 |18.46 |20.83 |20.21 32.38 |119.40 14.90 13.27 13.33 |6.94 |0.79 |4.75E-08 |5.33E+03 |0.0041 6.32 16.27 |18.59 |20.81 |20.14 32.32 |120.65 14.89 13.77 13.84 |7.19 |0.79 |4.46E-08 |5.36E+03 |0.0041 6.31 16.22 |}18.72 |20.95 }20.17 32.20 |121.60 14,90 13.98 14.04 |7.28 |0.79 |4.36E-08 |5.34E+03 |0.0041 6.26 16.16 |18.83 |21.04 |20.24 32.06 |121.70 14,90 13.94 14.00 |7.26 |0.79 |4.38E-08 |5.29E+03 |0.0041 6.17 16.13 |18.94 |21.10 |20.31 31.98 |120.49 14.90 13.80 13.86 |7.20 |0.79 |4.40E-08 |5.22E+03 |0.0041 6.11 16.22 |18.99 |21.15 |20.39 32.16 |118.90 14.91 13.53 13.59 |7.08 |0.79 |4.50E-08 |5.18E+03 |0.0041 6.18 16.26 |19.05 |21.19 |20.46 32.23 |117.78 14.91 13.64 13.70 |7.15 |0.79 |4.37E-08 |5.26E+03 |0.0041 6.21 16.26 |19.07 |21.25 |20.50 32.23 |117.64 14.91 13.68 13.74 |7.17 |0.79 |4.34E-08 |5.28E+03 |0.0041 6.24 16.30 |18.99 |21.33 |20.56 32.32 |118.23 14.92 13.48 13.54 |7.06 |0.79 |4.51E-08 |5.30E+03 |0.0041 6.27 16.31 |18.87 |21.34 |20.58 32.34 |119.31 14.92 13.31 13.37 |6.96 |0.79 |4.69E-08 |5.32E+03 |0.0041 6.32 16.30 |18.93 |21.32 |20.56 32.32 |120.66 14.92 13.62 13.68 |7.10 |0.79 |4.54E-08 |5.35E+03 |0.0041 487 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Mass |Pressure |Water |Water |Gas Gas Out |Gas In |Gas In Total Heat |Gas Side Nu Pr Gr Re Friction Flow (bar)In Out Out Density |(°C)Density |Transfer Heat Factor Meter (°C)(°C)(°C)|(kg/m3)(kg/m3)|Coefficient |Transfer(Ib/hr)(VU)Coefficient W/m2K (W/m2K) 6.32 16.26 |18.84 |21.36 |20.56 32.22 |122.11 14.91 13.47 13.53 |7.00 |0.79 |4.72E-08 |5.34E+03 |0.0041 6.29 16.19 |18.83 |21.28 |20.52 32.08 |122.49 14.91 13.48 13.54 |7.00 |0.79 |4.73E-08 |5.31E+03 |0.0040 6.21 16.23 |18.85 |21.25 |20.50 32.16 |121.99 14.91 13.36 13.42 |6.95 |0.79 |4.79E-08 |5.25E+03 |0.0041 6.22 16.28 |18.96 |21.29 |20.56 32.27 |121.01 14.91 13.44 13.50 |7.00 |0.79 |4.68E-08 |5.26E+03 |0.0041 6.27 16.25 |19.05 |21.36 |20.56 32.20 |120.62 14.91 13.71 13.77 |7.15 |0.79 |4.47E-08 |5.31E+03 |0.0041 6.25 16.25 |18.87 |21.18 |20.42 32.22 |120.29 14.91 13.59 13.65 |7.09 |0.79 |4.54E-08 |5.30E+03 |0.0041 Red Data is an average of all data points. 488 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Appendix C:Thar Phase Monitor Data Thar Unit Data Date -05 June 2008 Lab Notebook Page -22 At 5ml -2.5 bar At 15ml -1 bar After addition of carbon dioxide -50.1 bar Heated to 60°C -No liquid left GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0.51 0.5 0.49 0.48 0.495 CO2 97.36 97.23 97.13 97.34 97.265 Argon 1.87 1.2 1.2 1.18 1.3625 Notes - One data point (44.9°C,72.9bar)could not be repeated and thus omitted from the final table. Temperature |Pressure 35.1 69.1 33.8 68.6 32.9 68.1 31.4 67.1 30.4 66.6 29.1 65.8 28.4 64.8 27.6 64.4 26.4 62.4 25.2 61.1 24.4 60.4 489 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Temperature |Pressure 24 59.7 23.4 58.7 22.7 58.2 22 57.2 21.4 56.3 20.7 55.2 20 54 19.1 52 18.4 49.6 18.2 50.3 GC Analysis - Trial 1 |Trial2 |Trial3 |Trial4 |Average Air 0.51 0.5 0.49 0.48 0.495 CO2 97.36 97.23 97.13 97.34 97.265 Argon 1.87 1.2 1.2 1.18 1.3625 Notes - One data point (44.9°C,72.9bar)could not be repeated and thus omitted from the final table. Thar Unit Data Date -06 June 2008 Lab Notebook Page -24 At 5ml -2.3 bar At 15ml -0.8 bar After addition of carbon dioxide -50.3 bar,18.4°C Heated to 40°C -No liquid left 490 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Temperature |Pressure 27.6 69.6 27.1 68.3 26.4 66.6 25.9 65.4 25.5 64.6 25 63.9 24.7 63.3 24.3 63.1 23.9 62.7 23.5 62.3 23 61.9 22.5 61.1 22 60.6 21.4 59.9 20.5 58.7 20.1 58.2 19.5 57.3 19 56.5 18.6 56 18.2 55.5 49] Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 GC Analysis - Trial 1 |Trial2 |Trial3 |Average Air 1.84 1.82 1.88 |1.846666667 CO2 92.51 92.16 92.15 |92.27333333 Argon 7.13 7.18 7.29 7.2 Notes - Initial two data point (36.5°C,71.7bar;35.3°C,70.7bar)could not be repeated and thus omitted from the final table. Thar Unit Data Date -09 June 2008 Lab Notebook Page -26 At S5ml -3.5 bar,24.4°C At 15ml -1.0 bar,24.4°C After addition of carbon dioxide -55.2 bar,24.7°C Heated to 40°C (68.0 bar)-No liquid left Temperature |Pressure 30.2 70.3 28.9 68 28.2 67 26.9 64.6 26.3 63.8 26 63.1 25.6 62.2 24.6 60.2 24.2 59.9 23.7 59.5 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 492 Temperature |Pressure 23.3 58.5 22.6 57.9 22.1 57.4 21.7 56.9 GC Analysis - Trial1 |Trial2 |Trial3 |Trial4 |Average Air 0.78 0.78 0.77 0.77 0.775 CO2 96.07 96.43 96.21 96.4}96.2775 Argon 3.41 3.41 3.4 3.4 3.405 Thar Unit Data Date -11 June 2008 Lab Notebook Page -27 At 5ml -3.5 bar,24.7°C At 15ml -0.6 bar,24.7°C After addition of carbon dioxide -57.7 bar,23.8°C Heated to 35°C -Liquid still observed Heated to 40°C (73.7 bar)-No liquid left Temperature |Pressure 34.1 77.2 33.4 75.6 32.5 74.5 31.4 72.5 30.8 71.7 30.1 70.8 29.3 69.1 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 493 Temperature |Pressure 28.5 68.3 27.8 67.1 27.1 66.6 26.4 65.8 25.4 63.3 24.7 62.7 24.3 62.4 23.5 59.7 22.9 59.5 22.3 57.9 21.7 57 21.3 56.5 21 56 GC Analysis - Trial 1 |Trial2 |Trial3 |Trial4 |Average Air 0.6 0.67 0.65 0.66 0.645 CO2 97.8 97.7 97.66 97.74 97.725 Argon 2.05 2.26 2.21 2.24 2.19 Thar Unit Data Date -12 June 2008 Lab Notebook Page -28 At 5ml -3.8 bar,21.4°C At 15ml -0.5 bar,21.4°C After addition of carbon dioxide -53.8 bar,21.0°C Heated to 35°C -Liquid still observed Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Heated to 40°C -Liquid still observed Heated to 45°C -No liquid present 495 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Temperature |Pressure 35.1 78.4 34.5 77.1 33.5 76.2 31.7 73 30.1 70.8 29.4 69.5 28.6 68.3 28 67.1 27.2 66.4 26.5 65.4 25.9 64.9 25.2 63.6 24.6 62.7 24 62 23.5 61.6 22.9 60.9 22.5 60.4 21.8 58.2 21.1 57.7 20.5 55.5 20 55.2 19.4 53.1 496 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 GC Analysis - Trial 1 |Trial2 |Trial3 |Average Air 0.97 0.97 0.96 |0.966666667 CO2 97.03 96.91 96.78 |96.90666667 Argon 3.3 3.3 3.29 |3.296666667 Thar Unit Data Date -13 June 2008 Lab Notebook Page -30 At 5ml -3.0 bar,19.0°C At 15ml -n/a After addition of carbon dioxide -50.5 bar,18.7°C Heated to 40°C (75.4 bar)-No liquid observed Temperature |Pressure 33.5 76.2 30.8 71.7 28.8 69.5 27.6 66.8 26.9 66.1 26.1 65.3 25.6 64.1 24.7 62.9 24.2 62.2 23.3 59.7 22.6 59.1 21.8 58.2 21.2 57.4 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 497 Temperature |Pressure 20.8 56.5 20.4 54.3 20 54 GC Analysis - Trial 1 Trial 2 Trial 3 Average Air 0.6789 0.65662 0.62576 0.65376 CO2 97.60933 |97.98132]98.06101 |97.88388667 Argon 2.31454 2.22506 2.12781 2.22247 Thar Unit Data Date -16 June 2008 Lab Notebook Page -31 At 5ml -4.8 bar,18.2°C At 15ml -0.5 bar,18.0°C After addition of carbon dioxide -50.1 bar,17.8°C Heated to 35°C -Liquid observed Heated to 40°C -Liquid observed Heated to 45°C -No liquid observed Temperature |Pressure 32.7 76.6 31.5 75.5 30.6 73.9 29.9 72.8 28.7 71.2 28 70.3 27.1 68.3 498 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Temperature |Pressure 26.7 27.8 25.8 66.6 25.2 65.8 24.6 64.4 24 63.9 23.4 63.3 22.6 62.1 22 60.2 21.6 59 21.2 58.7 20.58 57.7 19.5 56.5 18.8 54.5 17.6 53.1 17 52.6 16.6 51.5 GC Analysis - Trial 1 |Trial2 |Trial3 |Trial4 |Average Air 1.56 1.55 1.56 1.56 1.5575 CO2 95.59 95.67 95.69 95.81 95.69 Argon 5.39 5.36 5.37 5.38 5.375 Thar Unit Data Date -17 June 2008 Lab Notebook Page -32 At 5ml -5.0 bar,17.0°C Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 At 15ml -0.6 bar,17.0°C After addition of carbon dioxide -49.3 bar,16.6°C Heated to 35°C -Liquid observed Heated to 40°C -No liquid observed Temperature |Pressure 32.1 73.7 29.8 70.7 28.6 69.6 28.1 69 27 67.8 26.1 66.4 25.2 65.4 24.7 63.6 24 63 23.5 62.2 22.9 61.1 22.3 60.7 21.8 59 21.4 57.9 20.9 57.2 20.5 56.2 19.9 55.5 19.5 54.8 18.8 54 18.4 52.6 500 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 GC Analysis - Trial 1 |Trial2 {|Trial3 |Average Air 1.23 1.3 1.34 1.29 Trial 1 |Trial2 |Trial3 |Average CO2 96.17 97.71 98.87 |97.58333333 Argon 3.91 4.06 4.15 4.04 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 501 Thar Unit Data Date -18 June 2008 Lab Notebook Page -33 At 5ml -4.8 bar,23.4°C At 15ml -1.0 bar,23.4°C After addition of carbon dioxide -n/a Heated to 35°C -No liquid observed Temperature |Pressure 24.4 63.3 23.8 62.2 23.5 61.6 23.1 60.6 22.5 59.5 21.4 58 20.5 56.2 19.9 55.2 19.2 54.5 GC Analysis - Trial 1 |Trial2 |Trial3 |Trial4 |Average Air 0.91 0.94 1.04 0.98 0.9675 CO2 94.54 92.99 94.41 94.37 |94.0775 Argon 2.87 3.02 3.28 3.1 3.0675 Notes - Initial start points:4.2 bar,18.2°C at 5ml;0.1 bar,18.2°C at 15ml;48.1 bar,18.2°C after addition of carbon dioxide yielded no results.New conditions were set and readings after carbon dioxide 502 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 was added to the system was not recorded. Thar Unit Data Date -19 June 2008 Lab Notebook Page -34 At 5ml -6.0 bar,18.3°C At 15ml -1.5 bar,18.2°C After addition of carbon dioxide -48.1 bar,17.6°C Heated to 35°C -Liquid observed Heated to 40°C -No liquid observed Temperature |Pressure 33.8 80.4 32.4 78.4 30.1 75.4 29.7 73.9 29.3 72.8 28.7 71.5 28.1 70.8 27.6 70.1 26.8]69.1 26.1 68.3 25.6 67.5 24.7 66.3 24.1 65.6 23.5 64.9 22.7 62.4 22.3 61.6 21.8 59.9 503 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Temperature Pressure 21.4 58.7 21 57.7 20.4 56.5 19.6 54.8 19 54 18.4 53.1 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 1.50345 1.49708 1.48986 1.51146 1.5004625 CO2 91.43952 |91.26178 |91.23382 |91.51949]91.3636525 Argon 4.76543 4.75878 4.73465 4.78427 4.7607825 Thar Unit Data Date -20 June 2008 Lab Notebook Page -35 At 5ml -4.3 bar,19.7°C At 15ml -0.5 bar,19.7°C After addition of carbon dioxide -50.6 bar,19.4°C Heated to 35°C -Liquid observed Heated to 40°C -No liquid observed Temperature |Pressure 29.4 73.4 8.5 72.3 27.6 70.5 26.8 68.8 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 504 Temperature |Pressure 26.3 67.6 25.9 67 25 65.6 24.6 64.8 24.2 564.2 23.8 63.3 23.4 62.5 22.7 61.6 22.2 60.7 21.7 60 21.2 59.4 20.5 58.5 19.9 57.7 19.3 57.2 18.8 55.1 18.6 54.8 GC Analysis - Trial 1 Trial 2 Trial 3 Average Air 1.6292 1.6293 1.60902 |1.622506667 CO2 90.52776 |90.38253 |90.08333 |90.33120667 Argon 5.20311 5.21403 5.16396 5.1937 Thar Unit Data Date -23 June 2008 Lab Notebook Page -36 At 5ml -8.9 bar,21.2°C Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 505 At 15ml -3.3 bar,21.2°C After addition of carbon dioxide -56.0 bar,20.3°C Heated to 35°C -Liquid observed Heated to 40°C No liquid observed Temperature |Pressure 31.5 84.2 30.6 82.3 29.4 79.1 28.5 77.9 28 76 27.4 74.8 26.9 73.7 26.4 72.6 25.7 71.8 25.2 70.9 24.6 69.6 24.2 69.1 23.4 68.74 22.9 67.5 21.8 66.1 21.4 65.6 20.7 64.9 20 63.3 19.4 62.4 506 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 GC Analysis - Trial 1 Trial 2 Trial 3 Average Air 2.37282 2.39315 2.39618 |2.387383333 CO2 86.70858 |86.78741]86.80552 86.76717 Trial 1 Trial 2 Trial 3 Average Argon 7.76049 7.79896 7.83488 7.79811 Thar Unit Data Date -24 June 2008 Lab Notebook Page -37 At 5ml-11.1 bar,19.1°C At 15ml -4.7 bar,19.1°C After addition of carbon dioxide -52.0 bar,18.6°C Heated to 35°C -Liquid observed Heated to 40°C -No liquid observed Temperature |Pressure 34.2 89.3 32.9 87.3 31.6 85.3 30.3 82.6 29.4 80.4 28.4 78.9 27.6 7.8 27 75.5 64.4 74.7 25.9 73.9 25.5 73 507 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Temperature |Pressure 25 72.3 24.3 71.5 23.1 70.3 22.1 8.6 21.1 67.5 20.5 66.6 20 65.6 19.5 64.9 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 2.74933 2.77779 2.78654 2.77175 2.7713525 CO2 84.09184 |84.62887 |84.47231 |84.18547 |84.3446225 Argon 9.21052 9.23593 9.2807 9.23248 9.2399075 Thar Unit Data Date -25 June 2008 Lab Notebook Page -38 At 5ml -11.7 bar,18.3°C At 15ml -4.8 bar,18.3°C After addition of carbon dioxide -49.8 bar,17.0°C Heated to 35°C -Liquid observed Heated to 40°C -No liquid observed Temperature |Pressure 34.1 91.4 32.9 88.2 508 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Temperature |Pressure 31.1 86.5 30.6 84.1 29.7 82.6 28.2 79.5 27.6 78.3 26.9 76.6 26.4 75.9 25.8 75 25.2 74 24.7 73.2 24.1 72.5 23.5 71.5 22.9 70.5 22.3 69.1 21.4 68.3 20.8 67.5 20.3 66.6 19.6 65.6 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 CO2 91.56917 |92.15395 |91.98346]91.67112 91.844425 Argon 11.15816 |11.18895 |11.24319|11.18477|11.1937675 509 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Thar Unit Data Date -26 June 2008 Lab Notebook Page -39 At 5ml -11.3 bar,18.7°C At 15ml -4.6 bar,18.7°C After addition of carbon dioxide -50.2 bar,18.2°C Heated to 35°C -Liquid still observed Heated to 40°C -No liquid left Temperature |Pressure 30.1 86.5 28.8 83.5 28 82.3 27.1 79.6 26.4 77.4 25.8 75.5 25.2 74.7 24.8 73.9 24.4 73 24 72.5 23.1 71.5 22.5 70.3 21.6 68.9 21.1 68.1 20.5 67.3 19.9 66.4 19.5 65.6 510 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 CO2 91.14946 |91.37793 |91.0275 |90.59342 |91.0370775 Argon 12.34751]12.35584 12.439 |12.44447 12.396705 Thar Unit Data Date -27 June 2008 Lab Notebook Page -40 At 5ml -11.9 bar,17.3°C At 15ml -5.8 bar,17.4°C After addition of carbon dioxide -54.8 bar,17.0°C Heated to 35°C -Liquid still observed Heated to 40°C -No liquid left Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 511 Temperature |Pressure 34.5 88 32.5 85.8 31.2 83.3 30.7 82.4 29.5 80.4 28.7 78.4 27.8 77.1 27.2 76.1 26.5 75.2 26.1 74.5 25.4 73.4 24.8 72.5 24.4 71.8 24 71.3 23.1 69.6 22.1 68.4 21 67 20.5 66.4 20.1 65.6 19.5 67.9 512 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 CO2 93.26965 |92.94752]92.99208 |92.91798 |93.0318075 Argon 9.01082 9.05603 9.07954 9.05628 9.0506675 Thar Unit Data Date -30 June 2008 Lab Notebook Page -41 At 5ml -11.6 bar,19.5°C At 15ml -5.0 bar,19.5°C After addition of carbon dioxide -51.0 bar,19.0°C Heated to 35°C -No liquid observed Temperature |Pressure 29.5 87.2 28.9 85.1 28.1 82.1 27.4 80.9 26.5 77.9 26 76.6 25.5 75.5 25 74.5 24.7 73.9 23.8 73 23 72 22.4 70.7 513 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Temperature |Pressure 21.8 69.6 21.2 68.6 20.7 68 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 CO2 90.65798 |90.80868 |90.14054 |90.05731 |90.4161275 Argon 11.53886 |11.55534 |11.54828 |11.61751 |11.5649975 Thar Unit Data Date -01 July 2008 Lab Notebook Page -42 At 5ml -12.4 bar,20.8°C At 15ml -5.7 bar,20.8°C After addition of carbon dioxide -54.0 bar,20.1°C Heated to 35°C -No liquid observed Temperature |Pressure 30.2 88.2 29.1 85.6 28.6 84.7 28.1 83.5 27.4 81.4 27.1 80.1 26.5 78.7 25.9 77.4 514 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Temperature |Pressure 25.5 76.2 25.2 75.7 24.8 74.9 24.1 73.9 21.6 69.4 20.9 68.8 20.4 68.1 20 67.5 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 CO2 88.4653 |88.54791 |88.53689 |81.23636 86.696615 Argon 11.60189 |11.54886 |11.57393 9.56083 11.0713775 Thar Unit Data Date -02 July 2008 Lab Notebook Page -43 At 5ml -12.6 bar,21.8°C , At 15ml -5.7 bar,21.8°C After addition of carbon dioxide -52.0 bar,20.4°C Heated to 35°C -No liquid observed Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 515 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 CO2 88.4653 |88.54791 |88.53689 |81.23636 86.696615 Argon 11.60189 |11.54886 |11.57393 9.56083 |11.0713775 Thar Unit Data Date -03 July 2008 Lab Notebook Page -44 At 5ml -13.1 bar,20.0°C At 15ml -5.8 bar,20.0°C After addition of carbon dioxide -53.0 bar,19.4°C Heated to 35°C -No liquid observed 516 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Temperature |Pressure 32.2 97.9 31 89.8 29.8 86.7 28.9 85.1 28 83.3 27.2 81.8 26.5 78.5 26 77.2 25.5 76.5 25.1 75.6 24.7 75 24.3 74.5 23.8 73.9 23.3 73.1 22.7 72.1 22.2 71.5 21.3 69.8 20.7 69.1 20.1 67.8 517 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 GC Analysis - Trial 1 Trial 2 Trial 3 Average Air 0 0 0 0 CO2 87.74438 |87.76574 |87.64445 87.71819 Trial 1 Trial 2 Trial 3 Average Argon 11.54914]11.67417|11.74026[11.65452333 Thar Unit Data Date -07 July 2008 Lab Notebook Page -45 At 5ml-13.1 bar,20.1C At 15ml -5.8 bar,20.1°C After addition of carbon dioxide -52.0 bar,19.4°C Heated to 35°C -No liquid observed Temperature |Pressure 28.9 86.3 28.1 85.1 27.4 83.1 26.8 81.4 26.1 78.9 25.7 77.6 25.2 75.9 24.8 74.9 24.1 73.4 23.5 72.4 22 70 21.4 69.1 518 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Temperature |Pressure 20.9 68.3 20.1 67 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 CO2 87.12635 |87.16707 |86.93918 |86.72721 86.9899525 Argon 12.54147 12.51321 12.54761 12.51944 12.5304325 Thar Unit Data Date -08 July 2008 Lab Notebook Page -46 At 5ml -10.2 bar,21.7°C At 15ml -4.3 bar,21.7°C After addition of carbon dioxide -53.8 bar,20.5°C Heated to 35°C -No liquid observed Temperature Pressure 36.1 86.3 32.9 86 31.7 85 30.8 83.1 29.7 80.6 519 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Temperature Pressure 28.9 78.7 28.4 77.2 (27.8 76.8 27.1 75.5 26.7 74.7 26.4 74.3 26 73.8 25.6 73 25.1 72.3 23.7 70 22.7 68.8 21.4 66.6 20.7 66 20 64.9 19.6 64.4 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 CO2 91.32852 |91.32251 91.13644 |91.13379 |91.230315 Argon 8.6026 8.69158 8.69147 8.62187 8.65188 Thar Unit Data Date -09 July 2008 Lab Notebook Page -47 At 5ml -12.6 bar,19.4°C At 15ml -5.5 bar,19.4°C Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 520 After addition of carbon dioxide -53.5 bar,28.8°C Heated to 35°C -No liquid observed Temperature Pressure 34.4 92.1 32.5 89.8 30.8 85.5 29.4 82.6 28.5 79.9 27.8 78.9 27.4 78.2 26.7 77.2 25.9 76.2 25.4 75.5 24.8 74.5 24.4 73.9 23.7 73.0 23.0 71.7 22.4 70.8 21.7 70.0 21.0 68.3 20.5 68.1 GC Analysis - Notes - Gas Chromatograph faulted,could not analyze gas. 521 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Thar Unit Data Date -10 July 2008 Lab Notebook Page -48 At Sml -14.8 bar,21.0°C At 15ml -7.2 bar,21.0°C After addition of carbon dioxide -54.0 bar,20.0°C Heated to 35°C -No liquid observed Temperature |Pressure 29.5 88.3 28.8 86.5 28.2 84.3 27.6 82.1 27.2 80.6 26.5 79.1 25.9 78.1 25.2 77.2 24.7 75.9 23.5 73.7 22.7 72.5 22 71.5 21.3 70.3 20.7 69.7 20.3 68.8 GC Analysis - Notes - Gas Chromatograph faulted,could not analyze gas. 522 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Thar Unit Data Date -18 July 2008 Lab Notebook Page -49 At 15ml -5.7 bar,20.0°C After addition of carbon dioxide -55.2 bar,21.0°C Heated to 40°C -No liquid observed Temperature |Pressure 40.9 94.1 36.7 89.3 33.7 86 31.6 83.3 30.2 80.6 29.4 78.7 28.2 76.6 27.4 75.2 26.8 74.2 26.3 73.5 25.7 72.8 25.2 72 24.8 71.7 24.3 70.8 23.4 68.7 22.3 68 21.3 66.6 20.5 66.3 19.9 64.6 523 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 CO2 91.25052 |91.19222 |91.0345}91.31973 |91.1992425 Argon 7.65494 7.59946 |7.55626 7.51001 7.5801675 Thar Unit Data Date -21 July 2008 Lab Notebook Page -50 At 15ml -8.4 bar,21.3°C After addition of carbon dioxide -55.7 bar,20.4°C Heated to 40°C -Liquid observed Heated to 45°C -No liquid observed Temperature Pressure 37 89.7 35.7 87.7 32.9 82.4 31.8 80.4 31 78.9 29.9 77 28.4 74,2 27.4 73.2 26.5 71.7 25.7 70.5 24.8 69.5 24.3 68.8 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 524 Temperature |Pressure 23.4 67.5 22.5 66.3 21.7 65.3 21 64.3 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 CO2 96.32897 |96.36823}96.39492 |96.66723 |96.4398375 Trial 1 Trial 2 Trial 3 Trial 4 Average Argon 3.81715 3.75694 3.73664 3.70169 3.753105 Thar Unit Data Date -22 July 2008 Lab Notebook Page -51 At 15ml -12.6 bar,18.3°C After addition of carbon dioxide -54.0 bar,17.8°C Heated to 40°C -No liquid observed Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 525 Temperature |Pressure 28.1 88.2 27.4 87.3 26.8 84.8 26 83.3 25.6 82.3 25.2 81.4 24.8 80.4 24.1 79.2 23 78 22.3 76.2 21.4 74.5 20.9 73.7 20.4 72.8 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 CO2 77.81726 |77.76606 |77.98013 |78.04045 77.900975 Argon 21.95241 |22.12405 |22.11913 |22.07244 |22.0670075 526 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Thar Unit Data Date -23 July 2008 Lab Notebook Page -52 At 15ml -12.7 bar,18.6°C After addition of carbon dioxide -53.6 bar,18.0°C Heated to 40°C -No liquid observed Temperature |Pressure 27.8 88.5 27.2 87.3 26.5 86.5 26 84.5 25.4 82.9 25 81 24.6 80.1 24.2 79.2 23.5 77.9 22.6 78.8 21.8 74.2 21 72.5 20.1 70.8 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 CO2 79.44962 |79.36717|79.42671 |79.34787 |79.3978425 Argon 20.44934 |20.54902 |20.40344 |20.50625 |20.4770125 527 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Thar Unit Data Date -24 July 2008 Lab Notebook Page -53 At 15ml -10.2 bar,18.2°C After addition of carbon dioxide -51.3 bar,17.7°C Heated to 40°C -No liquid observed Temperature Pressure 25.8 84 25.2 81.6 24.6 80.6 24 79.2 23.5 77.6 22.9 75.7 22.1 73.7 21.7 72.2 20.5 71.2 19.9 69 19.5 67.5 19.3 67.1 GC Analysis - Trial 1 Trial 2 Trial 3 Trial 4 Average Air 0 0 0 0 0 CO2 80.30269 |79.90601 |80.00222 |80.03819|80.0622775 Argon 19.55017 |19.54385 |19.54996|19.53768 19.545415 528 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Appendix D:Small Vessel Experiment Data Run 1 Data - Starting Composition - Trial 1 Trial 2 Trial 3 Trial 4 Average Carbon Dioxide |83.46859 |85.05612 |83.67514 |83.9613 |84.0402875 Argon 13.71958 |12.3842 |13.4486 |13.15694 13.17733 27 July 2008 - Initial Pressure -1375 Initial Temperature -80 Final Pressure -870 Final Temperature -9 Trial 1 Trial 2 Trial 3 Trial 4 Average Carbon Dioxide 95.4485 1 95.4774 95.61561 95.73106 |95.568145 Argon 3.37171 3.16831 3.19637 3.15763 3.223505 28 July 2008 - Initial Pressure -1025 Initial Temperature -23 Final Pressure -800 Final Temperature -10 Trial 1 Trial 2 Trial 3 Average Carbon Dioxide |96.31592 |96.13819 |95.83456 |96.0962233 Argon 1.99569 |2.06692 |2.14367 2.06876 05 August 2008 - Initial Pressure -650 Initial Temperature -22 Final Pressure -600 Final Temperature -7 529 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Trial 1 Trial 2 Trial 3 Trial 4 Average Carbon Dioxide |88.36072 |88.0206 |88.12301 |88.36887 |88.16811 Argon 10.27235 |10.31007 |10.27509 |10.27199 |10.282375 Final Gas Composition - Trial 1 Trial 2 Trial 3 Trial 4 Average Carbon Dioxide |88.38772 |88.3073 |88.50735 |88.52971 88.43302 Argon 10.14155 |10.14312 |10.14313 |10.14907 |10.1442175 Composition Data - Agilent Cerity QA/QC Report Sample name:0725ArCOOGasVessel6 Sample note: Submission time:Friday,July 25,2008 2:48:40 PM Operator: Injection date:Friday,July 25,2008 2:52:35 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM 530 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDI1A r- eis 5 min2515 TCDZA wea weg eequoqey-gzzd Tf a ae min16 TCD3 A ub BAxQsuoBry=ZSEL | "4 i ee -| nenney nameee openineeeneenebete= min15 oos oa4--- 531 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample Sampling source:Unknown Signal Retention Time [min]Type Area [!iV's]Amt/Area Amount [mass%]Name 1 1.500 ---Oxygen 1 1.637 ---Nitrogen 2 0.245 BP 2.4707e+005 0.00000e+000 0.00000 2 0.276 VB 1.6978e+006 4.94521e-005 83.96130 Carbon Dioxide 2 1.220 ---Sulfur Dioxide 3 1.352 BB 9.1023e+004 1.44545e-004 13.15694 Argon/Oxygen 3 2.112 ---Nitrogen_2 Agilent Cerity QA/QC Report Sample name:0725ArCOOGasVessel5 Sample note: Submission time:Friday,July 25,2008 2:48:39 PM Operator: Injection date:Friday,July 25,2008 2:49:02 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM 532 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 00g ; i A ;= := E E :[& 5 "bh + Oh ee2 ab | : ees 0edes ee i 4: : conde Lie) pe . . abe : wN NN :N + 5 E i hoses 4 % . ; a one Ln . . he eek : i f: : eeeeee (ee § "ee 4 . 4 nn ne©Oo) I> nesaeOy coy bd r - x ; <x ::x . : . S a" . N .-=53 nee an 4 o : ; o |G YabAxqsuobiy-LSet| = de bole ote§ . = sot an 4 es rsOsen Seen eb 4 rs eeee ae 4 - bow bee weeniennneaesteefage Lees a 4. { ” +t + 7| r onl IXOlg Ud : 2O en | pede taEbSo.|. qis) 533 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample Sampling source:Unknown Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount [mass%]Name 1 1.500 ---Oxygen 1 1.637 ---Nitrogen 2 0.245 BP =2.5248e+005 0.00000e+000 0.00000 2 0.276 VB 1.6920e+006 4.94521e-005 83.67514 Carbon Dioxide 2 1.220 ---Sulfur Dioxide 3 1.351 BB 9.3041e+004 1.44545e-004 13.44860 Argon/Oxygen 3 2.112 ---Nitrogen_2 Total amount =97.12374 Agilent Cerity QA/QC Report Sample name:0725ArCOOGasVessel4 Sample note: Submission time:Friday,July 25,2008 2:30:19 PM Operator: Injection date:Friday,July 25,2008 2:41:16 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM 534 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDI1A >:iarsoeoneY 9 7 a :iOewancyonae ; ==whe males eet ©1...Loe '; 4 :.'i 4 ..:a a i. .:_-a a beste ceeded, oO =:__: "we . " SESE EEL Le Pe --_---_-Sy 05 1 16 2 25 min TCDZA >;:=a * fo]':Oo we neg pee pe ao: ;T 7 i 7 1 15 2 25 min TCDZA >fo "eee,2 eo iRe:H oO;:.€!8!| |5 | }(Ww,: 8 i or!:=:rc:: 6 : fee :ire):j i iN: .::.:- :::H : : EE EEE A |oo rr 05 4 15 2 25 min ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 535 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Unknown ;Signal Retention Time [min]Type Area [jIV*s] 1 1.500 - 1.637 - 2 0.245 BP 2.5756e+005 2 0.276 VB =1.6879e+006 2 1.220 - 3 1.351 BB 9.4916e+004 3 T 2.112 - otal amount =97.18817 Agilent Cerity QA/QC Report Sample name:0725ArCOOGasVessel3 Sample note: Submission time:Friday,July 25,2008 2:30:18 PM Operator: Injection date:Friday,July 25,2008 2:37:42 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM 536 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Amt/Area Amount [mass%]Name 0.00000e+000 0.00000 4.9452 1e-005 83.46859 1.44545e-004 13.71958 Oxygen Nitrogen Carbon Dioxide Sulfur Dioxide Argon/Oxygen Nitrogen_2 TCDIA >*fo.-_; =|oo a bod.::; o ;\:': 8 4 -_..ceeribe ode L '.wh .10 oy . \:.Fe -: :-': :!L an oO 4 r -: i Aid emiiemstimip-nas 'J.psi fice -+-_--Sa ooo 0.5 1 15 2 25 min TCDZA 2 Senge,i :: _f Axo eee eee anaes nt Bs Hi .Oo?!:; a a }!:c=]{3 2 :': mn t t i oO.|:; i a Lhe hed. nt :|:f=)N :'po!o 4 OL.=_on 4 a penne gence ey °:i r T T T T T+ 05 1 15 2 25 min TCD3A £5.mon t .a 1 ; {/2 :iRB:+QO.;: |.§:: eo j ii(PY ::ni i mM,:;W,-t i /3 i __ee -_ T v r T T T Tr T +r T T T T T T T T r T T T T T T T v -++ 0.5 1 15 2 25 __min ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 537 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Unknown Signal Retention Time [min]Type Area[iv's]Amt/Area Amount [mass%]Name 1 1.500 ---Oxygen 1 1.637 ---Nitrogen 2 0.245 BP 2.3494e+005 0.00000e+000 0.00000 2 0.276 VB 1.7200e+006 4.94521e-005 85.05612 Carbon Dioxide 2 1.220 ---Sulfur Dioxide 3 1.352 BB 8.5677e+004 1.44545e-004 12.38420 Argon/Oxygen 3 2.112 ---Nitrogen_2 Total amount =97.44032 Agilent Cerity QA/QC Report Sample name:0725ArCOOVessel8 Sample note: Submission time:Friday,July 25,2008 2:06:14 PM Operator: Injection date:Friday,July 25,2008 2:17:17 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM 538 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >4 1 : a tet 4 : ]wd ; o ::!, o 4 vancesbe .mend .cae 4 i {t !\ i.i : o -\.Lo nade Ld nant onde T T *T 15 2 25 min TCD2Z2A 2 !. o +as 7 oo oom _ ra i i : 'e Z :7cod}{ 2 ||i 2 " Oo -.A... -eg ee hee.-awe:-peofe oe _ ° T T --S] 15 2 25 min TCDSA >i ca t 0 5 ”ae f wee=.''1 j .{ i '''!''[=]= Poo,oe BE |: po Be || re Q in i dee fo ete t .wun Le : Ls]T T i T .+ 4 18 2 25 min ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 539 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Unknown Signal Retention Time [min]Type Area [!iV's]Amt/Area Amount [mass%]Name 1 1.500 ---Oxygen 1 1.637 ---Nitrogen 2 0.245 BP 6.5066e+004 0.00000e+000 0.00000 2 0.274 VB =1.9358e+006 4.94521e-005 95.73106 Carbon Dioxide 2 1.220 ---Sulfur Dioxide 3 1.354 BB 2.1845e+004 1.44545e-004 3.15763 Argon/Oxygen 3 2.112 ---Nitrogen_2 Total amount =98.88869 Agilent Cerity QA/QC Report Sample name:0725ArCOOVessel7 Sample note: Submission time:Friday,July 25,2008 2:06:14 PM Operator: Injection date:Friday,July 25,2008 2:13:43 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM 540 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >4 '4°5 yoo .tay an=a :.'i :{ 4 ae -ee :a .j : i ee :4 Oo i ,},! od----es ;1 eee ae Deenn bow ee a nies D :otk F : +: || i t po Oo -im nea a te _-be he eae ene chee --,T T T T T 08 1 15 2 25 min TCD2A >or tee i .:A ; =2 '. o 4 MNKs ee be ee es bee a 4 * os i :: i :: 4 ;;: 2 7 a a : 2 i |_7 "i.:::::°oo : --t .j-a i :a. b i :: |i : g pa Hoo |: o Y7 |rs ;ee r +T -r T 7 7 7 7 T 7 .7 r r r 7 7 05 1 16 2 25 min TCD3A 3 poor boos:ck poor ty ,5 - ::1 :i1ianon:a reed ' i an :i ':: o .=..; 4 ':a tee }ii::2 i i :4 :soe HL G a i 'rroo 7 i "Bo |=}pot ete mo ! i)---Tt 05 1 15 2 25 min ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 541 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Unknown Signal Retention Time [min] 1 1.500 1 1.637 2 0.245 2 0.274 2 1.220 3 1.354 3 T 2.112 otal amount =98.81199 Agilent Cerity QA/QC Report Sample name:0725ArCOOVessel6 Sample note: Type Area [!iV's]Amt/Area Amount [mass%]Name -Oxygen ---Nitrogen BP 6.5648e+004 0.00000e+000 0.00000 VB =1.9335e+006 4.94521e-005 95.61561 Carbon Dioxide ---Sulfur Dioxide BB .2.2113e+004 1.44545e-004 3.19637 Argon/Oxygen ---Nitrogen_2 Submission time:Friday,July 25,2008 2:06:12 PM Operator: Injection date:Friday,July 25,2008 2:10:10 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM 542 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >}{H=t {oboA.i i i i ;i of 4 be -a.- Q |;o ain Sioa _fom "f fo epee pen eeioiii :o o A.iL | |r pos eee oO ter - 15 2 25 min TCDZ2A >p :aoO -op _ao ounces on : .| :i :i .i ': :i :: :Lie oer ;= 2 4 |:: go r wee ee be ee pone =--- %:i i : mT T T r r 045 4 15 2 25 min TCDSA >bees se &e Bo. =j ::':;: pode cee Ge hk pod ;Poe EEpoBe .4 bo he.F we |Poet.wk Se.a oi:a Be || fe foes :ak "y 1 i ::a od i ! &abe 3 a a Se ee he wk. :bo,.{i Tr T T T Y 1 15 2 25 min ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 543 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Unknown Signal Retention Time [min]Type Area [!iV*s]Amt/(Area Amount [mass%]Name 1 1.500 ---Oxygen 1 1.637 ---Nitrogen 2 0.245 BP 6.4949e+004 0.00000e+000 0.00000 2 0.274 VB 1.9307e+006 4.94521e-005 95.47740 Carbon Dioxide 2 1.220 ---Sulfur Dioxide 3 1.354 BB 2.1919e+004 1.44545e-004 3.16831 Argon/Oxygen 3 2.112 ---Nitrogen_2 Total amount =98.64571 Agilent Cerity QA/QC Report Sample name:0725ArCOOVessel5 Sample note: Submission time:Friday,July 25,2008 2:06:12 PM Operator: Injection date:Friday,July 25,2008 2:06:37 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Friday,July 25,2008 9:03:06 AM 544 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCD1A >7 ;: a i 8 - : p=4 ee ee nO i -codcnee enlenio-|i . ok ;-pod,:: |i : 7 "ae i 4 "+wet °---_met ns 15 2 25 min TCDZA z :i ' ae --c :° c-:od ofP|| & 3 .|| ¢be oO N ::|ifa)-OL.fee k -web eet ee +° :.| i T T - 05 1 18 2 25 min TCD3A 2 |es nee : i ens =Seen i A }=. :;.'oO::i ' |"4 'a.ee +7 t :1 Pot,a boot. cr aa i w {4 t rs re i tooi,or :i : i a .boa :1 i 4 i T T - 1 15 2 25 min ESTD Report Calibration last saved:Friday,July 25,2008 9:03:06 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 545 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Unknown Signal Retention Time [min] 1 1.500 1.637 2 0.245 2 0.274 2 1.220 3 1.354 3 T 2.112 otal amount =98.82022 Agilent Cerity QA/QC Report Sample name:0728ArCOOVessel8 Sample note: Type Area[iV*s]Amt/Area Amount [mass%]Name -Oxygen ---Nitrogen BP 6.9058e+004 0.00000e+000 0.00000 VB 1.9301e+006 4.94521e-005 95.44851 Carbon Dioxide ---Sulfur Dioxide BB 2.3326e+004 1.44545e-004 3.37171 Argon/Oxygen ---Nitrogen_2 Submission time:Monday,July 28,2008 2:41:19 PM Operator: Injection date:Monday,July 28,2008 2:54:02 PM GC Description:MIcro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Monday,July 28,2008 2:41:07 PM 546 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCD1A a7. :;.c |ke ee ee oe i 8 4 !Ds)Poo i : |.{ oh a" : --ry 05 1 15 2 25 min TCD2A >av .i t a id a 4 i ' ..mn cee of 'i ' a ;i c : |i°o i : a 5.i -€Poa.{f as 'bt }:-&:i sh °i |o :'i jorotececoctswee=i a we be ep ee PoaoOrTrTTT¥Tt 05 1 15 2 25 min TCDO3ZA 1S 4 ! =|130 i Y a ' 'a |'” =.::i ar i Dt i i : T T T r T + 1 15 2 25 min ESTD Report Calibration last saved:Monday,July 28,2008 2:41:07 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 547 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Unknown Signal Retention Time [min] 1 1.500 1.660 0.244 0.274 2 1.288 3 1.237 3 2.112 Total amount =98.31161 Agilent Cerity QA/QC Report Sample name:0728ArCOOVessel7 Sample note: Type Area [!iV's]Amt/Area Amount[mass%]Name -Oxygen ---Nitrogen BP 3.8810e+004 0.00000e+000 0.00000 VB =1.9477e+006 4.94521e-005 96.31592 Carbon Dioxide ---Sulfur Dioxide BB 1.3807e+004 1.44545e-004 1.99569 Argon/Oxygen ---Nitrogen_2 Submission time:Monday,July 28,2008 2:41:19 PM Operator: Injection date:Monday,July 28,2008 2:50:27 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Monday,July 28,2008 2:41:07 PM 548 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >4 j .i i|t :; ior 1 2 i ;i : 8 --oT |: x )fe : :i.thee e ete gee tee| -T 1 T T T * 05 1 15 2 25 min TCD2A ol 4 { 1x : oe H a : c i 3.7 ' 2 'i a)wf ia. ot rs d . a : -O.._.-.<a che .See 41 15 2 25 min TCDZA a fee sn Fe wefan -be a i ee i”” |&..| i ee |4i2!i : a Son !]rs a a - .>A i : !N :i fe |4 i 'i Lege eek ed oe }wick. --*>ry i i 06 1 15 2 25 min ESTD Report Calibration last saved:Monday,July 28,2008 2:41:07 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 549 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Unknown Signal Retention Time [min]Type Area [!iV's]Amt/(Area Amount[mass%]Name 1 1.500 ---Oxygen 1 1.660 ---Nitrogen 2 0.244 BP 3.9649e+004 0.00000e+000 0.00000 2 0.274 VB 1.9441e+006 4.94521e-005 96.13819 Carbon Dioxide 2 1.288 ---Sulfur Dioxide 3 1.234 BB 1.4300e+004 1.44545e-004 2.06692 Argon/Oxygen 3 2.112 ---Nitrogen_2 Total amount =98.20511 Agilent Cerity QA/QC Report Sample name:0728ArCOOVessel6 Sample note: Submission time:Monday,July 28,2008 2:41:15 PM Operator: Injection date:Monday,July 28,2008 2:46:55 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A;TCD3 A Method:July21Cal Method last saved:Monday,July 28,2008 2:41:07 PM 550 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >4 t srg :1 >:: og].a bbe '_. bed ' :| : -Cn 0.56 1 15 2 25 min TCD2A he,: ix . of \: a "4 i e {:: o.i i ' "2 4 r vLTi1ra)bolle,': t ; a bh i ' o nh i \if=)_9 i i84}--4 -3 --eee a _ne :.Se 05 4 15 2 25 min TCD3ZA aw neenee ot we sa che as te mn &.|Poe Ge 7BB|;i=i {2 i + mot a a . a.4 mt .{.2 !N ! t a en ': ob oS Z T mT 7 1 T OO 0.6 4 16 a 2.25 __min ESTD Report Calibration last saved:Monday,July 28,2008 2:41:07 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 551 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Unknown Signal 1 1 2 2 2 3 3 T otal amount Retention Time [min]Type Area [!iV*s]Amt/Area Amount [mass%]Name -Oxygen ---Nitrogen BP 4.0379e+004 0.00000e+000 0.00000 VB 1.9379e+006 4.94521e-005 95.83456 Carbon Dioxide ---Sulfur Dioxide BB 1.4830e+004 1.44545e-004 2.14367 Argon/Oxygen ---Nitrogen_2 97.97823 Agilent Cerity QA/QC Report Sample name:00805ArCOOVessel3 Sample note: Submission time:Tuesday,August 05,2008 2:09:47 PM Operator: Injection date:Tuesday,August 05,2008 2:11:57 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A Method:Aug4Cal Method last saved:Tuesday,August 05,2008 1:12:36 PM 552 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA :is : :o oO.:| £r : :os a 4 i €:| +"Oo .a -ope2.{ _t |e : oT,|-|i i "|ne ||1 |. ;| !H | +URE SRREAAIIRARAIEERLAEEEER AIEEE DEEEEAGEEEEE SEER EEE EES EER EER aEREEIA aoe eee meen een eee eee eee ee 06 1 15 2 25 min TCDOZA >|L=a } i Leche,| fo nn nn ' SooO qjOoth 1 - So So rd 4 i j SEEITEE EEESEAIEE SIREE EER EE SEIU AER RAR IR Sen Seen en pee ae ae ee oe mees|;ee __4 415 _2 7 25 min ESTD Report Calibration last saved:Tuesday,August 05,2008 1:12:36 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 553 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[!iV*s]Amt/Area Amount [mass%]Name 1 1.479 BB 8.1886e+004 1.25447e-004 10.27235 Argon/Oxygen 1 1.644 BB 911.62131 0.00000e+000 0.00000 1 1.894 ---Nitrogen 2 0.275 BB 1.7497e+006 5.05013e-005 88.36072 Carbon Dioxide 2 1.255 ---Sulfur Dioxide Total amount =98.63307 Agilent Cerity QA/QC Report Sample name:00805ArCOOVessel2 Sample note:Submission time:Tuesday,August 05,2008 2:04:31 PM Operator: Injection date:Tuesday,August 05,2008 2:08:26 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A Method:Aug4Cal Method last saved:Tuesday,August 05,2008 1:12:36 PM 554 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDTA 24 15 h,: =::-°! |a]pr Be8-ao a a :e || :05 7 1 15 2 i 25 min TCDZA 2 4 'io:-an |||||ee :op :| :|-!|87 7 aa op ;tom ee 7=Bo de.7 Sneha AeneaEeeae :-- ESTD Report Calibration last saved:Tuesday,August 05,2008 1:12:36 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 555 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount [mass%]Name 1 1.480 BB 8.1908e+004 1.25447e-004 10.27509 Argon/Oxygen 1 1.644 BB 909.66630 0.00000e+000 0.00000 1 1.894 ---Nitrogen 2 0.275 BB 1.7450e+006 5.05013e-005 88.12301 Carbon Dioxide 2 1.255 ---Sulfur Dioxide Total amount =98.39810 Agilent Cerity QA/QC Report Sample name:00805ArCOOVessel1 Sample note: Submission time:Tuesday,August 05,2008 2:04:31 PM Operator: Injection date:Tuesday,August 05,2008 2:04:54 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A Method:Aug4Cal Method last saved:Tuesday,August 05,2008 1:12:36 PM 556 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDIA >15a4o oOo”::goof ( oO-7 p '=::: Oo .:Lk s <|!aa ° ,: o -i i o =rt >',°o i i irj:i |' |i : os : LJ Li 'r t T v 08 1 16 2 25 min TCOZA >4 :{cote i aa:.: :i i i cues i :i !:;an |::4 i : ne 4 poe dee 7 a ||;oO -d-tot b | Qo | ,i :{°J i ; 8 4 aie yon :Qo q i t[=]q i :cr ..t i : '! | !i i °: ---a---eee eee T i + a 06 i 1 AS 2 25 _min ESTD Report Calibration last saved:Tuesday,August 05,2008 1:12:36 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 557 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[liV*s]Amt/Area Amount [mass%] 1 1.481 BB 8.2187e+004 1.25447e-004 10.31007 1 1.643 BB 854.69388 0.00000e+000 0.00000 1 1.894 --- 2 0.275 BB 1.7429e+006 5.05013e-005 88.02060 2 1.255 --- Total amount =98.33067 Agilent Cerity QA/QC Report Sample name:0806ArCOOGasVessel5 Sample note: Submission time:Wednesday,August 06,2008 2:02:11 PM Operator: Injection date:Wednesday,August 06,2008 2:15:44 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A Method:Aug4Cal Method last saved:Tuesday,August 05,2008 1:12:36 PM 558 Name Argon/Oxygen Nitrogen Carbon Dioxide Sulfur Dioxide Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 >i i=i i s »- : i |: i.shot ge .: ee 4 16 2 25 mir TCD2A >=a i : 9 i :4 ::oO t 9 --r -9 { o :re _ | i.i °o . i : rt ee 06 4 16 2.25 min ESTD Report Calibration last saved:Tuesday,August 05,2008 1:12:36 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 559 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[!iV*s]Amt/Area Amount [mass%]Name 1 1.478 BP 8.0856e+004 1.25447e-004 10.14313 Argon/Oxygen 1 1.894 ---Nitrogen 2 0.275 BB =1.7526e+006 5.05013e-005 88.50735 Carbon Dioxide 2 1.255 ---Sulfur Dioxide Total amount =98.65049 Agilent Cerity QA/QC Report Sample name:O806ArCOOGasVessel4 Sample note: Submission time:Wednesday,August 06,2008 2:01:16 PM Operator: Injection date:Wednesday,August 06,2008 2:12:11 PM GC Description:MIcro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A Method:Aug4Cal Method last saved:Tuesday,August 05,2008 1:12:36 PM 560 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 2 |:|an | .|: 3 |3 .i mt -- a LJ Lf UJ q 7 T 05 1 16 2 25 min TCDZA 2 |t pos ak | s :|3Qo T Tr q 7 -t _.to2||: o +.:..::;:.:::: neta anna EEE RE Sa - ESTD Report Calibration last saved:Tuesday,August 05,2008 1:12:36 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 561 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[iV's]Amt/Area Amount [mass%]Name 1 1.477 BP 8.0856e+004 1.25447e-004 10.14312 Argon/Oxygen 1 1.894 ---Nitrogen 2 0.275 BB 1.7486e+006 5.05013e-005 88.30730 Carbon Dioxide 2 1.255 ---Sulfur Dioxide Total amount =98.45042 Agilent Cerity QA/QC Report Sample name:0806ArCOOGasVessel3 Sample note: Submission time:Wednesday,August 06,2008 2:01:16 PM Operator: Injection date:Wednesday,August 06,2008 2:08:40 PM GC Description:Mlcro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A Method:Aug4Cal Method last saved:Tuesday,August 05,2008 1:12:36 PM 562 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 >i :i :ah ne wd.ceed eee eee |:| teed | 1 v T v T 15 T T r v T r T 7 25 v r r nid TCD2A a i 4 a ee || 2 || 8 || 3 7 "ih -i :. 4 q | om 27 ESE)a Aner ane ESTD Report Calibration last saved:Tuesday,August 05,2008 1:12:36 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 563 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area ['iV*s]Amt/Area Amount [mass%]Name 1 1.478 BP 8.0843e+004 1.25447e-004 10.14155 Argon/Oxygen 1 1.894 ---Nitrogen 2 0.275 BB 1.7502e+006 5.05013e-005 88.38772 Carbon Dioxide 2 1.255 ---Sulfur Dioxide Total amount =98.52926 Agilent Cerity QA/QC Report Sample name:0806ArCOOGasVessel2 Sample note: Submission time:Wednesday,August 06,2008 2:01:15 PM Operator: Injection date:Wednesday,August 06,2008 2:05:09 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD1 A;TCD2 A Method:Aug4Cal Method last saved:Tuesday,August 05,2008 1:12:36 PM 564 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 a qo.bout 7 Foch ee |4 a a SS + tome d _ 4 415 2 25 a "min TCD2A 3 I : e|-|4 t 4 _r a a - .| )27)REE EE)SET ET ESTD Report Calibration last saved:Tuesday,August 05,2008 1:12:36 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 mass% Sample type:Sample 565 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min] 1 1.477 1 1.894 2 0.275 2 1.255 Total amount =98.67879 Type Area [iV*s]Amt/Area Amount [mass%]NameBP 8.0903e+004 1.25447e-004 10.14907 BB 1.7530e+006 5.05013e-005 88.52971 566 Argon/Oxygen Nitrogen Carbon Dioxide Sulfur Dioxide Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Run 2 Data: Starting Composition - Trial 1 Trial 2 Trial 3 Average Carbon Dioxide 74.24185 74.07071 74.00295 74.10517 Argon 11.81779 11.91732 12.00136 |11.91215667 Nitrogen 14.15018 14.26 14.22462 14.2116 Sulfur Dioxide 0.4813 0.49518 0.49163 0.48937 18 August 2008 - Initial Pressure -850 Initial Temperature -23 Final Pressure -750 Final Temperature -9 Trial 1 Trial 2 Trial 3 Trial 4 Average Carbon Dioxide |73.52727 73.91677 73.7084 73.77508 73.73188 Argon 12.16311 12.13681 12.10345 12.16288 |12.1415625 Nitrogen 14.35181 14.31585 14.29626 14.32416 14.32202 Sulfur Dioxide 0.49614 0.50655 0.50973 0.51268 0.506275 18 August 2008 - Initial Pressure -750 Initial Temperature -23 Final Pressure -690 Final Temperature -10.5 Trial 1 Trial 2 Trial 3 Trial 4 Average Carbon Dioxide |68.07692 68.4489 68.4419 68.45859 |68.3565775 Argon 14.82957 14.9077 14.68084 14.91454 |14.8331625 Nitrogen 17.47834 17.52955 17.52377 17.56148 17.523285 Sulfur Dioxide 0.689 0.59417 0.597 0.59969 0.619965 567 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Final Gas Composition - Trial 1 Trial 2 Trial 3 Trial 4 Average Carbon Dioxide |68.56309 68.401 68.53805 68.40833 |68.4776175 Argon 14.8921 14.85411 14.76574 14.75165 14.8159 Nitrogen 17.53611 17.49617 17.52005 17.54715 17.52487 Sulfur Dioxide 0.60585 0.60458 0.60583 0.60496 0.605305 Notes - As can be seen from the GC analysis,at this composition,no liquid state could be achieved. Composition Data: Agilent Cerity QA/QC Report Sample name:0818CO2MixVesselGas2 Sample note: Submission time:Monday,August 18,2008 12:18:24 PM Operator: Injection date:Monday,August 18,2008 12:22:16 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 568 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDZA >i \>4 i + i '|A. | L |foeee ek 2 i ;Oo T i]yredir " || . i : |}: 4 i pop r o 7 :i t j : ;|: A an Sine i A Pe a SA aa ne Geen anaes05115225 min TCDSA >!|a i :jae3 i i 4.: l !| i || 'i ; |:: a T T T T T 05 _1 15 2 25 _min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 569 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV's]Amt/Area Amount[]Name 2 0.277 BB 1.4747e+006 5.02281e-005 74.07071 Carbon Dioxide 2 1.247 BB 1.2746e+004 3.88493e-005 0.49518 Sulfur Dioxide 3 1.147 BB 8.2076e+004 1.45198e-004 11.91732 Argon 3 1.698 PB =7.7874e+004 1.83115e-004 14.26000 Nitrogen Total amount =100.74321 Agilent Cerity QA/QC Report Sample name:0818CO2MixVesselGas1 Sample note: Submission time:Monday,August 18,2008 12:18:24 PM Operator: Injection date:Monday,August 18,2008 12:18:47 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 570 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 >i>i o : O 4.__oe . i bi 2" 7 --- 05 2 25 min TCD3A >D4 ;2 |ied.io a :| 4 7 oF !i 74 .t ro ye {: i i ee ee ee ob i ot i |i me wet m i”a :i i bok r r r T t 7 T 7 +T +T -r t os 1 __15 2 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 571 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.277 BB =1.4781e+006 5.02281e-005 74.24185 Carbon Dioxide 2 1.248 BB =1.2389e+004 3.88493e-005 0.48130 Sulfur Dioxide 3 1.148 BB 8.1391e+004 1.45198e-004 11.81779 Argon 3 1.698 PB =7.7275e+004 1.83115e-004 14.15018 Nitrogen Total amount =100.69111 Agilent Cerity QA/QC Report Sample name:0818CO2MixVesselGas3 Sample note: Submission time:Monday,August 18,2008 12:25:43 PM Operator: Injection date:Monday,August 18,2008 12:26:06 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 572 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDZ2A min min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 573 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[iV*s]Amt/(Area Amount[]Name 2 0.277 BB 1.4733e+006 5.02281e-005 74.00295 Carbon Dioxide 2 1.247 BB =1.2655e+004 3.88493e-005 0.49163 Sulfur Dioxide 3 1.148 BB 8.2655e+004 1.45198e-004 12.00136 Argon 3 1.698 PB _7.7681e+004 1.83115¢e-004 14.22462 Nitrogen Total amount =100.72056 Agilent Cerity QA/QC Report Sample name:0818CO2MixVessel4 Sample note: Submission time:Monday,August 18,2008 1:11:10 PM Operator: Injection date:Monday,August 18,2008 1:21:43 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 574 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 25 min 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 575 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.277 BB =1.4688e+006 5.02281e-005 73.77508 Carbon Dioxide 2 1.247 BB 1.3197e+004 3.88493e-005 0.51268 Sulfur Dioxide 3 1.147 BB 8.3768e+004 1.45198e-004 12.16288 Argon 3 1.698 PB =7.8225e+004 1.83115e-004 14.32416 Nitrogen Total amount =100.77481 Agilent Cerity QA/QC Report Sample name:0818CO2MixVessel1 Sample note: Submission time:Monday,August 18,2008 1:10:50 PM Operator: Injection date:Monday,August 18,2008 1:11:13 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 576 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCD2A 2 re ||=ee |:iire]»a - _>A on : yo a5 15 2 25 min TCD3A >i=i i a 2°2,: | fa 1 nnd -; +So ooo OF eee ee eee 0.6 4 15 2.25 _min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 577 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area ['iV*s]Amt(Area Amount[]Name 2 0.277 BB 1.4639e+006 5.02281e-005 73.52727 Carbon Dioxide 2 1.248 BB 1.2771e+004 3.88493e-005 0.49614 Sulfur Dioxide 3 1.148 BB 8.3769e+004 1.45198e-004 12.16311 Argon 3 1.698 PB 7.8376e+004 1.83115e-004 14.35181 Nitrogen Total amount =100.53833 Agilent Cerity QA/QC Report Sample name:0818CO2MixVessel2 Sample note: Submission time:Monday,August 18,2008 1:10:50 PM Operator: Injection date:Monday,August 18,2008 1:14:44 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 578 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCO2ZA vein --s +e oa vo oye -h i ape oe -7 25 min i i i-$ oa . : Loy. : i : at nee - T 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 579 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[liV*s]Amt/Area Amount[]Name 2 0.277 BB 1.4716e+006 5.02281e-005 73.91677 Carbon Dioxide 2 1.247 BB =1.3039e+004 3.88493e-005 0.50655 Sulfur Dioxide 3 1.147 BB 8.3588e+004 1.45198e-004 12.13681 Argon 3 1.698 PB =7.8179e+004 1.83115e-004 14.31585 Nitrogen Total amount =100.87597 Agilent Cerity QA/QC Report Sample name:0818CO2MixVessel3 Sample note: Submission time:Monday,August 18,2008 1:11:09 PM Operator: Injection date:Monday,August 18,2008 1:18:13 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 580 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCD2A { 4 ; -|AOR GE ee 1 2 25 min 1 | '| | i i i i i ! Sooo 0.6 _4 oo 15 2 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 581 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[iiV*s]Amt/Area Amount[]Name 2 0.277 BB =1.4675e+006 5.02281e-005 73.70840 Carbon Dioxide 2 1.247 BB 1.3121e+004 3.88493e-005 0.50973 Sulfur Dioxide 3 1.147 BB 8.3358e+004 1.45198e-004 12.10345 Argon 3 1.697 PB 7.8072e+004 1.83115e-004 14.29626 Nitrogen Total amount =100.61785 Agilent Cerity QA/QC Report Sample name:0818CO2MixVesse!lB4 Sample note: Submission time:Monday,August 18,2008 1:52:10 PM Operator: Injection date:Monday,August 18,2008 2:03:00 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 582 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDZ2A >SS eas ---t-wie a -: .-2 L ='']i ree HEP -" :::: Berea |\'2 Garren ee 4 | ;»HN '::4 ee |,8 es ! Jou:oe! ,'\'i oO ::':i :o :: oc a yo .:be e ar T T T 0.5 1 2 25 min >:: =4 4 , i i i t : | 1 :i 4 : i : |EELS TA a SRR ER Gen ER eRe eee 4 _ 16 2 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 583 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.278 BB =1.3630e+006 5.02281e-005 68.45859 Carbon Dioxide 2 1.243 BB 1.5436e+004 3.88493e-005 0.59969 Sulfur Dioxide 3 1.147 BB 1.0272e+005 1.45198e-004 14.91454 Argon 3 1.697 PB 9.5904e+004 1.83115e-004 17.56148 Nitrogen Total amount =101.53431 Agilent Cerity QA/QC Report Sample name:0818CO2MixVesse!lB3 Sample note: Submission time:Monday,August 18,2008 1:52:10 PM Operator: Injection date:Monday,August 18,2008 1:59:29 PM GC Description:Mlcro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 584 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDZA a ee es cheep es +a 1 :OTR ':| . d :u ...2 a a rs co.a eeAPP Jo.}Ld . nine BO | 8 : oc oor 6 5 .Es : . : 4 . =ooo Se 05 4 15 2 25 min TCD3A > a 4 : o t {i i t 4 ; 2oO iOo-¢o ct:st eerNer 0.6 1 16 2 _..28 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 585 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[!iV*s]Amt/Area Amount[]Name 2 0.278 BB =1.3626e+006 5.02281e-005 68.44190 Carbon Dioxide 2 1.243 BB 1.5367e+004 3.88493e-005 0.59700 Sulfur Dioxide 3 1.146 BB 1.0111e+005 1.45198e-004 14.68084 Argon 3 1.696 PB 9.5698e+004 1.83115e-004 17.52377 Nitrogen Total amount =101.24350 Agilent Cerity QA/QC Report Sample name:0818CO2MixVesselB2 Sample note: Submission time:Monday,August 18,2008 1:52:08 PM Operator: Injection date:Monday,August 18,2008 1:56:00 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 586 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 >4 speed os -pene mee gee -+ a ::j : :i i i :i Hl H i 't i i ! :'t 3 i i H .H i i i a 4 }a i :{t :i :i i i 4 i t r qe 70000.5 1 15 2 25 min TCDS A i j i t q t ;!|7 i i i i :iit } ta]|ifayi:§tL.:|::Y oS -_---_i t i-_-_ 0.5 1 15 2 25 mir] ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 587 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.277 BB 1.3628e+006 5.02281e-005 68.44890 Carbon Dioxide 2 1.243 BB =1.5294e+004 3.88493e-005 0.59417 Sulfur Dioxide 3 1.147 BB =1.0267e+005 1.45198e-004 14.90770 Argon 3 1.697 PB =9.5730e+004 1.83115e-004 17.52955 Nitrogen Total amount =101.48033 Agilent Cerity QA/QC Report Sample name:0818CO2MixVesselB1 Sample note: Submission time:Monday,August 18,2008 1:52:08 PM Operator: Injection date:Monday,August 18,2008 1:52:30 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 588 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 5000pV100005 41 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 589 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area ['iV*s]Amt/Area Amount[]Name 2 0.278 BB =1.3554e+006 5.02281e-005 68.07692 Carbon Dioxide 2 1.239 BB _1.7735e+004 3.88493e-005 0.68900 Sulfur Dioxide 3 1.147 BB =1.0213e+005 1.45198e-004 14.82957 Argon 3 1.697 PB 9.5450e+004 1.83115e-004 17.47834 Nitrogen Total amount =101.07383 Agilent Cerity QA/QC Report Sample name:0818CO2MixVesselC8 Sample note: Submission time:Monday,August 18,2008 2:27:19 PM Operator: Injection date:Monday,August 18,2008 2:38:12 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 590 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Lara10004 -eee eeeeetene foo._ve eed --pF T =- 08 1 25 min > =4 : rat 4 AS 2 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 591 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.278 BB 1.3618e+006 5.02281e-005 68.40100 Carbon Dioxide 2 1.242 BB 1.5562e+004 3.88493e-005 0.60458 Sulfur Dioxide 3 1.146 BB 1.0230e+005 1.45198e-004 14.85411 Argon 3 1.696 PB 9.5547e+004 1.83115e-004 17.49617 Nitrogen Total amount =101.35586 Agilent Cerity QA/QC Report Sample name:0818CO2MixVesselC9 Sample note: Submission time:Monday,August 18,2008 2:41:45 PM Operator: Injection date:Monday,August 18,2008 2:42:07 PM GC Description:Mlcro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 592 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 >Log i :ae nmr ente |,|meee ap -"- mI ; os i BP Cy :i ot :7 WS ' q &4 a 1 ae co ;' |e !| maine | a !| i ee a A REA Ne SR a DE Ee EE'0.6 1 18 2 25 min TCD3A >; =a 7 : q i | i i i :: !a ||: ooo T T _ 1 _15 2 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 593 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.278 BB 1.3645e+006 5.02281e-005 68.53805 Carbon Dioxide 2 1.242 BB 1.5594e+004 3.88493e-005 0.60583 Sulfur Dioxide 3 1.147 BB 1.0169e+005 1.45198e-004 14.76574 Argon 3 1.697 PB =9.5678e+004 1.83115e-004 17.52005 Nitrogen Total amount =101.42967 Agilent Cerity QA/QC Report Sample name:0818CO2MixVesselC10 Sample note: Submission time:Monday,August 18,2008 2:41:45 PM Operator: Injection date:Monday,August 18,2008 2:45:37 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 594 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 ooa ': .ioEARLEGRREEEL SEER EER Gna eens :0.6 1 14 2 25 min TCDSA 2 |So +j a 1 .Hq °. ;A;= con i ':i cn ns i : 7 .i ; i 17 | ;' T --yr r r T r nen |v r v T v r 1 46 2 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 595 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[iV*s]Amt/Area Amount[]Name 2 0.278 BB =1.3620e+006 5.02281e-005 68.40833 Carbon Dioxide 2 1.242 BB 1,.5572e+004 3.88493e-005 0.60496 Sulfur Dioxide 3 1.147 BB 1.0160e+005 1.45198e-004 14.75165 Argon 3 1.697 PB 9.5826e+004 1.83115e-004 17.54715 Nitrogen Total amount =101.31209 Agilent Cerity QA/QC Report Sample name:0818CO2MixVesselC7 Sample note: Submission time:Monday,August 18,2008 2:27:19 PM Operator: Injection date:Monday,August 18,2008 2:34:42 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 596 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDOZ A i ii { i1g ! | an ;or -- 1 1.6 2 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 597 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min] 2 0.278 2 1.242 3 1.147 3 1.697 Total amount =101.59715 Type Area [!iV*s]Amt/Area Amount[] BB BB BB PB 1.3650e+006 5.02281e-005 68.56309 Carbon Dioxide 1.5595e+004 3.88493e-005 0.60585 Name Sulfur Dioxide 1.0256e+005 1.45198e-004 14.89210 Argon 9.5765e+004 1.83115e-004 17.53611 598 Nitrogen Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Run 3 Data: Starting Composition - Trial 1 Trial 2 Trial 3 Average Carbon Dioxide 72.6101 72.72745 72.63673 |72.65809333 Argon 12.37961 12.38764 12.50265 12.4233 Nitrogen 15.11773 15.07068 15.06717 |15.08519333 Sulfur Dioxide 0.4955 0.50175 0.50522 |0.500823333 19 August 2008 - Initial Pressure -850 Initial Temperature -23 Final Pressure -775 Final Temperature 9 Trial 1 Trial 2 Trial 3 Average Carbon Dioxide 73.87559 74.19011 73.78309 |73.94959667 Argon 11.84434 11.75869 11.88194 |11.82832333 Nitrogen 14.24126 14.3507 14.33437 |14.30877667 Sulfur Dioxide 0.48559 0.48084 0.48272 0.48305 Final Gas Composition - Trial 1 Trial 2 Trial 3 Average Carbon Dioxide 73.81936 74.09441 74.08196 |73.99857667 Argon 11.95299 11.86876 11.68538 11.8357] Nitrogen 14.29284 14.28503 14.26931 |14.28239333 Sulfur Dioxide 0.48143 0.49126 0.49198 |0.488223333 Notes - As with the previous run,no liquid state was achieved.This may be attributed to the high composition of the inert species in the system.The inert gases compose of over a quarter of the 599 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 composition by mass of the system. Composition Data: Agilent Cerity QA/QC Report Sample name:0819CO2MixVesselGas2 Sample note: Submission time:Tuesday,August 19,2008 12:15:53 PM Operator: Injection date:Tuesday,August 19,2008 12:16:15 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 600 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 601 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[iV's]AmtArea Amount[]Name 2 0.276 BB 1.4456e+006 5.02281e-005 72.61010 Carbon Dioxide 2 1.250 BB 1.2754e+004 3.88493e-005 0.49550 Sulfur Dioxide 3 1.145 BB 8.5260e+004 1.45198e-004 12.37961 Argon 3 1.693 PB 8.2559e+004 1.83115e-004 15.11773 Nitrogen Total amount =100.60294 Agilent Cerity QA/QC Report Sample name:0819CO2MixVesselGas3 Sample note: Submission time:Tuesday,August 19,2008 12:15:53 PM Operator: Injection date:Tuesday,August 19,2008 12:19:45 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 602 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 603 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.277 BB 1.4479e+006 5.02281e-005 72.72745 Carbon Dioxide 2 1.250 BB =1.2915e+004 3.88493e-005 0.50175 Sulfur Dioxide 3 1.145 BB =8.5316e+004 1.45198e-004 12.38764 Argon 3 1.693 PB =8.2302e+004 1.83115e-004 15.07068 Nitrogen Total amount =100.68752 Agilent Cerity QA/QC Report Sample name:0819CO2MixVesselGas4 Sample note: Submission time:Tuesday,August 19,2008 12:16:05 PM Operator: Injection date:Tuesday,August 19,2008 12:23:16 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 604 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 =:am |:: ol:oy raf .?T N :: ------S-- 05 2 25 min >.|= :: .7 :! °| | ; 7 7 TET a a T T T T T 05 1 _15 2 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 605 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.277 BB 1.4461e+006 5.02281e-005 72.63673 Carbon Dioxide 2 1.249 BB 1.3005e+004 3.88493e-005 0.50522 Sulfur Dioxide 3 1.145 BB =8.6108e+004 1.45198e-004 12.50265 Argon 3 1.693 PB 8.2282e+004 1.83115e-004 15.06717 Nitrogen Total amount =100.71178 Agilent Cerity QA/QC Report Sample name:0819CO2MixVesselA1 Sample note: Submission time:Tuesday,August 19,2008 1:26:44 PM Operator: Injection date:Tuesday,August 19,2008 1:27:06 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 606 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCD2A >go...:el dee a a.oe vta,+..|:i i 4 tea eee ie.toe "4:oie aa ::::i :i i ''' :|:}i 4 sR eek 4 -...iS o ':.!i 'B qi tee aoe woe ee beet t i _2 ene chine ns L N ,t Hq qocni sd a :j .i : : :i i :Pots :+:i yon.en 7 i .:j i .:i ;4 rss \|"+ i : o 4 -nn "+:a io an i : é r 7 +T 1 T T 7 T 7 7 7 + 0s 1 15 2 25 min TCDS A py- t ; i ce ' i ' bo i :' :i :i :4 Sn AEE SE A A SE A a ee ee re ee es eee en ee ee os 4 15 2 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 607 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.276 BB =1.4708e+006 5.02281e-005 73.87559 Carbon Dioxide 2 1.249 BB =1.2499e+004 3.88493e-005 0.48559 Sulfur Dioxide 3 1.146 BB 8.1574e+004 1.45198e-004 11.84434 Argon 3 1.694 PB 7.7772e+004 1.83115e-004 14.24126 Nitrogen Total amount =100.44678 Agilent Cerity QA/QC Report Sample name:0819CO2MixVesselA2 Sample note: Submission time:Tuesday,August 19,2008 1:27:48 PM Operator: Injection date:Tuesday,August 19,2008 1:30:36 PM GC Description:MIcro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 608 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCO2A >4 "4 .a.a =i :a 1 :{H 4 4 : jl i i cee 4 +4-; i }| 9BA :ot 'coy :!j| i t i :{i 3 :5 ee! "i 4 ! :|i |!| r ' ;j i +1 {{iti ': i } q J J u T 0.6 1 15 2 25 min TCD3 A >i i ' a J jee klde i Le :i ;{!iae-4 wk. i {i f 2 2 !H o -i i ! q +iv i t \ '!i i j i : '3 \i F i g |: oa tOo3 N !.5 r 7 +r T +r r -T 7 +++T r r 7 +T +”7 +T + 0.6 4 15 2 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 609 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[iV's]Amt/(Area Amount[]Name 2 0.276 BB 1.4771e+006 5.02281e-005 74.19011 Carbon Dioxide 2 1.250 BB =1.2377e+004 3.88493e-005 0.48084 Sulfur Dioxide 3 1.146 BB 8.0984e+004 1.45198e-004 11.75869 Argon 3 1.694 PB 7.8370e+004 1.83115e-004 14.35070 Nitrogen Total amount =100.78034 Agilent Cerity QA/QC Report Sample name:0819CO2MixVesselA3 Sample note: Submission time:Tuesday,August 19,2008 1:27:49 PM Operator: Injection date:Tuesday,August 19,2008 1:34:11 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 610 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 >4 wees Sed -4 i :a :am :i .i 1 H en ||3 rn oe [ :'''j H i Lobe f a a is i:roe :i '2 oeHed-4 eee mene nn mee foes -oe a fo N :i .i |i t 1 t -a bore te Roe ot f.-ib ' i ::{: ::::t :i oes ||) oe | ::i :;H ::ep cde ce hoe |-; od-.ne . '.i £i :i H i i 4 -::>t i i 'i i i ,rn wed i i wet 7 t '7 T -7 T T "r T TCDS A }!H : i : oa eke gee ee ee wee {t :::i :: ::t ! ;iit |' :i i t:i !I |: 7 q Li iM LI v Lf - 0.5 we 1 A8 2 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 611 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV's]Amt/Area Amount[]Name 2 0.276 BB =1.4690e+006 5.02281e-005 73.78309 Carbon Dioxide 2 1.249 BB 1.2426e+004 3.88493e-005 0.48272 Sulfur Dioxide 3 1.145 BB 8.1833e+004 1.45198e-004 11.88194 Argon 3 1.693 PB 7.8281e+004 1.83115e-004 14.33437 Nitrogen Total amount =100.48213 Agilent Cerity QA/QC Report Sample name:0819CO2MixVesselB1 Sample note: Submission time:Tuesday,August 19,2008 1:59:44 PM Operator: Injection date:Tuesday,August 19,2008 2:00:05 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 612 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDZ2A 05 1 415 2 25 ;mir ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 613 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.276 BB 1.4697e+006 5.02281e-005 73.81936 Carbon Dioxide 2 1.250 BB 1.2392e+004 3.88493e-005 0.48143 Sulfur Dioxide 3 1.146 BB 8.2322e+004 1.45198e-004 11.95299 Argon 3 1.695 PB =7.8054e+004 1.83115e-004 14.29284 Nitrogen Total amount =100.54662 Agilent Cerity QA/QC Report Sample name:0819CO2MixVesselB2 Sample note: Submission time:Tuesday,August 19,2008 1:59:44 PM Operator: Injection date:Tuesday,August 19,2008 2:03:35 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 614 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Peoo:;1i+.11ia.;FSa'.aeeearn25 min TCDSA pVSTETE EEEIA:InARRIE AEEEEEEL AR REE REESE AEE RE UR A MU a AU en pee een eee ene eee ee 0.6 1 15 2 25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 615 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[!iV's]Amt/Area Amount[]Name 2 0.276 BB =1.4752e+006 5.02281e-005 74.09441 Carbon Dioxide21.249 BB 1.2645e+004 3.88493e-005 0.49126 Sulfur Dioxide 3 1.146 BB 8.1742e+004 1.45198e-004 11.86876 Argon 3 1.694 PB 7.8011e+004 1.83115e-004 14.28503 Nitrogen Total amount =100.73946 Agilent Cerity QA/QC Report Sample name:0819CO2MixVesselB3 Sample note: Submission time:Tuesday,August 19,2008 2:00:00 PM Operator: Injection date:Tuesday,August 19,2008 2:07:05 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 616 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDZ2A :[| 7 A v i i : 1 i t '2 - 06 1 2 25 min >'as]Lk oO 4 a r \i :| i t i |{3||8Qo $:oOo i i9 artee 08 _4 oe 15 2.25 min ESTD Report Calibration last saved:Monday,August 18,2008 10:39:40 AM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 617 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min] 2 0.276 2 1.249 3 1.145 3 1.694 Total amount =100.52863 Type Area [!iV*s]Amt/Area Amount[] BB BB BB PB 1.4749e+006 5.02281e-005 74.08196 1.2664e+004 3.88493e-005 0.49198 8.0479e+004 1.45198e-004 11.68538 7.7925e+004 1.83115e-004 14.26931 618 Name Carbon Dioxide Sulfur Dioxide Argon Nitrogen Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Run 4 Data: Starting Composition - Trial 1 Trial 2 Trial 3 Average Carbon Dioxide 92.06266 91.58212 92.09044 91.91174 Argon 4.39712 4.46013 4.38982 4.41569 Nitrogen 5.12252 5.0095 4.85768 |4.996566667 Sulfur Dioxide 0.19213 0.19282 0.22088 |0.201943333 21 August 2008 - Initial Pressure -850 Initial Temperature -23 Final Pressure -800 Final Temperature -9 Trial 1 Trial 2 Trial 3 Trial 4 Average Carbon Dioxide |97.55802 96.74931 96.58062 95.24626 |96.5335525 Argon 1.45757 1.68719 1.86735 2.54299 1.888775 Nitrogen 1.51478 1.78556 2.0046 2.72349 2.0071075 Sulfur Dioxide 0.54604 0.53469 0.52184 0.48112 0.5209225 21 August 2008 - Initial Pressure -N/A Initial Temperature -N/A Final Pressure -600 Final Temperature -8 Trial 1 Trial 2 Trial 3 Trial 4 Average Carbon Dioxide |89.89933 89.89379 89.77933 90.02839 89.90021 Argon 5.08853 5.02972 5.09918 5.06462 5.0705125 Nitrogen 5.8694 5.77133 5.85351 5.84141 5.8339125 Sulfur Dioxide 0.12327 0.1252 0.1237 0.12151 0.12342 619 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Final Gas Composition - Trial 1 Trial 2 Trial 3 Trial 4 Average Carbon Dioxide |89.76122 89.96137 89.9332 90.10985 89.94141 Argon 5.04085 5.03903 5.02298 5.01807 5.0302325 Nitrogen 5.78458 5.77701 5.78137 5.73679 5.7699375 Sulfur Dioxide 0.12436 0.12587 0.12607 0.12691 0.1258025 Compostion Data: Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2ArVesselGas5 Sample note: Submission time:Thursday,August 21,2008 11:28:28 AM Operator: Injection date:Thursday,August 21,2008 11:28:53 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 620 ijenFnSe i i.| ' 1 i i : I i | Lj Lf v qT 4 15 2 25 min TCD3A tee Bi .L.§ae nee ss 4aeeeA2-0 |: @ |aensae ;ro a) L rs 2 i as ee fe ai..i a i L 1 T T T T T r 06 1 15 2.25 min ESTD Report - Calibration last saved:Thursday,August 21,2008 2:17:46 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 621 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.274 BB =1.8329e+006 5.02281e-005 92.06266 Carbon Dioxide 2 1.302 BB 4945.41242 3.88493e-005 0.19213 Sulfur Dioxide 3 1.229 PB 3.0284e+004 1.45198e-004 4.39712 Argon 3 1.579 BB =_.2.7974e+004 1.83115e-004 5.12252 Nitrogen Total amount =101.77443 Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2ArVesselGas6 Sample note: Submission time:Thursday,August 21,2008 11:35:04 AM Operator: Injection date:Thursday,August 21,2008 11:35:28 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 622 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 °a-_>=deinecaeagenosesa=aiNeNamin z24-_cette be oo Go ad ce eeevadji: jife.He i i 7 4 is cone te iz .se:er Pod er GM FY Qe ; ae /:: a : .:\:\:£}.{i ipeedced;ts '[ws]:'|::ao :i :i ''Qo Ae 1 von t _Bee aL.i a o i .i i07 | «oft ::' i :i ' : |f i :i eed lk 2 4 Leo i a to:|; ----i i [eR]1 16 2 25 _min ESTD Report Calibration last saved:Thursday,August 21,2008 2:17:46 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 623 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/(Area Amount[]Name 2 0.274 BB 1.8233e+006 5.02281e-005 91.58212 Carbon Dioxide 2 1.301 BB 4963.19190 3.88493e-005 0.19282 Sulfur Dioxide 3 1.235 PB =3.0718e+004 1.45198e-004 4.46013 Argon31.600 PB 2.7357e+004 1.83115e-004 5.00950 Nitrogen Total amount =101.24456 Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2ArVesselGas7 Sample note: Submission time:Thursday,August 21,2008 11:41:21 AM Operator: Injection date:Thursday,August 21,2008 11:41:43 AM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 624 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 >'\}a :i i 2 !|ionoeavnencbey}2 iri'iiciz =i :; wee eed ro ;eek Ae. 5 :: : Kr i :[-:i c IN :4 :3 i i :i oo ------<+--r 06 1 15 2 25 min TCD3A 2 4 .-eee ree edie ras re '|'oO |= :oO!, : '2M.6....@..o :7!o |:::ba i=]. :S a _sted eee ceceap eect ee eee ete Q ;ad i !i.- | qT tT 7 7 T i =T 05 1 15 2 25 min ESTD Report Calibration last saved:Thursday,August 21,2008 2:17:46 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 625 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!IV*s]Amt/Area Amount[]Name 2 0.274 BB =1.8334e+006 5.02281e-005 92.09044 Carbon Dioxide 2 1.297 BB 5685.65401 3.88493e-005 0.22088 Sulfur Dioxide 3 1.238 PB 3.0233e+004 1.45198e-004 4.38982 Argon 3 1.616 PB 2.6528e+004 1.83115e-004 4.85768 Nitrogen Total amount =101.55883 Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2MixVessel1-5 Sample note: Submission time:Thursday,August 21,2008 12:32:06 PM Operator: Injection date:Thursday,August 21,2008 12:32:30 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 626 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Bon :| ] coke .-4 °4oOJaeonadeeeeeeeSenneatewdteceeod aaa e weoOoesd' N ne : re "i -F eae rn eect 2)ee ae : °i ! i-.a ee ee a i es 7 T ++7 T 7 .---y T ?++r T +7 +T r 7 06 1 15 2 25 min TCO3A 2 i a i:2 i i :<::=1 a &.2 a R i :(oor j i ': °:g :ioOwheea-aoe re -=cp eeSo1ag: {| T T -T T T 05 1 15 2 25 min ESTD Report Calibration last saved:Thursday,August 21,2008 2:19:43 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 627 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[iV's]Amt/Area Amount[]Name 2 0.273 BB 1.8963e+006 5.02281e-005 95.24626 Carbon Dioxide 2 1.276 BB =:1.2384e+004 3.88493e-005 0.48112 Sulfur Dioxide 3 1.261 PB 1.7514e+004 1.45198e-004 2.54299 Argon 3 1.723 PB 1.4873e+004 1.83115e-004 2.72349 Nitrogen Total amount =100.99385 Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2MixVessel1-2 Sample note: Submission time:Thursday,August 21,2008 12:08:27 PM Operator: Injection date:Thursday,August 21,2008 12:12:15 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 628 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCD2A >i 1 ::=4 4 i .i |::ieeeedGRE.eee eee ee ee ge ee ge 4.i 7:ob | i ::meee |3 eee a be L.: 9So L _L bh.ee i aeq| 4 ;os :1 - .y ;i i a | Codes ' T "T T ."1 7 0.5 1 15 2 25 min TCDSA 21 As et "oO!:= : _%:= 1 @:4 = a 3vbaeFLTheo: 2 : i ; [=]::[a]:i :ioOo:i.wee bee i 9 :{|::©| T T T T i 06 1 1.5 _2 25 ___min ESTD Report Calibration last saved:Thursday,August 21,2008 2:19:43 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 629 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[!iV's]Amt/Area Amount[]Name 2 0.273 BB =1.9423e+006 5.02281e-005 97.55802 Carbon Dioxide 2 1.274 BB =1.4055e+004 3.88493e-005 0.54604 Sulfur Dioxide 3 1.253 PB 1.0039e+004 1.45198e-004 1.45757 Argon 3 1.684 PB 8272.29121 1.83115e-004 1.51478 Nitrogen Total amount =101.07641 Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2MixVessel1-3 Sample note: Submission time:Thursday,August 21,2008 12:16:58 PM Operator: Injection date:Thursday,August 21,2008 12:17:22 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 630 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDZA bw .2 |re :| K :l :B @}--7--4 se -wee deee oe ol 1 wep dee heed :| S W i ':ay foo ore $e -as eeeracan ban moa|,i :i vee g rr cere ee eae b N |i D 7 ; i ' : ; i iiiv * i i :os :mE! |;| T t T T T 06 1 15 2 25 min TCDSA >_aw Fed wee Gin ee a i eeeeg eee2:fe 'a ne ; F 4 a r CMG =|| +_.i .+be1)': on)rr 1BTbl a }:i ;| 1: ;a "ft 3 : '?: o i : 3 !|: o St ; a - 'T T rT r Ls Ls tT r rT T t T rT r t r T Tv T ¥r T rT a T T 05 1_15 -2 25 min ESTD Report Calibration last saved:Thursday,August 21,2008 2:19:43 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 631 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.273 BB =1.9262e+006 5.02281e-005 96.74931 Carbon Dioxide 2 1.274 BB =1.3763e+004 3.88493e-005 0.53469 Sulfur Dioxide 3 1.255 PB 1.1620e+004 1.45198e-004 1.68719 Argon 3 1.695 PB 9751.01374 1.83115e-004 1.78556 Nitrogen Total amount =100.75674 Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2MixVessel1-4 Sample note: Submission time:Thursday,August 21,2008 12:23:18 PM Operator: Injection date:Thursday,August 21,2008 12:23:39 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 632 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCD2A >:.ae \4a4iue:i ;:ee) "|i!| tr "TE a?4:.7 ft ,7 4 ':i |:i : :cepe ede i L. .,t t H ,o ::;::9 Jj _ae eb Fy nee see de3]if |i |i { N my .t ,: 4 sete i i a. |)on || |cone i ; :ce i i i :ae :i necetcgeeene a oa Bb -_as +o een -.-.cod -- Do ||: pot kd ;: --T Tl T T T 06 1 15 2 25 min wllit}|tItifoo.vue|Vrs\.qVFO?«Nie|{Hl}|f|ttESTD Report Calibration last saved:Thursday,August 21,2008 2:19:43 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 633 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[!iV*s]Amt/Area Amount[]Name 2 0.273 BB =1.9228e+006 5.02281e-005 96.58062 Carbon Dioxide 2 1.274 BB 1.3432e+004 3.88493e-005 0.52184 Sulfur Dioxide 3 1.257 PB 1.2861e+004 1.45198e-004 1.86735 Argon 3 1.707 PB 1.0947e+004 1.83115e-004 2.00460 Nitrogen Total amount =100.97440 Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2MixVessel2-4 Sample note: Submission time:Thursday,August 21,2008 1:11:32 PM Operator: Injection date:Thursday,August 21,2008 1:11:53 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 634 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDZA >4 '4 OF i bol L | . ,re oO e io+-+->-t [eer ee eo 0.6 1 15 2 25 min TCDSA 2 |A os BD o -Pn.ey eeBN 4 : o Done.4 tO.: BR |7 post Rt 7 :i om :i 4 ... +a a oe ee ee ee es oe ee ee oe 0.6 _ {15 2 25 _.__min ESTD Report Calibration last saved:Thursday,August 21,2008 2:21:23 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 635 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.274 BB =1.7924e+006 5.02281e-005 90.02839 Carbon Dioxide 2 1.299 BB 3127.60414 3.88493e-005 0.12151 Sulfur Dioxide 3 1.270 PB 3.4881e+004 1.45198e-004 5.06462 Argon 3 1.777 PB 3.1900e+004 1.83115e-004 5.84141 Nitrogen Total amount =101.05593 Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2MixVessel2-2 Sample note: Submission time:Thursday,August 21,2008 12:55:29 PM Operator: Injection date:Thursday,August 21,2008 12:55:52 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 636 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 i4i4Hi|'{i :i Bnennct cote fod not mt deren te wah coterie tines bone :!{: :i |:i _royco ,i oF{}it1i :H at i i ;|i ,iH . -ote on -- min 1=f-wopoopsenmorseperssrsoeeo>ReneS[eenennevaneaf;..acs :2 = :':1.ts |-_|'7 :Oe 4 \rr.;7 1:} :t :co ( :rc :J.i ',om.| +j ian + 1 }t aT i r :sy}i Poo i : t {t Sr .t :; i es 2 wien od pre nen enpee E i - T T T T TT min ESTD Report Calibration last saved:Thursday,August 21,2008 2:21:23 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 637 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.274 BB 1.7874e+006 5.02281e-005 89.77933 Carbon Dioxide 2 1.299 BB 3183.99595 3.88493e-005 0.12370 Sulfur Dioxide 3 1.267 PB 3.5119e+004 1.45198e-004 5.09918 Argon 3 1.757 PB 3.1966e+004 1.83115e-004 5.85351 Nitrogen Total amount =100.85571 Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2MixVessel2-1 Sample note: Submission time:Thursday,August 21,2008 12:45:40 PM Operator: Injection date:Thursday,August 21,2008 12:45:59 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 638 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 :a oo a0 nn nn en eee ee ee ee 0.5 4 15 2 25 min TCDZA 1 &.bee tg oe :19,Po ZL.; .Fog:7 poops te ' oe r _ i a -wee bees ce ee i -eer weed ep -;foL:a . 4 7 i os bow bo.te 4 _at i cad 4 : 7 Sn nny r 0.6 41 _15 2 26 sami ESTD Report Calibration last saved:Thursday,August 21,2008 2:21:23 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 639 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area[!iV*s]AmtArea Amount[]Name 2 0.274 BB 1.7897e+006 5.02281e-005 89.89379 Carbon Dioxide 2 1.300 BB 3222.60332 3.88493e-005 0.12520 Sulfur Dioxide 3 1.265 PB 3.4640e+004 1.45198e-004 5.02972 Argon 3 1.743 PB 3.1517e+004 1.83115e-004 5.77133 Nitrogen Total amount =100.82003 Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2MixVessel2-3 Sample note: Submission time:Thursday,August 21,2008 1:00:07 PM Operator: Injection date:Thursday,August 21,2008 1:00:31 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 640 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 | i _a4 weet 5 ;: i : Hf|: :: ;oy }:in . 1 ,,i 'i _rr'i ennens ee ce .;: :oe |.,.tee .j t i ..: : T tT rT T 1 15 2 25 min TCD3A Cc :bo Bt teed oeeeerey fe weed - |*:., Y :t-root og,sat p = |ts) ::.-O ..f., : i ,ied : :;:Lr ; :{mF i”so ra . *i 5 .. a 4 L i ii toe i '.a -+--+'fa --T -r -ee!. 06 1 15 _2.25 min ESTD Report Calibration last saved:Thursday,August 21,2008 2:21:23 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 641 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.274 BB 1.7898e+006 5.02281e-005 89.89933 Carbon Dioxide 2 1.299 BB 3172.90292 3.88493e-005 0.12327 Sulfur Dioxide 3 1.268 PB 3.5045e+004 1.45198e-004 5.08853 Argon 3 1.763 PB 3.2053e+004 1.83115e-004 5.86940 Nitrogen Total amount =100.98051 Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2MixEnd2 Sample note: Submission time:Thursday,August 21,2008 1:18:47 PM Operator: Injection date:Thursday,August 21,2008 1:22:30 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 642 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 >!j .=a t i } ]r 4 ; |: oOo fo f 2 '7 i ;. Mole ed !I.i HA t . ||oe ne .+ ofo]: : So dee .a _ -ere --_--_-_- 06 1 15 4 25 min TCDSA =Bn hence terete cane bres en -Nitrggen4.2731,a;.i1.790.?||wee eee bon |i]|4!t{ji{|$f}IIiaan EEE AIEEE AEE EERSTE GEESE ER SER EA EE EE EER ER A Ieee eee eee 06 1 16 2 25 min ESTD Report Calibration last saved:Thursday,August 21,2008 2:23:25 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 643 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.274 BB 1.7911e+006 5.02281e-005 89.96137 Carbon Dioxide 2 1.298 BB 3240.07974 3.88493e-005 0.12587 Sulfur Dioxide 3 1.273 PB 3.4705e+004 1.45198e-004 5.03903 Argon 3 1.790 PB 3.1548e+004 1.83115e-004 5.77701 Nitrogen Total amount =100.90328 Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2MixEnd3 Sample note: Submission time:Thursday,August 21,2008 1:18:48 PM Operator: Injection date:Thursday,August 21,2008 1:26:01 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 644 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 +a on ne nene nen!a 4 15 2 25 min TCD3A i Cc CcPoRes@{-_1 tfn.7 fo - i :/oN ::Poo 3 Lobe. S|7 i . t *LJ T 0.6 1 15 2_25 min ESTD Report Calibration last saved:Thursday,August 21,2008 2:23:25 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 645 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV*s]Amt/Area Amount[]Name 2 0.274 BB 1.7905e+006 5.02281e-005 89.93320 Carbon Dioxide 2 1.298 BB 3244.98722 3.88493e-005 0.12607 Sulfur Dioxide 3 1.273 PB 3.4594e+004 1.45198e-004 5.02298 Argon 3 1.794 PB 3.1572e+004 1.83115e-004 5.78137 Nitrogen Total amount =100.86361 Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2MixEnd4 Sample note: Submission time:Thursday,August 21,2008 1:18:49 PM Operator: Injection date:Thursday,August 21,2008 1:29:33 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 646 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Neata3]-1797--aodi|||i[ee 0.6 4 18 2 26 _-min ESTD Report Calibration last saved:Thursday,August 21,2008 2:23:25 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 647 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min]Type Area [!iV's]Amt/(Area Amount[]Name 2 0.274 BB 1.7940e+006 5.02281e-005 90.10985 Carbon Dioxide 2 1.298 BB 3266.61561 3.88493e-005 0.12691 Sulfur Dioxide 3 1.273 PB 3.4560e+004 1.45198e-004 5.01807 Argon 3 1.797 PB =3.1329e+004 1.83115e-004 5.73679 Nitrogen Total amount =100.99162 Agilent Cerity QA/QC Report Sample name:*Reprocessed:0821CO2MixEnd1 Sample note: Submission time:Thursday,August 21,2008 1:18:39 PM Operator: Injection date:Thursday,August 21,2008 1:18:58 PM GC Description:Micro GC -SN:CN10804010 Signal description:TCD2 A;TCD3 A Method:Aug18Cal Method last saved:Monday,August 18,2008 11:01:59 AM 648 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 TCDZA tA. i whee ee {t -3 at i ; :|:H |i 2 25 minohod|4 *-2 doe Pe : eee:££a es as aa eee a aan _sbene crrnteetes ds wanes .pr all .Ls{!ato.BL.te af :|Do,:B |: j o :: a Bee ij t rr 'i i need 4 : : .|.i a ae i a i b- | ;'i :{"t i ;: 4 :: 4 boot l.L. T T T i T -- 0.5 1 15 2 25 min ESTD Report Calibration last saved:Thursday,August 21,2008 2:21:23 PM Multiplier:1.0000 Dilution:1.0000 Sample amount:0.0000 Sample type:Sample 649 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Sampling source:Inlet Signal Retention Time [min] 2 0.274 2 1.298 3 1.273 3 1.786 Total amount =100.71101 Type Area [!iV*s]Amt/Area 1.7871e+006 5.02281e-005 89.76122BB BB PB PB 3200.99341 3.88493e-005 0.12436 3.4717e+004 1.45198e-004 5.04085 3.1590e+004 1.83115e-004 5.78458 650 Amount []Name Carbon Dioxide Sulfur Dioxide Argon Nitrogen Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Appendix E:Synthesis,characterization and SO;oxidation behavior of noble metal loaded (Pt,Pd)on mixed oxide support (Al,O3-TiO,) I.Catalyst support composite synthesis 1.1 Synthesis of mixed oxide (Al,Q3-TiO;): Reverse micelle method has been adopted for the preparation of mixed oxides supports. In this method,an equimolar ratio of aluminum and titanium precursors have been taken in a reverse micelle with AOT (Sodium bis(2-ethylhexyl)sulfo-succinate in iso-octane.Water/oil ratio was kept constant as 15.The precipitating agent was NH4OH in AOT reverse micelle.The detailed synthesis procedure is given in Scheme 1.The solution is centrifuged to separate the precipitate.The sample is then dried and calcined at different temperatures (500,650,750 and 900 °C)in oxygen atmosphere at 3 °C/min.The calcined samples were characterized using scanning electron microscopy (SEM-EDS)and X-ray diffraction (XRD). Scheme 1.Reverse method synthesis of mixed oxide support Al,03-TiOp, 651 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 0.1M Titanium . 0.1M Aluminum (isopropoxide)1 'hydroxidechlorideininDiwater1MHCIinDiwater. Add drop by drop Add drop by drop Add drop by drop q y 0.1 M AOT 0.1 M AOT 0.1 M AOT in in Isoctane in Isoctane Isoctane J Ultrasonicate for1 hour |Ultrasonicate for1 hour | White colloid White colloid White colloid |Add drop by drop | Ultrasonicate for 1 hour White colloid |Add drop by drop White ppt A at 150 C overnight White powder 1.2 Noble metal (Pt and Pd)loading on mixed oxide (Al,03-TiOQ>): Wet impregnation method has been adapted to load 5 wt%of Pt and Pd on the mixed oxide support prepared by the above method.125 ml of 100 ppm solution H2PtCl¢.6H20 (PdCl, was used as the Pd source)was added to 250 mg of mixed oxide sample stirred and heated to 90 °C until the solution evaporates.The metal loaded samples were reduced under Hz atmosphere for 3 h at 450 °C to obtain metallic Pt or Pd loaded on the mixed oxides.Characterization of the support and metal deposits over the support was performed by SEM and XRD prior to SQ) oxidation. II.Characterization using SEM,XRD,adsorption studies 652 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 (BET &Pulse chemisorption of H2) 2.1 Characterization of mixed oxide (Al,O3-TiO2)support: The synthesized mixed oxides were analyzed by SEM-EDS to find the surface morphology and the composition.Figure 1 shows the SEM image of the support.The formation of a porous structure is evident as shown in the circled regions.A qualitative analysis using EDS shows an equal ratio between Ti and Al.This suggest equimolar ratio of Al,O3 :TiO in the mixed oxide composite. p 2 4 8 8 10 12 14 16 18 Full Scale 2926 cts Cursor.0.000 ke' XRD has been carried out to find the crystalinity of the prepared mixed oxides.Figure 2 shows the XRD of support calcined at different temperatures (500,650,750 and 900 °C).As the calcination temperature increases,there is change in phase from amorphous to crystalline. Crystalline phase of both TiO2 and Al2O3 are observed at 900 °C.In the 900 °C calcined samples the formation of rutile peak becomes predominant. 653 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 #TiO,rutile #21-1276*TiO,Anatase#21-1272 (a)500 °C$AIO,#10-0173 (b)650°C (c)750 °C "(d)900 °C Intensity(a.u)20 30 40 50 60 70 80 20 Figure 2.XRD pattern of in-house support calcined at different temperature. BET single point specific surface area (SSA)has been calculated by physisorption of nitrogen using Micromeritics chemisorb 2720.Nitrogen and helium (30%and 70%)mixture has been used for this study at liquid Nz temperature.Figure 3 shows reduction in surface area with increase in calcination temperature.The insert of Figure 3 provides an estimate of the change in surface area with temperature.The decrease in surface area due to temperature can be attributed to the sintering and agglomeration of particles at higher temperature. 654 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 "att Single point 1 Support calcination 300 =temperature of ae eneAl,O,-TiO,(°C)(m?/e) =250 -500 220 £oO 7 650 161 5 200-750 70 3 4 . 500 10 t 150- ba]"”-_tu 100tf 4 | " 50 0 i t |T T T : 500 600 700 900 Temperature (°C) Figure 3.BET surface area of the in-house prepared support. 2.2 Characterization of the catalyst composite: Figure 4 shows the SEM image and XRD of Pt-loaded on the inhouse synthesized Al203- TiO,support.The porous nature of the support was maintained after loading the Pt metal as well. The circle in the image indicates the Pt particles dispersed on the support.XRD shows the presence of metal deposits over the inhouse support.The Pt is zero valent state confirming the metallic form and a 20 angle =39.8 corresponds to (111)plane,46.39 corresponds to (200)plane and 67.7 corresponds to the (220)plane of Pt (JCPDS #87-0640).The peaks correspond to the underlying support remains intact confirming that the crystalline nature of the support is not altered after the Pt-loading. 655 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 Pt JCPDS #87-0640 Pt-inhouse support Pt (111)Pt (220)Intensity(a.u.)40-4 Inhouse support 20- *T Mi T tT LU v T r 20 30 40 50 60 70 80 Figure 4.SEM and XRD of Pt loaded in-house support. Hydrogen pulse chemisorption using Micromeritics chemisorb 2720 has been carried out to determine the catalyst (Pt)dispersion and metallic surface area.Supports calcined at high temperatures result in lower dispersion and more agglomeration of Pt.This results in a decrease in the active surface area of the Pt catalyst.Table 1.provides the details about the metal dispersion and metallic surface area for supports calcined at different temperatures. Table 1.Pulse hydrogen chemisorption data for the Pt loaded on different support. Pt/AhO3-TiO,Diameter of Metallic Metallic F "oftheparticle surface area Support calcination P Dispersion (SA)/gm of temperature (°C)(nm)sample (m'/g metal) 500 3.8 29.12 3.6 71.9 650 8.04 14 1.73 34.7 656 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 750 14.25 7.94 0.98 19.62 900 856 0.132 0.0163 0.3266 IIT.SO,oxidation kinetics 3.1 Experimental protocol for SO;oxidation: A quartz tube with an inflated middle section that contains a ceramic frit to avoid the loss of catalyst during gas flow was used as the reactor. Schematic representation of the quartz reactor: ¢scm >oD=14mm ID=4.06 mm t ID=8.8mm OD=6.36mm |4 «70cm > 200 mg of sample is loaded in the reactor before it is placed inside the tubular furnace The temperature of the furnace can be programmed to ramp from 100 °C to 700 °C. Reactor set up: 657 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 :vO 4 'TI Ea Lip Ot e a Fi,BA 4 *.on .+-AN Sy:"4iGaraN 4ae Hla2 ” e Simulation of flue gases: The flue gas composition is as follows:The total flow rate as 100 ml min'and the feed gas composition as 10%SO»,11%O2,and 79%No.The exit gas concentration is measured while the temperature is steady during the reaction. e The gas coming out of the reactor is collected in a gas collector and 30 microliter of gas is injected to Gas Chromatography (GC). e The GC is equipped with column "Gaspro”(Agilent Technologies)which can detect SO and other gases. e GC conditions as follows: **Helium was used as the carrier gas.A TCD (thermal conductivity detector)mode was adopted while the temperature was ramped from 50 to 200 °C,SQ?has a (retention time)RT of 10 min in the gas chromatogram. The details of the calculations and the procedure adopted to calculate the percentage of conversion from the GC data is given in Appendix Table A1.The same procedure is adopted for all the samples.The Al,03-TiO,demonstrates a conversion of 7.3 %without Pt,whereas Pt loading causes this conversion to increase to 34 %at 400 °C.This is an improvement of 78 % in the conversion of SO;in the presence of Pt. 3.2 Comparison with commercial catalyst: SO,oxidation at various temperatures for Pt loaded on Al,O3-TiO2 prepared by micro emulsion method was compared to a commercial aluminum titanate powder purchased (Aldrich, Catalog #520209).5 wt%Pt loading on commercial sample was carried out by wet 658 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 impregnation method.The comparison between our sample and commercial sample has been evaluated.The maximum SO),conversion of 18%was observed at 700 °C for the commercial catalyst,whereas the in-house catalyst shows a maximum activity of 40%at a significantly lower temperature of 400 °C.Thus an increase of 60%in SO,conversion is demonstrated when the in-house synthesized mixed oxide is used as the catalyst support compared to the commercial catalyst. 3.3 Comparison between Pt and Pd metal catalyst: The comparison of the effects of Pt and Pd loaded commercial samples is currently being performed.Commercial supports loaded with Pt by wet impregnation shows 5%conversion at 400 °C.Similar experiments with Pd loaded over commercial supports are yet to be done.Table 2 provides the percentage conversion data of SO2 oxidation using Pt and Pd catalyst supported over in-house Al,03-TiO2.The maximum conversion of 40%has been obtained at 400 °C for Pt catalyst deposited over a support calcined at 750 °C.Both Pt and Pd shows a maximum conversion when a mixed oxide calcined at 750 °C was used as the support for these metals.The preliminary results reported so far indicates a 30%higher conversion using Pt compared to the Pd catalyst. Table 2.Percentage of SO2 oxidation on Pt and Pd loaded in-house support,support calcined at different temperature. Catalyst %of conversion calicnation temperature of 5 Wt%Pt catalyst 5 Wt%Pd catalyst AlO3-TiO2 (°C) 500 34 17 650 36 19 659 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 750 40 28 900 20 14 commercial 18 to be done 3.4 Stability of the catalyst: The long term stability of the catalyst has been tested using the Pt-deposited over Al2O3- TiO,calcined at 750 °C.The composite shows an increase in SO2 conversion with respect to time during the first 11 hrs of operation from 47%to 70%.After 11 hrs the conversion remains stable up to 15 hr at 70%conversion.The catalyst is stable for 26 hrs of operation as shown in Figure 5.The percentage conversion with time for the Pt loaded catalyst at a reaction temperature 400 °C is shown in Figure 5. Figure 5.Plot of percentage conversion of SO)vs.time at 400 °C reaction temperature. 660 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 100 90-%ofSo,conversionanQol0 T T T T T r T T T 0 5 10 15 20 25 Time (hours) 661 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 4.Highlights of the research:°,reA simple method for the synthesis of a mixed oxide support consisting of TiO2 and Al,O3 using a reverse micelle method has been developed. Calcination of the support at 750 °C shows an oxide with a low rutile phase (rutile phase is detrimental for metal dispersion and SO;oxidation). The inhouse synthesized supports show a much better Pt utilization.A stable SQ: conversion of 40 %was noted with Pt catalyst deposited over support calcined at 750 °C. This conversion is significantly higher (80%)than the Pt loaded over commercial support. Preliminary results indicate that Pt catalyst shows a 30 %higher SOQ conversion compared to Pd loaded catalyst. Stability studies using the Pt loaded over inhouse catalyst supports shows a maximum SO2 conversion of 47%for the first 11 hrs and 70%for the latter 15 hrs at an operating temperature of 400 °C. 5.Appendix: Table Al.Percentage of SO oxidation on in-house support and Pt-loaded support.(A calibration chart was used to relate GC counts with concentration). Peak area Peak Conversion sample |Temp areaof |[SOo]/[N2]% of N> SO, AlO3- ; 400 °C 1979531 235003 0.118717 0.073386 7.3% TiO, Pt 33.9% Al,03-400 °C 805158 58841 0.073080 0.3392399 TiO, 662 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008 663 Interim Draft Report Fed Grant Number EM-833233301-0 August 22,2008